• Title/Summary/Keyword: viscosity agent

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Rheological Properties and Cure Kinetics of Cycloaliphatic/DGEBA Epoxy Blend System Initiated by Cationic Latent Curing Agent (잠재성 경화제를 이용한 Cycloaliphatic/DGEBA계 에폭시 블렌드 시스템의 유변학적 특성 및 경화 동력학)

  • 곽근호;박수진;이재락;김영근
    • The Korean Journal of Rheology
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    • v.10 no.4
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    • pp.227-233
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    • 1998
  • The effects of 1 mol% N-benzylpyrazinium hexafluoroantimonate(BPH) as a thermal latent initiator and blend compositions composed of cycloaliphatic and DGEBA epoxies were investigated in the rheological properties and cure kinetics. Latent properties were performed by measurement of the conversion as a function of reaction time using isothermal DSC at $150^{\circ}C$ and $50^{\circ}C$ Rheological properties of the blend systems were investigated in terms of isothermal experiments using a rheometer. The gelation time was obtained from the evaluation of storage modulus (G'), loss modulus (G") and damping factor (tan$\delta$)). Cross-linking activation energy ($E_c$) was also determined from the Arrhenius equation based on gel time and curing temperature. As a result, the gel time and cross-linking activation energy increased with increasing DGEBA composition. The cure activation energies ($E_a$) were obtained by Kissinger method using dynamic DSC thermograms. In this work, the cure activation energy decreased with increasing CAE concentration, which might be resulted from the short repeat units, simple side-groups and viscosity of reaction media.edia.

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Characteristics of Flour Ferment Using Lactobacillus acidophilus as Starter (Lactobacillus acidophilus로 발효시킨 밀가루 발효물의 특성)

  • Cha, Wook-Jin;Lee, Si-Kyung;Lee, Jeong-Hoon;Cho, Nam-Ji
    • Korean Journal of Food Science and Technology
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    • v.36 no.1
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    • pp.116-122
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    • 2004
  • Growth of Lactobacillus acidophilus in flour was investigated for production of noodle and bread. L. acidophilus grew when fermented in flour, and growth continued upon fermentation with salt for 72 hr. pH of L. acidophilus-fermented flour with salt decreased up to 72 hr, reaching 3.06. Fermented flour with salt showed no decomposition as compared to that without salt. In flour fermented by L. acidophilus, amounts of lactic and acetic acids produced increased with incubation time, and reached, after 72 hr incubation, 6,821 and 0.191 mg/g, respectively, resulting in significantly higher production of lactic acid. Viscosity of fermented flour with salt increased, whereas that without salt decreased with incubation time. Results reveal L. acidophilus-fermented flour with salt could be applied as effective agent in noodle and bread productions.

Preparation and Properties of Ethylene Vinyl Acetate/Ethylene-1-Butene Copolymer Blend Based Foam (Ethylene Vinyl Acetate / Ethylene-1-Butene Copolymer 블렌드 발포체의 제조와 특성)

  • Cha, Gil-Soo;Kim, Jin-Tae;Yoon, Jung-Sik;Kim, Won-Ho
    • Elastomers and Composites
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    • v.36 no.1
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    • pp.14-21
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    • 2001
  • To increase the properties of EVA foam such as tensile strength, rebound resilience, and compression set, ethylene-1-butene copolymer (EtBC) was blended with EVA. After that crosslink characteristics of the blends and cell structures and mechanical properties of the foam were studied. As the amount of EtBC increased in EVA/EtBC blends, torque values of oscillating disc rheometer(ODR) increased and the foaming ratio decreased because the viscosity and crosslink density of EVA/EtBC blends increased. Foaming ratio and cell size of the foam increased by increasing the amount of foaming agent. When compared the mechanical properties of the foam which have same densities, tensile strength, rebound resilience, and compression set properties of the foam were improved by increasing the amount of EtBC in the EVA/EtBC blends.

