• 한국염색가공학회지
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• 제10권6호
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• pp.20-26
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• 1998

100％ viscose rayon fabric was treated with 1,2,3,4-butanetetracarboxylic acid (BTCA) by pad-dry-cure process in the presence of various catalysts. The dimensional stability, mechanical properties and hand values of fabric treated with BTCA were investigated. The ester-crosslinking reaction was influenced by the concentration of BTCA and type of catalyst. The fabric treated with BTCA was comparable or superior to that treated with conventional crosslinking agents such as dimethyloldihydroxyethyleneurea and 4,5-dihydroxy-1,3-dimethyl-2-imidazolidinone in respect of wrinkle recovery, shrinkproof property, retention of strength, and hand values. But in yellowing of fabric, the fabric treated with BTCA was inferior to that treated with conventional crosslinking agents. The fabric treated with BTCA/sodium formate was inferior to that treated with BTCA/sodium hypophosphite in respect of WRA, but had better strength retention and whiteness.

• 한국의류학회지
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• 제28권11호
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• pp.1507-1515
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• 2004

Washable wool was developed using environmental-friendly spray UV-cure technique. Photocrosslinkable polymer, dextran-methacrylate, was synthesized starting from natural biopolymer, dextran. The aqueous solution of dextran-methacrylate was applied to wool fabric with various concentrations to find out the optimum condition in minimizing felting shrinkage. The wool fabric subsequently cured by 365 nm UV, The effects of UV-cure time and photoinitiator concentration on felting behavior of wool were examined. As the concentration of dextran-methacrylate increased, the felting shrinkage decreased gradually. At concentration 0.5g/ml, the felting shrinkage of wool was negligible. Other properties such as air permeability, moisture content, wrinkle recovery, thickness and wettability were also evaluated. The surface coating of dextran polymer onto wool fiber was identified by SEM.

• 한국가정과교육학회지
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• 제7권1호
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• pp.1-10
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• 1995

This study was intended to provide an improved method for testing textiles in high school. Four kinds of test subjects were selected and applied to the classes. Problems of the methods in the textbooks were corrected as follows: 1)Burning test: The number of specimen is reduced to 3 kinds of fibers(cotton, wool, and polyester) and recommends are given to make result by comparing with the burning characteris-tics of paper and hair. 2) Absorbency test: Test Method is changed to drop test. The result is recorded by measuring time required for the water drops absorbed to the specimen. 3) Wrinkle recovery test: A glass is provided instead of metal weight. The method of measuring angle which is made by the specimen is shown in figure. 4) Effects of Detergent: 0.2% of detergent solution is provided before class. The amount of oil and carbon black is specified. Students have generally agreed that the improved methods were better than those in the text-books after they made the above 4 recommendable experiments(p<.001)

• 한국염색가공학회지
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• 제11권1호
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• pp.48-60
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• 1999

In this paper, a new regenerated celluosic fiber, "Tencel" was treated with cellulase enzyme. Also Tencel fabrics were pretreated with NaOH and dyed with various reactive dyes, and subsequently finished with DMDHEU. $\Delta{E}^*_{ab}$ value was calculated by measuring color difference before and after wet abrasion test to rubbing. The fibrillation propensity was estimated on Tencel by means of weight loss, $\Delta{E}^*_{ab}$ value, and SEM observation. Weight loss of NaOH pretreated Tencel fabric is more lower than that of original fabric. The cellulase treatment decreased tensile strength but improved wet abrasion strength, wrinkle recovery, and bending properties. Tendency of fibrillation for Tencel fabric was reduced by NaOH-pretreatment, dyeing with multifunctional reactive dyes, and afterfinishing by DMDHEU.by DMDHEU.

