• Title/Summary/Keyword: wet strength

Search Result 643, Processing Time 0.023 seconds

Effects of dentin moisture on the push-out bond strength of a fiber post luted with different self-adhesive resin cements

  • Turker, Sevinc Aktemur;Uzunoglu, Emel;Yilmaz, Zeliha
    • Restorative Dentistry and Endodontics
    • /
    • v.38 no.4
    • /
    • pp.234-240
    • /
    • 2013
  • Objectives: This study evaluated the effects of intraradicular moisture on the pushout bond strength of a fibre post luted with several self-adhesive resin cements. Materials and Methods: Endodontically treated root canals were treated with one of three luting cements: (1) RelyX U100, (2) Clearfil SA, and (3) G-Cem. Roots were then divided into four subgroups according to the moisture condition tested: (I) dry: excess water removed with paper points followed by dehydration with 95% ethanol, (II) normal moisture: canals blot-dried with paper points until appearing dry, (III) moist: canals dried by low vacuum using a Luer adapter, and (IV) wet: canals remained totally flooded. Two 1-mm-thick slices were obtained from each root sample and bond strength was measured using a push-out test setup. The data were analysed using a two-way analysis of variance and the Bonferroni post hoc test with p = 0.05. Results: Statistical analysis demonstrated that moisture levels had a significant effect on the bond strength of luting cements (p < 0.05), with the exception of G-Cem. RelyX U100 displayed the highest bond strength under moist conditions (III). Clearfil SA had the highest bond strength under normal moisture conditions (II). Statistical ranking of bond strength values was as follows: RelyX U100 > Clearfil SA > G-Cem. Conclusions: The degree of residual moisture significantly affected the adhesion of luting cements to radicular dentine.

Characteristics of Natural Hydraulic Lime Mortar Mixed with Basalt Fiber (바잘트 섬유를 혼합한 천연수경성석회 모르타르의 특성)

  • Moon, Ki-Yeon;Cho, Jin-Sang;Cho, Kye-Hong;Hong, Chang-Woo
    • Resources Recycling
    • /
    • v.24 no.6
    • /
    • pp.61-68
    • /
    • 2015
  • In this study, the strength properties of NHL based mortar with blending basalt fiber were investigated. In the first step, it was evaluated that physical properties of NHL based mortar according to mixing method of four types of basalt fiber and then mixing method of one type was selected. As a result of assessment, it showed that the physical properties with mixing method of dry blending were better than that of wet blending and mixing method that basalt fiber pre-mixed with NHL for 5 min in a blender was selected and water and aggregate were finally added. Secondly, the investigation of blending fiber length on the compressive and flexural strength for basalt fiber reinforced NHL based mortars was carried out. The compressive strength was decreased with adding fiber, and the flexural strength was increased more than plain mortar. In the case of adding 6 mm fiber, the compressive and flexural strength were improved more than that of others.

Formation of Hydrophobic Self-assembled Monolayers on Paper Surface with Silanes (실란화 반응에 의한 종이 표면의 소수성 자기조립 단분자막 형성)

  • Oh, Min-Jeong;Lee, Hyoung;Paik, Ki-Hyon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
    • /
    • v.42 no.1
    • /
    • pp.64-73
    • /
    • 2010
  • This study was conducted to modify the surface properties of papers by formation of hydrophobic self-assembled monolayer(SAM) on paper surface with silanes. A base paper I(0.5% AKD) and base paper II(1.0-1.5% AKD) were reacted with silanes(PFDTES, DMDCS, MODDCS) by immersion method and vapor deposition method. Hydrophobic SAMs(contact angle value>$120^{\circ}C$) were obtained on all papers after treatment with $10^{\mu}l$ PFDTES for 15min, with $50^{\mu}l$ DMDCS for 30min, with $50^{\mu}l$ MODDCS for 300min. When applying PFDTES to paper surface, lower silane concentration and shorter reaction time were required, whereas MODDCS with long alkyl chain required the longest reaction time of 300min. The st$\ddot{o}$ckight sizing degree of silane treated papers were increased between 105sec(base paper I) and 130sec(base paper II). The wet tensile strength of PFDTES-treated base papers(I, II) increased by 10-34% after SAM formation. However, the wet tensile strength of the DMDCS-treated base paper(I) was found to decrease from 0.067kN/m to 0.038kN/m; this may due to the cellulose degrading as a result of generated hydrogen chloride when hydroxyl group of cellulose were reacted with DMDCS. No apparent changes of PPS roughness on silane-treated papers are observed. The ATR-IR spectrum showed absorption peak located at 465 and 1200cm-1 which can be assigned to the Si-O-C asymmetric stretching and Si-O-C bonds, respectively.

