• Journal of the Korean Society of Clothing and Textiles
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• v.22 no.8
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• pp.1060-1068
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• 1998

The effects of various catalysts and softners on the anti-crease finish of ramie with glyoxal were investigated. A number of metal salts commonly used as Lewis acid catalysts in DP finishing of cotton with formaldehyde and N-methylol agents were screened for glyoxal treatment of ramie fabric. Various organic and inorganic acids were mixed with Lewis acid catalyst as co-catalysts to improve catalytic activity. As a result, the combination of aluminum sulfate and citric acid was proven highly effective in catalyzing the crosslinking of ramie cellulose by glyoxal under lower curing temperature. With a mixed catalyst, performance properties, such as whiteness and tearing strength as well as wrinkle recovery of treated ramie fabric were improved as compared with that treated with aluminum sulfate alone. Additional improvement of tearing strength and wrinkle recovery was achieved by applying silicons softner in the treatment bath.

• Fashion & Textile Research Journal
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• v.3 no.4
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• pp.367-372
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• 2001

Five kinds of commercial ramie and hemp fabrics were treated with cellulase under different concentrations. Samples were mercerized before enzyme treatment to investigate the effect of mercerization on cellulase enzyme treatment. Physical characteristics(weight loss, tear strength retention, wrinkle recovery, drape stiffness, dyeability) of cellulase enzyme treated and untreated samples were measured and compared. X-ray diffractions were examined to verify if there were any changes in their crystallinity of enzyme treated fabrics. Weight loss, wrinkle recovery and degree of crystallinity increased as the concentration of cellulase enzyme increased. In the meanwhile, tear strength retention and drape stiffness and dyeability decreased. Enzyme activity was more effective on mercerized samples. Particularly, there was distinct tendency to increase weight loss and flexibility.

• Journal of the Korean Society of Clothing and Textiles
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• v.20 no.6
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• pp.992-1001
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• 1996

The binding of polyethylene glycol (PEG, average molecular weight 600) to cotton fabrics was achieved by using pad-dry-cure process in the presence of citric acid, MgCl3·6H3O, DMDHEU, and TEAHCL. Treated fabrics were dyed with direct, acid, and basic dye. Wrinkle recovery angles, durable press rate, wettability, dyeability and color fastness to washing of all treated cottons were evaluated. The results of this study were as follows: 1. The wrinkle resistance of the PEG treated cottons was increased by increasing PEG and DMDHEU concentration. 2. The wettability of the PEG treated cottons was decreased by increasing PEG and DMDHEU concentration, increased by increasing TEAHCL concentration. 3. PEG/DMDHEU/TEAHCL treated cottons had greater affinity on direct, acid, and basic dye than untreated cottons, and dyeability of the modified cottons was improved compare to untreated fabrics. 4. Color fastness to washing of the PEG/DMDHEU/TEAHCL treated cottons was good except for the wash fastness of the direct dye.

• Textile Coloration and Finishing
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• v.14 no.1
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• pp.43-50
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• 2002

Silk/Cotton fabrics were treated with butanetetracarboxylic acid(BTCA) to improve crease recovery and anti-shrinking properties at various curing temperatures and pH values. We investigated the effects of finishing conditions on add-on of BTCA, bending property(E, 2HB), wrinkle recovery angle, shrinkage, and dyeing properties. The Add-on of BTCA increased with increasing curing temperature and concentration. Crease recovery was improved with decreasing shrinkage. Maximum add-on of BTCA was showed at pH 2.5. In case of dyeing and mercerization, silk side treated with BTCA was more flexible than untreated, whereas cotton side was more stiff. In dyeing after mercerization, B and 2HB values were higher and K/S values were doubled nearly. The hand of fabric improved with decreasing B and 2HB by the BTCA treatment. BTCA treatment after reactive dyeing improved crease recovery, and caused no change of color difference. However, BTCA treatment after reactive dyeing didn't improve crease recovery, whereas B and 2HB were decreased considerably by the treatment.

• Journal of the Korean Society of Clothing and Textiles
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• v.41 no.3
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• pp.458-467
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• 2017

There is increased interest in clothes dryers and garments made of spandex-blend woven fabrics; however, there is limited information available for the laundering and drying these clothes. This study investigates the effects of washing and drying on shrinkage, skewness, and wrinkle for woven fabrics with and without spandex. When spandex with good elastic recovery was blended, the deformed shape from washing and drying improved skewness and wrinkle by easily returning to its original shape. However, these properties had a negative effect on shrinkage in terms of length and area change. When the influence of clothes maintenance was classified, the drying process had the biggest influence of 58%, followed by spinning-rinsingwashing. Tumble drying, in which the fabric is exposed to mechanical force and heat for a long period, had more negative effects on the dimensional stability than line drying. The spandex blend had the effect of preventing skewness and wrinkle in garments, but it was also shown to accelerate shrinkage by garment maintenance cycles. It was important to control drying in order to reduce shrinkage during the maintenance process; consequently, this had the greatest influence on the dimensional stability of fabrics. Therefore, line drying was more advantageous for spandex-blend fabrics than tumble drying in terms of management for shrinkage, skewness, and wrinkle.