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Suggestion of Segregation Evaluation Method based on Evaluation Index for Segregation(EIS) (재료분리 평가정수(EIS)에 의한 재료분리 평가법의 제안)

  • Han, Cheon-Goo;Kim, Gi-Cheol;Park, Byung-Kwan
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.923-926
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    • 2008
  • Currently more high flow and high performance concrete is used for construction of buildings in the world. However, when high flow and high performance concrete put high performance water reducing agent in quantity to improve flow, it has a negative effect on concrete structures since segregation arises from it though flow will be improved. There are naked-eye observation, coarse aggregate washing test, L Flow test for permeation among reinforcing rods and measurement of viscosity to judge concrete segregation resistance. However, it is difficult to apply them to practical affairs since they are very complicated and troublesome. Therefore, the study analyzed EIS dividing slump flow value into slump value, how to valuate concrete segregation resistance more easily, on the basis of the existing reference materials to propose EIS. As the results, in the event of high flow concrete, it is desirable that EIS value is prescribed to be less than 2.5 at the time of managing segregation. Also, at the time of prescribing EIS with performance, it is judged that it is desirable to manage segregation as less than 2.2 (Grade 1), 2.2$\sim$2.4 (Grade 2) and more than 2.6 (Grade 3).

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Physicochemical and Sensory Properties of Yogurt Supplemented with Corni fructus during Storage

  • Noh, Hyo Ju;Seo, Hye Min;Lee, Jun Ho;Chang, Yoon Hyuk
    • Preventive Nutrition and Food Science
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    • v.18 no.1
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    • pp.45-49
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    • 2013
  • This study was carried out to determine a possibility of adding Corni fructus extract (CFE) into yogurt for improving the neutraceutical properties of yogurt and the effects of adding CFE (2~6%, v/v) on the physicochemical and sensory properties of the products during a 15-day storage period at $4^{\circ}C$. Incorporation of CFE into the yogurt samples resulted in a significant pH reduction and a significant increase in titratable acidity. When evaluating the color of the yogurt, the $L^*$-values were not significantly influenced by CFE supplementation; however, the $a^*$- and $b^*$-values significantly increased with the addition of CFE during storage. The power law and Casson models were applied to assess the flow behavior of CFE-added yogurt samples. The magnitudes of apparent viscosity (${\eta}_{a,100}$), consistency index (K), and yield stress (${\sigma}_{oc}$) for 4~6% CFE yogurt samples were significantly greater than those for the control, indicating that CFE can be used as a thickening agent for yogurt. The sensory test revealed that addition of CFE (2~4%) to yogurt did not significantly affect the overall scores, but the overall preference score for 6% CFE yogurt was significantly decreased. Based on the data obtained from the present study, we concluded that the concentrations (2~4%) of CFE could be used to produce a CFE-added yogurt without the significantly adverse effects on the physicochemical and sensory properties.

Restoration and Reproduction Study for Antique Documents (고문서 복원 및 재현 시스템 연구)

  • Kim, Young-Sung;Kim, Su-Ho;Shin, Jong-Il;Park, Soo-Youl;Shin, Seung-Rim;Jun, Kun;Son, Young-A
    • Textile Coloration and Finishing
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    • v.21 no.2
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    • pp.48-53
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    • 2009
  • Reproduction of antique document is of importance with the concept of sharing the their contents and original aspects in terms of textual and artistic message. 'Pine tree ink stick' and 'Oil ink stick' are greatly enjoyed in their uses in the most written documentary works. Thus, it is said that the approach of this study has implied considerable meanings to cultural aspects. In this work, we have performed to investigate the reproduction and restoration study for antique documents. With comparison and analysis of some types of "ink stick", we have prepared several ink samples, controlling viscosity, surfactant, thickness agent, and applied these inks to the target antique document. Several reproduced samples showed a practical application possibility in terms of reproduction and restoration.

Studies on the Application of Starch for paper surface sizing(III) - The influence of surface sizing treatment with starch on the quality of uncoated printing paper - (종이 표면 사이즈 프레스용 전분의 적용에 관한 연구 -표면 사이즈용 전분이 백상지 품질에 미치는 영향 -)

