• Title/Summary/Keyword: yield conditions

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A Study on the Extraction of Alumina from Kaolin (카오린으로부터 $Al_2O_3$의 용출에 관한 연구)

  • 백용혁;이종근
    • Journal of the Korean Ceramic Society
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    • v.19 no.2
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    • pp.157-161
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    • 1982
  • The possibility of extraction of alumina from domestic Ha-dong kaolin was studied by sulfuric acid treatment. Raw kaolin was calcined at various temperature (500-110$0^{\circ}C$) and calcined kaolin were treated with sulfuric acid. The tendency of extraction yield of alpha alumina have been investigated by relating reaction time, temperature, and acid concentration. After reaction, precipitates were analyzed by DTA, TGA, and identified alpha alumina by X-ray diffractometer with calcined sample at 120$0^{\circ}C$. The results were as follows; 1. The optimum calcination temperature was 800-86$0^{\circ}C$. 2. The most suitable extracting conditions of alpha alumina were 40 wt%-$H_2SO_4$, 2-3 hours acid-treating time and 8$0^{\circ}C$ acid-treating temperature. 3. Precipitates were composed of $(NH_4)_2SO_4$, $Al_2SO_4(OH)_4$ 5-7 $H_2O$ and $Al(OH)_3$.

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Fabrication and Characterization of High Purity Al2O3 by Decomposition of Selicite (세리사이드 분해에 의한 고순도 Al2O3의 제조 및 특성에 관한 연구)

  • 이경희;박한수;송명신
    • Journal of the Korean Ceramic Society
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    • v.24 no.5
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    • pp.431-436
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    • 1987
  • High purity Al2O3 has been extracted from serlcite of clayminerals, selicite was treated by H2SO4(2N∼18N) solution, NH4OH treatment(PH8.5∼10.0) and metallic impurities such as Fe were removed by NaOH treatment. The tendency of extraction yield of ${\alpha}$-Al2O3 have been investigated by relating reaction time, acid concentration. Reaction products were analyzed by DT-TGA, chemical analysis and X-ray diffractometer. Prepared ${\alpha}$-Al2O3 power is fired in air at 1400$^{\circ}C$, 1600$^{\circ}C$ 2hr. The results are as follows; 1. The most suitable extracting conditions of ${\alpha}$-Al2O3 from Selicite were N-H2SO4, 120 min acidtreating time. 2. The optimum pH condition was 9.0. 3. Physical properties of sintered Al2O3 bodies were as follows. Relative density is 99%. Water absorption is 0.26%. Rock well hardness is 89.

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Transesterification for FAME production of Rapeseed Oil

  • Jeong, Gwi-Taek;Yun, Dae-Hyeon;Gang, Chun-Hyeong;Choe, Byeong-Cheol;Lee, Un-Taek;Park, Don-Hui
    • 한국생물공학회:학술대회논문집
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    • 2003.04a
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    • pp.164-168
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    • 2003
  • Fatty acid methyl esters (FAMEs) show large potential applications as diesel substitutes, and they are known as biodiesel fuel. Biodiesel fuel as a renewable energy is an alternative that can reduce energy dependence on petroleum and air pollution. Several processes for the production of biodiesel fuel have been developed. Transesterification process under alkali-catalysis and short-chain alcohol gives high level yield of methyl esters in short reaction times. In this research, transesterification of rapeseed oil was investigated to produce the FAMEs. Experimental reaction conditions included molar ratio of oil to alcohol, concentration of catalyst, types of catalysts, reaction time, and reaction temperature. The conversion ratio of rapeseed oil enhanced with the alcohol-oil mixing ratio and with the reaction temperature.

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A study on the stress distribution and plastic area propagation in the beams with a circular hole (원형공을 가진 보의 응력분포와 소성역 전파거동에 관한 연구)

  • 김희철;왕지석;이경호
    • Journal of Advanced Marine Engineering and Technology
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    • v.9 no.3
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    • pp.225-239
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    • 1985
  • The beams with a circular hole are often used for constructing structures. The center of the circular hole is normally located in neutral axis and the stress state around the hole due to bending moment is trivial. But the stress level around the hole due to shear force is expected to be significant especially in the case of beams made of shape steels. In this paper, the stress distributions around the circular hole of beams were presented. Using polar coordinates and generallized stress function, the formulas of stress components were derived. The aspects of plastic area propagations based on von Mises yield criteria were also shown graphically. In order to verify the formulas presented in this paper, a beam of I-shape steel with a circular hole was made and the strains around the hole were measured under various loading conditions. The experimental results were proved to coincide fairly well with the calculated values.

