Application of Inverse Pole Figure to Rietveld Refinement: II. Rietveld Refinement of Tungsten Liner using Neutron Diffraction Data

  • Kim, Yong-Il (Korea Research Institute of Standards and Science, P.O. Box 102) ;
  • Lee, Jeong-Soo (Korea Atomic Energy Research Institute, HANRO Utilization Research Group, P.O. Box 105) ;
  • Jung, Maeng-Joon (Department of Chemical Engineering, Sangju National University) ;
  • Kim, Kwang-Ho (Department of Inorganic Materials Engineering, Pusan National University)
  • 발행 : 2000.09.01

초록

The three-dimensional orientation distribution function of a conical shaped tungsten liner prepared by the thermo-mechanical forming process was analyzed by 1.525$\AA$ neutrons to carry out the Rietveld refinement. The pole figure data of three reflections, (110)(220) and (211) were measured. The orientation distribution functions for the normal and radial directions were calculated by the WIMV method. The inverse pole figures of the normal and radial directions were obtained from their orientation distribution functions. The Rietveld refinement was performed with the RIETAN program that was slightly modified for the description of preferred orientation effect. We could successfully do the Rietveld refinement of the strongly textured tungsten liner by applying the pole density of each reflection obtained from the inverse pole figure to the calculated diffraction pattern. The correction method of preferred orientation effect based on the inverse pole figures showed a good improvement over the semi-empirical texture correction based on the direct usage of simple empirical functions.

키워드

참고문헌

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