Fermented soybeans by Rhizopus oligosporus reduce femoral bone loss in ovariectomized rats

  • Yoo, Hyun-Wook;Chang, Moon-Jeong;Kim, Sun-Hee
    • Nutrition Research and Practice
    • /
    • v.8 no.5
    • /
    • pp.539-543
    • /
    • 2014
  • BACKGROUND/OBJECTIVES: Soy isoflavones are structurally similar to estrogen and bind to estrogen receptors, suggesting that they exhibit estrogenic activities; therefore, they are referred to as phytoestrogens. Fermentation may affect the bioavailability of isoflavones altering soy isoflavone glycosides in the form of aglycones. Thus, this study investigated the effects of fermented soybeans by Rhizopus oligosporus on bone metabolism in both young rats as a pilot test and in ovariectomized (ovx) old rats as a model of menopause. MATERIALS/METHODS: In the pilot test, a total of 24 seven-week-old female Sprague-Dawley (SD) rats were fed one of three diets for a period of four weeks: casein, unfermented soybean product, or fermented soybean product by R. oligosporus. In the ovx rat model, 20-week-old SD rats weighing 260-290 g underwent either sham-operation (n = 10) or bilateral ovariectomy (n = 30) and were then fed the AIN-93M diet for one week. Thereafter, rats were fed sham-casein, ovx-casein, ovx-soybean, or ovx-fermented soybean diet for five weeks. After decapitation, femoral bones were isolated and preserved in 9% formalin for assessment of bone mineral density (BMD), bone mineral content (BMC), and bone-breaking strength (BBS). RESULTS: Ovx rats showed significantly increased weight gain and decreased uterine wet weight. Of particular interest, ovx rats fed fermented soybeans showed increased uterine wet weights compared to control rats. Fermented soybean diet caused a significant increase in plasma 17-${\beta}$ estradiol concentrations in young rats, and 17-${\beta}$ estradiol levels were enhanced in ovx rats to match those of sham-operated ones. Significantly lower femoral BMD and BMC were observed in ovx rats compared to sham-operated controls, whereas bone areas did not differ statistically among the groups. In addition, BBS tended to be increased in ovx rats fed soybeans and fermented soybeans. CONCLUSIONS: Supplementation of fermented soybeans could have preventive and therapeutic effects against osteoporosis in postmenopausal women.

Strength and Durability of Polymer-Modified Mortars Using Ground Granulated Blast-Furnace Slag (고로슬래그 미분말을 혼입한 폴리머 시멘트 모르타르의 강도 및 내구성)

  • 주명기;김남길;연규석
    • Journal of the Korea Concrete Institute
    • /
    • v.14 no.2
    • /
    • pp.164-170
    • /
    • 2002
  • Effect of the polymer-binder ratio and slag content on the properties of combined wet/dry-cured polymer-modified mortars using granulated blast-furnace slag are examined. Results shows that the flexural and compressive strengths of polymer-modified mortar using the slag tend to increase with increasing slag content, and reaches a maximum at a slag content of 40 %, and is inclined to increase with increasing polymer-binder ratio. Water absorption, carbonation depth and chloride ion penetration depth tend to decrease with increasing polymer-binder ratio and slag content. Accordingly, the incorporation of slag into polymer-modified mortars at a slag content of 40% is recommended for a combined wet/dry curing regardless of the types of polymer.

Effects of Silane-treated Silica on the Cure Temperature and Mechanical Properties of Elastomeric Epoxy (실란 커플링제로 처리된 실리카가 탄성에폭시의 경화온도 및 기계적 물성에 미치는 영향)

  • Choi, Sun-Mi;Lee, Eun-Kyoung;Choi, Seo-Young
    • Elastomers and Composites
    • /
    • v.43 no.3
    • /
    • pp.147-156
    • /
    • 2008
  • In this work, epoxy/carboxyl-terminated butadiene acrylonitirile (EP/CTBN) composites were prepared by employing a reinforcing filler, silica treated with silane coupling agent in different ratio by dry and wet method. Their curing characteristics, surface free energy, interface morphologies and mechanical properties such as tensile strength and impact resistance were carefully investigated. Differential scanning calorimetry(DSC) results showed that curing temperature was lowered with the increase of silane coupling agent because of the increase of relative curing agent cotent by filling the pores of silica. Wet method was proved to be more effective for lowering curing temperature of EP/CTBN composite. In general, surface free energy and impact resistance were increased with the increase of silane coupling agent in this work. Tensile strength, however, was observed to be decreased at 4 wt% of silane coupling agent. It was found that the dry method was proved to be preferable for pretreatment of silica with coupling agent.