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Fluidized Bed Drying Effect on the Aerogel Powder Synthesis

  • Hong, Seong-Hoon;Lee, Dong-Kyu;Oh, Chang-Sup;Kim, Yong-Ha
    • Journal of Energy Engineering
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    • v.21 no.1
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    • pp.43-46
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    • 2012
  • A fluidized bed drying approach was utilized to the synthesis of water glass based silica aerogel powders. The effects of the fluidized bed drying conditions such as the superficial velocity and temperature of hot air and bead size as well as bead/wet-gel ratio, on the physical properties such as tapping density and productivity of the aerogel powders were systematically investigated. The experimental results showed that the amount of beads mixed with wet-gels in the fluidized bed column has the most profound impact on the fluidization efficiency, greatly enhancing the yield of the aerogel powders up to 98% with a proper bead/wet-gel weight ratio as compared to 72% without using beads. No significant change was observed in the tapping density over a wide range of the fluidized drying condition. Consequently the fluidized bed drying approach shows a good promise as an alternative route for the large-scale production of the aerogel powders.

A Study on Dyeing Properties of Cafionicagent Treated Cotton Fibre with Reactive Dye (캐티온화제 처리한 면섬유에 대한 반응성 염료의 염색성)

  • Jung, Young Jin;Lee, Young Hee;Kim, Kyung Hwan
    • Textile Coloration and Finishing
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    • v.6 no.4
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    • pp.46-53
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    • 1994
  • Polymer cationic agent was prepared by the initial polymerisation of epichlorohydrin followed by amination with diethylamine. Cotton fibre treated with the polymer (6~8% o.w.f.) is highly cationic and exhibit increased substantivity for reactive dyes under neutral to weakly acid conditions. The modified substrate could be dyed with reactive dyes without salt or a little salt from dye bath. The increased concentration of cationic agents resulted in an increase the colour yield. Futhermore, treated cotton has an electropositive surface charge. Adsorption of Reactive dye can be attributed to both van der waals force and electrostatic attraction.

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Design Analysis of Ride Comfort- and Driving Safety-control Strategies for the Continuously Controlled Semi-active Suspension Systems (연속 가변식 반능동형 현가시스템의 승차감 및 주행안전성 제어기 설계 해석)

  • 허승진;황성호;박기홍
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.14 no.1
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    • pp.17-23
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    • 2004
  • The semi-active suspension system is getting widely adopted in passenger vehicles for its ability to improve ride comfort over the passive suspension system while not degrading driving safety. A key to the success is to develop practical controllers that yield performance enhancement over the passive damper under various driving conditions. To this end, several control strategies have been studied and evaluated in this research in consideration of practical aspects such as nonlinearity and dynamics of the damper. From simulation results. it has been observed that, with the proposed control schemes, ride comfort can be significantly upgraded while suppressing degradation of driving safety.

반응표면분석(反應表面分析)과 그의 전산화(電算化)

  • Park, Seong-Hyeon
    • Journal of Korean Society for Quality Management
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    • v.7 no.1
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    • pp.3-14
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    • 1979
  • The primary objective of this paper is to aid the scientists and engineers in applying response surface procedures to obtain optimum operating conditions for many technical fields, particularly, for industrial manufacturing process. When a set of data is available from an experimental design, it is often of interest to fit a second order polynomial regression model in k independent variables, and find the condition of the independent variables (e. g., temperature, pressure, etc.) that optimize the response variable (e. g., yield, strength, etc.). This paper proposes a method how to obtain the optimum operating condition, and how 10 find the condition by using the computer. A computer program written in FORTRAN language is attached for the readers who may want to use the computer program.

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Effect of Ground Subsidence on Reliability of Buried Pipelines (지반침하가 매설배관의 건전성에 미치는 영향)

  • 이억섭;김동혁
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.1
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    • pp.173-180
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    • 2004
  • This paper presents the effect of varying boundary conditions such as ground subsidence, internal pressure and temperature variation for buried pipelines on failure prediction by using a failure probability model. The first order Taylor series expansion of the limit state function incorporating with von-Mises failure criteria is used in order to estimate the probability of failure mainly associated with three cases of ground subsidence. Using stresses on the buried pipelines, we estimate the probability of pipelines with von-Mises failure criterion. The effects of varying random variables such as pipe diameter, internal pressure, temperature, settlement width, load for unit length of pipelines, material yield stress and pipe thickness on the failure probability of the buried pipelines are systematically studied by using a failure probability model for the pipeline crossing ground subsidence regions which have different soil properties.

Microplant Module (마이크로 플랜트 모듈)

  • Seo J.H.;Shon J.M.;Cho J.Y.;Kwon Y.W.;Choe J.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.211-215
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    • 2005
  • Microsystems combine several microcomponents, optimized an entire system, to provide several specific technical functions by the shape of the microstructure. Microfabrication and micromachining techniques have played the key role in the fast development and commercialization of microsystems. Microreaction technology based on microsystems is a powerful tool for the evaluating new process and reaction pathways in chemical engineering. Because of the small characteristic dimensions of microreaction devices, mass and heat transfer processes are enhanced and, in addition, reaction conditions can be precisely controlled for optimizing yield and selectivity. The paper will report on the mixer design principle and explore several application fields of microreaction technology in the chemical synthesis

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