• 제목/요약/키워드: vacuum furnace

검색결과 281건 처리시간 0.031초

Manufacturing Characteristics of Woodceramics from Thinned Small Logs (II) - Dimensional Change, Weight Change and Compressive Strength -

  • Oh, Seung-Won;Hirose, Takashi;Okabe, Toshihiro
    • Journal of the Korean Wood Science and Technology
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    • 제28권4호
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    • pp.56-60
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    • 2000
  • A new porous carbon material "woodceramics" was developed by carbonizing wood or woody materials impregnated with thermosetting resin. Steamed board and non-steamed board were made from thinned small log of Aomori Hiba (Thujopsis dolabrata S. et. Z. var. hondae M.). They were impregnated with phenol resin and sintered in a vacuum furnace at $650^{\circ}C$. In this paper, the manufacturing method of woodceramics and changes of dimension, weight and compressive strength were investigated. The changes of dimension, weight and compressive strength depend on the types of board and density.

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Y2O3가 분산된 Fe-C 및 Fe-CNT 소결체의 미세구조 및 기계적 특성 (The Microstructure and Mechanical Properties of Y2O3-Dispersed Fe-C and Fe-CNT Sintered Steels)

  • 임진영;안중호
    • 한국분말재료학회지
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    • 제24권4호
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    • pp.298-301
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    • 2017
  • In the present work, we use multiwall carbon nanotubes (MWCNT) as the starting material for the fabrication of sintered carbon steel. A comparison is made with conventionally sintered carbon steel, where graphite is used as the starting material. Milling is performed using a horizontal mill sintered in a vacuum furnace. We analyze the grain size, number of pores, X-ray diffraction patterns, and microstructure. Changes in the physical properties are determined by using the Archimedes method and Vickers hardness measurements. The result shows that the use of MWCNTs instead of graphite significantly reduces the size and volume of the pores as well as the grain size after sintering. The addition of $Y_2O_3$.to the Fe-MWCNT samples further inhibits the growth of grains.

가스용사에 의한 Ni-Cr 기 자용성합금 용사 의 특성에 미치는 용사조건의 영향 (Effect of Spraying Conditions in Flame Spraying of Ni-Cr Base Self Fluxing Alloy on Mild Steel)

  • 배종규;박경채;정인상
    • 한국표면공학회지
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    • 제22권1호
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    • pp.26-42
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    • 1989
  • It has between investigated that the optimum spaying conditions, such as, spraying distance, fusing temperature and fusing time, ect, in a Ni-cr base self fluxing alloy sprayed on the mild steel substrate by oxygen-acetylenc flame spraying. Sprayed specimens on various conditions were fuused in a vacuum furnace and the results were as follows. The optimum spraying condition for excellent coating layer are obtained under spraying distances, fusing temperature and fusing and time ; 180~240mm,1050~110$0^{\circ}C$and 15~30min, respectively. The adhesive strength and surface hurface hardness of the as sprayed specimens were very low by mechanical bonding becaus of the diffusion layer during process. The carbides and borides and formed in the sprayed coating layer and densification of the layer was resulted from the elimination of pores and oxides. The hardness of sprayed coating layer, particularly in the high temperature, was superior to ordinary tool steels.

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Corrosion Behaviors of Ti-xNb Alloys for Biomaterials

  • Byeon, In-Seop;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.186-186
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    • 2014
  • In this study, corrosion behaviors of Ti-xNb alloys for biomaterials. The Ti-xNb binary alloys contained from 10 wt. % to 50 wt. % contents were manufactured by vacuum arc-melting furnace. Microstructures of the alloys were examined by optical microscope (OM) and field emission scanning electron microscope (FE-SEM). In order to identify the phase constitutents of the Ti-xNb alloys, X-ray diffractometer (XRD) with a Cu K radiation was used. The corrosion behaviors were investigated using potentiostat (Model2273,EG & GCo, USA) in NaCl solution at $(36.6{\pm}1.0)^{\circ}C$.

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Mechanical Properties and Surface Characteristics of Ti-25Ta-xHf Alloys

  • Park, Seon-Yeong;Kim, Jeong-Jae;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.187-187
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    • 2014
  • In this study, we investigated mechanical properties and surface characteristics of Ti-25Ta-xHf alloys. The samples were manufactured for composition of Ti-25Ta-xHf(x=0 to 15 wt. %) alloys. Each alloy was melted twenty times in an arc-melting vacuum furnace. The microstructural phases and phase transformation of Ti-25Ta-xHf alloys were identified with the aid of an XRF, XRD and DSC. And mechanical properties were investigated using Vickers hardness, nanoindentation, and tensile test.