• Textile Coloration and Finishing
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• v.24 no.3
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• pp.221-231
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• 2012

Rayon fabrics were treated with some commercial non-formaldehyde and low-formaldehyde resins, and then their effect on the physicochemical properties of fabrics, including formaldehyde release, tear strength, shrinkage, and wrinkle recovery, were investigated respectively. Rayons treated with non-formaldehyde resin, little formaldehyde release was observed. Considering other factors, the optimal concentration of non-formaldehyde resin was shown to be 11-13%, and curing temperature was $170{\sim}175^{\circ}C$. In case of low-formaldehyde type, 9-11% resin concentration and curing temperature of $170{\sim}180^{\circ}C$ were recommended for optimal finishing condition. The choice and combination of resins and catalysts were also important factors, and preliminary considerations before resin-finishing of rayon are also important to get much better results.

• Journal of the Korean Society of Clothing and Textiles
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• v.13 no.3 s.31
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• pp.242-251
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• 1989

The purpose of this study was to investigate the changes in easy-care and strength properties of the wet fixation processed viscose rayon fabrics. Rayon fabrics were treated with mixed resins of melamine formaldehyde (MF) and DMDHEU by one bath and two bath wet fixation processes. The MF/DMDHEU mixed resin concentrations were 50/100, 50/150, 100/100, 100/150 and 150/100(g/1). Magnasium chloride was used as a catalyst. Treated fabrics were evaluated by nitrogen content, DP rating, wrinkle recovery angle, breaking strength, tearing strength and abrasion resistance. The properties were compared to the fabrics treated by conventional Pad-Dry-Cure (PDC) method. Wet fixation processed fabrics showed DP ratings of higher than 3 and higher than 275 degrees of wrinkle recovery angles in all the mixed resin concentrations. Wet fixation processed fabrics showed increase in breaking strength and tearing strength but decrease in abrasion resistance. However, the decrease in abrasion resistance was much less than the conventional PDC treated fabrics. The one bath wet fixation processed fabrics showed better physical properties than the two bath processed fabrics in general. The optimum treatment condition was the mixed resin concentration of MF/DMDHEU, 100/100 g/l in one bath wet fixation process.

• Journal of the Korean Society of Clothing and Textiles
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• v.22 no.7
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• pp.862-871
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• 1998

In this study, the effect of sizing on the physical and mechanical characteristics of Hansan ramie was studied. 2 kinds of Hansan ramie were used for this study and one kind of the chinese ramie was also used for comparing with the characteristics of Hansan ramies. The following results were obtained from this experimental study. The wrinkle recovery angle was gradually reduced according to the increasing of the concentration of sizing agent. As the size agent could easily penetrate between the thick yarms, the effect of sizing on the wrinkle recovery angle was evident on the Chinese and Hansan coarse ramie. The result of KES-F system showed that the sizing affected much on the bending properties and shear properties. As the size concentration was increased the shear properties were increased more evidently on the Chinese and Hansan coarse ramie. The result of KES-F system showed that the sizing affected much on the bending properties and shear properties. As the size concentration was increased the shear properties were increased more evidently than the bending properties. The other mechanical properties didn't changed much by sizing. The calculated primary hand value also showed that the ramie became more stiff after sizing.

• Textile Coloration and Finishing
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• v.9 no.5
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• pp.30-41
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• 1997

A purpose of this research is to prove unknown relation -ship between finish bath pH and crosslinking. In pursuit of these goals, we have treated 100% cotton broad cloth with PTCA and BTCA at different pH values. They were used with H$_{3}$PO$_{4}$, NaH$_{2}$PO$_{2}$, NaH$_{2}$PO$_{4}$, Na$_{2}$HPO$_{4}$, Na$_{3}$PO$_{4}$, catalysts to produce nonformaldehyde fabrics finishes. Treatments were applied to all cotton fabrics using a parletry-cure process. For the fully understood on the relationship of finish bath pH effect and cotton cellulose esterification, the relative concentrations of chemical species were calculated from ionization constants. The effect of pH on the cotton cellulose ester was investigated using Fourier transform infrared spectra, the surface area measurement by BET method and wrinkle recovery analysis. Results of differential FT-IR spectra and their relative concentration analysis were compared with those of catalyst treated controls. FT-IR and wrinkle recovery data indicated that the esterfication by polycarboxylic acids is pridependent. A similar phenomenon also occurred when a phosphate or hypophosphite was used. Therefore, it is necessary to choose the optimum pH range of a finishing bath in order to achieve the most effective esterification.

• Textile Coloration and Finishing
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• v.24 no.2
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• pp.121-130
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• 2012

Cotton fabrics were treated with some commercial non-formaldehyde and low-formaldehyde resins, and then their effect on the physicochemical properties were respectively investigated including formaldehyde release, tear strength, shrinkage, and wrinkle recovery. Formaldehyde release less than 10ppm was obtained only by non-formaldehyde resin. Considering other factors, the optimal concentration of non-formaldehyde resin was shown to be 9-11%. In case of low-formaldehyde type, 5-7% resin concentration and curing temperature of $160{\sim}170^{\circ}C$ were recommended for optimal finishing condition. The choice and combination of resins and catalysts were also important factors, and preliminary considerations before treating cotton fabrics with resins used in this study are also important to get much better results.