• 한국의류학회지
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• 제21권8호
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• pp.1346-1352
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• 1997

The purpose of this study was to help the consumer as well as the producer by investigating the properties such as tensile strength, extention, tear strength, wrinkle recovery, drapability, bending property, moisture regain, and shrinkage on commercial polyurethane coated fabrics. Seven commercial polyurethane coated fabrics having various base fabrics were used. The performance properties of base fabrics and polyurethane coated fabrics were measured. The relationships between base fabrics and polyurethane coated fabrics on the performance properties were identified. It was concluded that the properties of polyurethane coated fabric mainly depend on the characteristics of base fabric. Therefore the proper use of base fabric is recommended in order to improve the performance of polyurethane coated fabric.

• 한국염색가공학회지
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• 제2권1호
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• pp.14-20
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• 1990

The cotton fabrics were treated with formaldehyde in the presence of zinc nitrate catalyst and urea. The effects of HCHO concentration, urea concentration, catalyst ratio, cure time and cure temperature on the physical properties of fabrics were studied. Cotton fabric finished with HCHO and urea had the lower tensile strength and tear strength than untreated one. These strength losses resulted from tighter oxymethylene crosslinks. The enhanced wrinkle recovery for fabric treated with formaldehyde in the presence of urea was indicative of the formation of urea-formaldehyde polymer. These experimental conditions were set up according to table of orthogonal arrays.

• 한국의류학회지
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• 제30권3호
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• pp.481-486
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• 2006

한지를 의류용으로 사용하기 위한 시도들이 있었지만, 습윤상태에서 물리적 성질이 크게 감소한다는 문제점 때문에 많은 한계를 가지고 있었다. 따라서 한지의 습윤상태에서의 물리적 성질을 향상시키기 위해 내수성을 부여하고자, 실리콘 수지를 이용하여 한지에 발수가공을 행하였다. 패드-드라이-큐어 방법을 사용하여 처리하였고, 가공의 최적조건을 알아보기 위해 수지의 농도와 촉매의 농도, 큐어링 시간과 온도를 변화시켜 실험하였다. 한지의 발수도, 강연도, 방추도를 측정하였고, 습윤과 건조상태에서의 인장강도, 인열저항 마찰저항을 비교하였다. 그 결과 한지의 발수가공을 위한 최적처리조건은 실리콘 수지농도 40g/l, 촉매농도는 수지농도의 1/2인 20g/l, 큐어링 온도 160$^{circ}C$, 큐어링 시간 120초였다. 가공 후에도 한지의 유연성은 크게 저하되지 않았으며, 방추도는 약간 증가하였다. 가공 후, 건조상태에서의 인장강도, 인열저항은 큰 변화가 없었으나 내마모도는 증가하였고, 습윤상태에서의 인장강도, 인열저항, 내마모도 모두 증가하였다.

• 대한화장품학회지
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• 제30권4호
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• pp.515-524
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• 2004

쌀눈에서 추출한 inositol과 phytic acid를 화장품에 적용하기 위해 피부에 미치는 영향에 대해 연구하였다 $20{\~}40$대의 아시안 여성 45명을 대상으로 7주간 inositol $0{\~}3.0\;wt\%$와 phytic acid $0{\~}1.50\;wt%$가 함유된 스킨로션을 제조, 사용 후 피부의 수분, 유분, 탄력, 주름에 미치는 영향에 대해서 알아보았다 Inositol $1.0\;wt\%가$ 함유된 스킨로션을 사용한 경우 피부의 수분 함유량은 $19\%$ 증가하였으며, 주름은 $12.4\%$ 개선되었고, 피부탄력은 $12.4\%$ 증가되었다. 또한 phytic acid $0.50\;wt\%$를 함유한 스킨 로션을 사용한 경우 피부의 수분은 $71.6\%$ 증가하였으며, 주름은 $16.9\%$ 감소하였고, 탄력은 $21.9\%$가 증가하였다. Inositol과 phytic acid를 지성과 건성피부에 적용한 결과 $2{\~}4$주 후면 정상피부의 유분량으로 조절됨을 알 수 있었다 Inositol과 phytic acid는 모두 피부개선에 효과적이나, phytic acid는 민감한 피부에는 적용하기 어려운 점이 있다. 따라서 $1.0\;wt\%의$ inositol에 $0{\~}0.5\;wt\%$의 phytic acid를 첨가한 스킨로션을 제조하여 그 효과에 대해서 알아보았다. 이 경우 $1.0\;wt\%$의 phytic acid에 $1.0\;wt\%$의 inositol을 사용한 경우 수분은 $63.8\%$, 탄력은$17.2\%$ 증가하였으며, 주름은 $17.4\%$ 개선되었고, 피부 유분량은 약 2주 후에 정상적인 상태로 개선됨을 알 수 있었다. 따라서 inositol $1.0\;wt\%$에 $0.10\;wt\%$의 phytic acid를 첨가하여도 피부 개선효과가 나타남을 알 수 있다. 본 연구의 결과 내에서 $1.0\;wt\%$의 phytic acid와 $1.0\;wt\%$의 inositol을 사용한 경우 적은 양으로도 피부 개선 효과가 우수한 상승효과가 나타남을 알 수 있었다.