  • 윤지영;이용규
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.34 no.2
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    • pp.1-12
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    • 2002
  • Starch dissolved in paper-mill wastes, either as a result of poor retention on the paper web or recycling of surface-treated broke, was a major pollutant Laboratory tests were performed by using different kinds of starch as a surface treatment. It was concluded that the use of cationic starch can positively affect the level of starch dissolved in liquid effluents. When cationically modified starches were used for surface sizing, the starch was tightly bound to the paper fibers, it was not removed during the repulping of broke. The result of mill trial in fine paper manufacture for the application of low-viscosity cationic starches used in size press reduced COD load in the effluents and increased One Pass Retention. It had been found that when cationic starch used as a surface sizing agent, more starch was retained on or near the surface of the sheet than with conventional oxidized starches. Thus surface strengths and quality were improved. In addition it is possible to maintain the desired level of starch penetration into the fiber net and improve porosity, opacity and brightness. In contrast, in most cases, dusting problems are notably eliminated. Cationic surface sized starch improved black and color ink-jet print quality in terms of feathering and optical density of the print image. These improved properties were believed to be due to a combination of fiber bonding and surface orientation more uniform starch concentration on the paper surface was resulted. Moreover cationic charges in the paper surface lend themselves excellently to fix ink jet ink anionic in nature.

Study on the Epoxy/BaTiO$_3$Embedded Capacitor Films for PWB Applications (인쇄회로기판 용 Epoxy/BaTiO$_3$내장형 커패시터 필름에 관한 연구)

  • 조성동;이주연;백경욱
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.4
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    • pp.59-65
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    • 2001
  • Epoxy/$BaTiO_3$composite capacitor films with excellent stability at room temperature, uniform thickness, and electrical properties over a large area ware successfully fabricated. The composite capacitor films with good film formation capability and easy process ability were made from epoxy resin developed for ACF as a matrix and two kinds of $BaTiO_3$powders as fillers to increase the dielectric constant of the composite film. The crystal structure of the powders and its effects on dielectric constant of the films were investigated by X-ray diffraction (XRD). And the optimum amount of dispersant, phosphate ester, was determined by viscosity measurement of suspension. DSC and dielectric property tests were conducted to decide the right curing temperature and the optimum amount of the curing agent. As a result, the capacitors of 7 $\mu \textrm{m}$ thick film with 10 nF/$\textrm{cm}^2$ and low leakage current were successfully demonstrated.

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Crosslinking Characteristics of High Density Polyethylene by Reactive Melt Processing (반응 용융 가공에 의한 고밀도 폴리에틸렌의 가교 특성 연구)

  • Lee Jong Rok;Lee Dong Gun;Hong Soon Man;Kang Ho-Jong
    • Polymer(Korea)
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    • v.29 no.4
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    • pp.385-391
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    • 2005
  • Reactive melt processing has been carried out to investigate crosslinking characteristics of high density polyethylene OTDPE) with dicummyl peroxide (DCP) and perbutyle peroxide (PBP). The increase of torque in the internal mixer indicated that the crosslinking in HDPE has been occurred by peroxides. As a result, the substantial decrease of density, melting temperature, and melt enthalpy were found while the melt viscosity increased in partially crosslinked HDPE. In the mechanical properties of partially crosslinked HDPE, the increase of maximum strength and the decrease in elongation at break were clearly noticed and these were more pronounced when PBP was applied as a crosslinking agent. It seems that the maximum strength was obtained with reactive processing temperature at $150^{circ}C$, however, the mixing time did not affect to the strength of partially crosslinked HDPE.

Characteristics of Germinated Colored Rice as a Potential Raw Material for Sikhe (잠재적 식혜원료로서 발아유색미의 특성)

  • Kim, Suk-Shin;Kim, Sang-Yong;Lee, Won-Jong
    • Korean Journal of Food Science and Technology
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    • v.30 no.5
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    • pp.1092-1096
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    • 1998
  • This work was to study the possibility of using germinated colored rice as a raw material for sikhe. Colored rice was soaked in water at $15^{\circ}C$ for 2 days and then germinated at 15, 20, 25 and $30^{\circ}C$ for upto 10 days. The higher the germination temperature, the higher the germination speed, the rate of increase in ${\alpha}-amylase$ activity, and the rate of increase in extract and its sugar content. The viscosity of extract rapidly decreased first and then slightly increased during germination. The germination speed of colored rice was lower than that of brown rice at $25^{\circ}C$. The germinated colored rice can be used for sikhe not as a saccharifying agent but as a substitute for white rice for the nutritional purpose.

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