The Evaluation of the Application of Modified Wood Powder Spacers to Liner Board Mill Trials (개질처리된 목질계 스페이서의 산업용지 생산현장 적용평가)

  • Seo, Yung Bum;Yoon, Doh-Hyun;Sung, Yong Joo;Gwon, Wan-Oh;Kim, Jin-doo
    • Journal of Korea Technical Association of The Pulp and Paper Industry
    • /
    • v.47 no.5
    • /
    • pp.98-103
    • /
    • 2015
  • The reduction of the energy consumption in papermaking process become more important issue because of the regulation of green house gas (GHG) emission. Since more than half of energy for papermaking process is consumed during drying process, the increase of the drying efficiency would be very important solution for saving energy and reduction of GHG emission. The improvement of drying efficiency could be very difficult for the liner board mill because the liner board are usually made of recycled paper, OCC (old corrugated container). The short fiber and fines originated the OCC lead to compact sheet structure and delay the water flow out during wet pressing process and drying process. The application of lignocellulose spacer could provide more loose wet sheet structure and result in the higher drainage rate and the improved drying efficiency. In this study, the effects of the application of lignocellulose spacer to the liner board mill were evaluated based on the mill trial. In order to overcome the common disadvantage of the spacer, the loss of strength properties, the spacer was pretreated with amphoteric polyelectrolyte during mill trial. The results showed the application of pretreated spacer improved the drying efficiency by reducing steam consumption. And the loss in the strength properties by the spacer could be supplemented by the pretreatment.

Effect of Processing Agent on Physical Properties of Leather (혁의 물성에 미치는 가공제 첨가 효과)

  • Lee, Jong-Seok;Seo, Gyo-Taeg;Kim, Young Chai;Moon, Sei-Ki
    • Applied Chemistry for Engineering
    • /
    • v.10 no.6
    • /
    • pp.934-938
    • /
    • 1999
  • Effect of processing agents on physical properties on aniline-type leathers such as wet blue, crust leather, and finished leather has been investigated. These leathers were manufactured from pelts obtained by the chemical, the enzyme, and the bio-tech treatment. There was no difference in physical properties between crust leather and finished leather. All finished leathers with the three treatments were satisfied with the Korean Industrial Standard like a tensile strength of $1.2kg_f/mm^2$, an elongation of 30%, a tear strength of $3.0kg_f/mm$, a grain crack weight of $15kg_f$, and a $Cr_2O_3$ content of 2.5%. In peculiar, application of the bio-tech treatment gave the best leather. This improvement of physical quality could be explained by the results of SEM and image analyser.

  • PDF

Synthesis and Biocompatibility of the Hydroxyapatite Ceramic Composites from Tuna Bone(II) - The Sintering Properties of Hydroxyapatite Treated with Wet Milling Process - (참치 뼈를 이용한 Hydroxyapatite 세라믹 복합체의 합성 및 생체 친화성(제2보)-습식법에 의한 Hydroxyapatite 소결체의 특성-)

  • Kim, Se-Kwon;Choi, Jin-Sam;Lee, Chang-Kook;Byun, Hee-Guk;Jeon, You-Jin;Lee, Eung-Ho
    • Applied Chemistry for Engineering
    • /
    • v.8 no.6
    • /
    • pp.1000-1005
    • /
    • 1997
  • The properties of ceramics by solid-state reaction with hydroxyapatite[$Ca_{10}(PO_4)_6(OH)_2$], which was isolated from tuna bone by wet milling process were investigated. The bulk density $2.93g/cm^3$ at $1350^{\circ}C$ was close to the calculated density $3.21g/cm^3$. On X-ray measurements, the major phases were identified as hydroxyapatite at below $1300^{\circ}C$, but the whitlockite [$Ca_3(PO_4)_2$] phases were appeared due to a decomposition of hydroxyapatite with temperature. The microstructures of sintering specimens were shown as small closed pores between grain boundaries. The mean bending strength of the sintered hydroxyapatite by solid-state reaction is about 58 MPa and this value is higher than that of the articular cartilage maximum strength, 40MPa.

  • PDF

Adhesion Properties of Urea-Melamine-Formaldehyde (UMF) Resin with Different Molar Ratios in Bonding High and Low Moisture Content Veneers

  • Xu, Guang-Zhu;Eom, Young-Geun;Lim, Dong-Hyuk;Lee, Byoung-Ho;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
    • /
    • v.38 no.2
    • /
    • pp.117-123
    • /
    • 2010
  • The objective of this research was executed to investigate the effect of molar ratio of formaldehyde to urea and melamine (F/(U+M)) of urea-melamine-formaldehyde (UMF) resin on bonding high and low moisture content veneers. For that purpose, UMF resin types with 5 different F/(U+M) molar ratios (1.45, 1.65, 1.85, 2.05, and 2.25) synthesized were used in present study. First, their curing behavior was evaluated by differential scanning calorimetry. Second, their adhesion performance in bonding high and low moisture content veneers was evaluated by probe tack and dry and wet shear strength tests. Curing temperature and reaction enthalpy decreased with the increase of F/(U+M) molar ratio. And the dry and wet shear strengthsof plywood manufactured from low moisture content veneers were higher than thoseof plywood manufactured from high moisture content veneers. Also, the maximum initial tack force on the low moisture content veneer was higher than that on the high moisture content veneer.