• KSBB Journal
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• 제23권6호
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• pp.513-518
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• 2008

재조합 대장균으로부터 베타-카로틴을 추출/정제하고 정제된 베타-카로틴의 주름개선 성능을 평가하였다. 탈수 용매, 추출 용매에 따른 추출량의 큰 변화는 발견되지 않았으나, wet-cell cake으로부터 추출한 경우가 dry cell로부터 추출한 경우에 비하여 2배 많은 양의 베타-카로틴이 추출되었다. 5 g의 wet-cell cake을 파쇄하고, 아세톤으로 탈수한 후, isobutyl acetate로 추출한 결과 36 mg의 베타-카로틴이 추출되었는데, 이는 61.2% 회수율에 해당한다. 베타-카로틴의 결정을 생성시키고 이를 분리한 결과 순도가 증가하였다. 재조합 대장균 배양액 2.5 L로부터 얻은 wet-cell cake 223 g의 탈수, 세포 파쇄 후 세포 잔사물로부터 베타-카로틴 추출, 농축, 결정화 등을 통하여 최종적으로 순도 93%인 베타-카로틴 결정 633 mg을 얻었다. 사람섬유아세포 배양을 통하여 정제된 베타-카로틴의 세포 독성 및 콜라겐 합성에 미치는 영향을 조사하였다. $1.7{\mu}M$의 베타-카로틴을 첨가 시 세포에 독성을 거의 나타내지 않았으며 콜라겐 합성양은 첨가하지 않은 경우에 비하여 1.4배 증가하였다. 본 결과는 저 유독성 용매를 사용하고 기존보다 간단한 방법을 사용하여 재조합 대장균으로부터 고순도의 베타-카로틴을 정제할 수 있고 이를 기능성 화장품의 주름개선제로 사용될 수 있음을 시사한다.

• 한국염색가공학회지
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• 제20권6호
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• pp.26-34
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• 2008

Wool fabric having high moisture content were treated with fluorocarbon-based water and oil repellent finishing agents by pad-dry-cure system. Three types of finishing agents which were regular-type or nano-type were adapted to compare the surface chemical composition, water and oil repellent property, crease recovery angle, and durability to repeated laundering. From the surface chemical compositions resulted by ESCA and C1s curve-fitting, it was shown that the regular-type finishing agent were easily taken off from the finished wool fabrics after repeated laundering. On the other hand, the fluoroalkyl groups of nano-type finishing agents turned round from fabric surface to fiber internal after repeated laundering. The water repellency of the wool fabrics treated with regular-type agent had a little changes according to the treatment condition changes and sharply decreased with repeated laundering. However, these values when treated with nano-type agents increased with the concentration and cure temperature and were maintained after 20 times laundering. The wool fabrics treated with nano-type agent had a great oil repellency irrespective of treatment conditions. Furthermore, the wrinkle recovery values of the wool fabrics treated with nano-type agents were higher than those of the fabrics treated with regular-type agent and were unchanged after 20 times laundering.