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삼나무 간벌재로 제조된 우드세라믹의 전기적성질 (Electrical Properties of Woodceramics Made from Thinned Logs of Cryptomeria japonica D.DON)

  • 오승원
    • 한국가구학회지
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    • 제11권1호
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    • pp.31-36
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    • 2000
  • Woodceramics are new porous carbon materials obtained by carbonization of wood or woody materials impregnated with thermosetting resin in a vacuum furnace. This study examined the electrical properties of woodceramics made from thinned logs of Cryptomeria japonica as a use for electric articles. The summarized results were as follows: 1. The volume resistivity of woodceramics decreased with increasing density of woodceramics made from 3 type board. And the volume resistivity of woodceramics made from non- steamed board was somewhat higher than steamed board. 2. The consumption of electric power of woodceramics decreased with increasing density of woodceramics and resin contents made from 3 type board. And the consumption of electric power of woodceramics made from non-steamed board was somewhat higher than steamed board. 3. When the woodceramics were coated by silicon, the consumption of electric power increased about 7%.

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Preparation of Silicon Nitride-silicon Carbide Composites from Abrasive SiC Powders

  • Kasuriya, S.;Thavorniti, P.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1091-1092
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    • 2006
  • Silicon nitride - silicon carbide composite was developed by using an abrasive SiC powders as a raw material. The composites were prepared by mixing abrasive SiC powder with silicon, pressing and sintering at $1400^{\circ}C$ under nitrogen atmosphere in atmosphere controlled vacuum furnace. The proportion of silicon in the initial mixtures varied from 20 to 50 wt%. After sintering, crystalline phases and microstructure were characterized. All composites consisted of ${\alpha}-Si_3N_4$ and ${\beta}-Si_3N_4$ as the bonding phases in SiC matrix. Their physical and mechanical properties were also determined. It was found that the density of the obtained composites increased with an increase in the $Si_3N_4$ content formed in the reaction.

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분위기 소결공정에 의한 ZnO 바리스터의 열화기구 연구 (The Study of Degradation Mechanism as ZnO Varistor with The Ambient Sintering-Process)

  • 소순진;김영진;최운식;박춘배
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
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    • pp.117-120
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    • 1999
  • The relationship between the DC degradation characteristics of the ZnO varistor and the ambient sintering-process is investigated in this study. ZnO varistors made of Matsuoka's composition were fabricated by standard ceramic techniques. The ambient sintering-process is performed at the extraordinary electrical-furnace which is equipped with the vacuum system. The Gas of sintering process was oxygen, nitrogen, argon, air respectively. The microstructure of ZnO varistors be made use of SEM equipment. The condition of DC degradation tests were conducted at $115\pm2^{\circ}C$ for periods up to 13 h. Current-voltage analysis is used to determine nonlinear coefficients($\alpha$). Resistance-frequency and capacitance-frequency analysis are accomplished to the understanding of electrical properties as DC degradation test. From above analysis, it is found that the ZnO varistor sintered in oxygen atmosphere showed superior properties at the DC degradation test.

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Ti-실리사이드 형성에 관한 연구 (A Study on the Ti-Silicide Formation)

  • 김학균;주승기
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1987년도 전기.전자공학 학술대회 논문집(I)
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    • pp.454-457
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    • 1987
  • Formation of the titanium silicides was performed by the furnace annealing. Ti-silicide was formed by reacting Ti films with singlecrystalline silicon in vacuum or nitrogen ambient in the temperature range $500{\sim}900^{\circ}C$. The Ti-Si interaction in such films was investigated by using X-ray diffraction, and sheet resistance measurements. It was found that the dorminant crystal phase of silicide formed during annealing at $600{\sim}700^{\circ}C$ was TiSi, and $TiSi_2$ phase is associated with a very low sheet resistance(<$2{\Omega}/{\Box}$).

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Sintered Duplex Stainless Steels Corrosion Properties

  • Dobrzanski, L.A.;Brytan, Z.;Grande, M. Actis;Rossob, M.;Park, Woo-Young;Kim, Cheol-Su
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.583-584
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    • 2006
  • This work presents mechanical properties and corrosion resistance of duplex stainless steels obtained through powder metallurgy starting from austenitic, martensitic powders by controlled addition of alloying elements in the right quantity to obtain the chemical composition of the structure similar to biphasic one. In the mixes preparations the Schaffler's diagram was taken into consideration. Prepared mixes of powders have been sintered in a vacuum furnace with argon backfilling. After sintering rapid cooling was applied using nitrogen. Corrosion properties have been studied through electrochemical methods in 1M NaCl.

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