• Title/Summary/Keyword: uniform size

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Observation of Size Effect and Measurement of Mechanical Properties of Ti Thin Film by Bulge Test (벌지 실험을 통한 Ti 박막의 크기 효과 관찰 및 기계적 물성 측정)

  • Jung, Bong-Bu;Lee, Hun-Kee;Hwang, Kyung-Ho;Park, Hyun-Chul
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.37 no.1
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    • pp.19-25
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    • 2013
  • In this study, the mechanical properties of a Ti thin film are measured by a bulge test. In the bulge test, uniform pressure is applied to one side of the film. Measurement of the membrane deflection as a function of the applied pressure allows one to determine the mechanical properties of the film. Ti thin films with thicknesses of 1.0, 1.5, and $2.0{\mu}m$ were deposited on a Si wafer by using an RF magnetron sputtering system. These specimens were annealed at $600^{\circ}C$ for 150, 300, and 600 s to investigate the effect of temperature on the yield stress and mechanical properties of the Ti films. The elastic modulus, residual stress, and yield stress of these membranes are measured by a bulge test. The experimental results suggest that the yield stress is sensitive to the film thickness and annealing time.

A Synthesis of $(Ba_{1-x}Sr_x)TiO_3$ Powders by Sol-Gel Route (졸-겔법을 이용한$(Ba_{1-x}Sr_x)TiO_3$분말합성)

  • Kim, Young-Seok;Kim, Duk-Jun;Kim, Hwan
    • Korean Journal of Materials Research
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    • v.2 no.2
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    • pp.151-156
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    • 1992
  • Using $Ba(OH)_2{\cdot}8H_2O, \;Sr(OH)_2{\cdot}8H_2O$ and $Ti(i-OC_3H_7)_4$, fine $(Ba_{1-x}, \;Sr_{x})TiO_3$ powders were synthesized through sol-gel process. The particle size of the powders calcined at $700^{\cric}C$ proved to be 20-40nm by the observation of TEM micrographs and measurement of BET specific surface area. The analysis of XRD patterns showed that the phase of the powders was cubic, and it was identified with the lattice parameters determined through XRD patterns and the shift of (112) peaks that the solid solution powders were synthesized. It was expected through the analysis of relative ratio of cations and the uniformity of compositions in the powders examined by EDAX analysis and relative dielectric constant measurements for sintered body that the distribution of cations was uniform in particle unit.

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Fabrication and Sensing Properties of Pt-electrode/NASICON Solid Electrolyte/ Carbonate(Na2CO3-K2CO3-CaCO3system ) Electrode for CO2gas sensor (CO2용 Pt전극/NASICON고체전해질/Carbonate (Na2CO3-K2CO3-CaCO3 계) 전극의 가스 센서제작 및 특성)

  • Choi, Jin-Sam;Bae, Jae-Cheol;Bang, Yeong-Il;Lee, Deok-Dong;Huh, Jeung-Su
    • Korean Journal of Materials Research
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    • v.12 no.4
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    • pp.269-273
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    • 2002
  • The NASICON solid electrolyte films, $Na_{1+x}Zr_2Si_xP_{3-x}O_{12}$(1.5< x < 2.3), was prepared from ceramic slurry by modified doctor-blade process. The NASICON solid electrolyte and fabricated sensors, Pt-electrode/NASICON/Carbonate$(Na_2CO_3-K_2CO_3CaCO_3\; system)$ electrode, were investigated to measure phase, microstructure and e.m.f variation for sensing $CO_2$ concentration. The uniform grain size of $2-4{\mu}m$ and major phase of sodium zirconium silicon phosphate phase, $Na_{1+x}Zr_2Si_xP_{3-x}O_{12}$was identified with X-ray diffraction patterns and scanning electron microscopy, respectively. The Nernst's slope of 84 mV/decade for $CO_2$ concentration from 500 to 8000 ppm was obtained at operating temperature of $400^{\circ}C$.

Effect of Stretching on the Microstructure and Mechanical Properties of Al-Li-Cu-Mg Alloys (Al-Li-Cu-Mg(Ag, Ce)합금의 미세조직 및 기계적성질에 미치는 stretching의 영향)

  • Sin, Hyeon-Sik;Jo, Gwon-Gu;Jeong, Yeong-Hun;Sin, Myeong-Cheol
    • Korean Journal of Materials Research
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    • v.5 no.8
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    • pp.1005-1112
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    • 1995
  • The Effects of 0~9% stretching on the microstructure and mechanical properties have been investigated in Al-Li-Cu-Mg alloys. Stretching made T$_1$(Al$_2$CuLi) precipitates finer and more uniform, however, had no effect on the size of $\delta$'. The number of sheared $\delta$'precipitates distributed in the matrix were reduced. The 6% stretching improved the yield strength of the alloys aged at 15$0^{\circ}C$ for 120 hours from 328~342 MPa to 466~488MPa, however, decreased the elongation from 9.7~10.4% to 5.7%.

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Dispersion Characteristics of Wettable Powder Suspension by Ultrasonication (초음파 처리에 의한 수화제 현탁액의 분산 특성)

  • 나우정;주은선;김영복;송민근;이경렬
    • Journal of Biosystems Engineering
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    • v.28 no.4
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    • pp.351-360
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    • 2003
  • This study was carried out to settle the plugging problem which occurs frequently when agricultural wettable powder is used in pest control work using the crushing and the dispersing effects caused by irradiation of ultrasonic wave. Sonication was applied to the wettable powder suspension in a beaker for 30 seconds using a 28 kHz, 200 W PZT BLT, and the image of suspension before and after sonication was observed using a microscope and a SEM. The image of tow commercial wettable powder suspensions in water observed using an optics microscope showed that the agglomerated particles were irregularly distributed over the whole observed region when stirred mechanically, while showing more uniform distribution composed of comparatively single particles in the whole observed region after sonication. Concerning the above, the projected areas of particles in the four suspensions after sonication were decreased distinctively in the observed range of the microscope and the atomization of crystals was much developed. Over the measured range of 5.6∼4,157 ${\mu}$m particle size, the overall projected area of particles was decreased to 58.3∼89.6% on the average after sonication. When the SEM images of sonicated wettable powder suspensions dissolved in water and CH$_3$OH were compared to the suspensions before sonication, such phenomena as the atomization of particles, the expansion of voids between particles, the reduction and the decrease of agglomerated particle groups, and the progress of crack developments on the surface of flake-shaped particles were observed. It seemed possible that the plugging problem that occurs frequently in pest control machine when using wettable powder would be settled by the use of sonication.

Effects of Aluminum Oxide Particles on the Erosion of Nozzle Liner for Solid Rocket Motors (고체 추진기관에서 산화알루미늄 입자가 노즐 내열재의 삭마에 미치는 영향)

  • 황기영;임유진;함희철
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.8
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    • pp.95-103
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    • 2006
  • The compositions, the gas properties in motor chamber and the aluminum oxide (Al2O3) particle size for two kinds of solid propellants with approximately 20% aluminum powder have been investigated. The SEM photographs of $Al_2O_3$ taken from nozzle entrance liner show that the aluminized PCP propellant with 47% volumetric fraction AP/HNIW and bimodal oxidizer 200-5 ${\mu}m$ can offer greater possibility for increasing aluminum agglomeration than the aluminized HTPB propellant with 64% volumetric fraction AP and trimodal oxidizer 400-200-6 ${\mu}m$. The nozzle entrance liner of solid rocket motor with the PCP propellant shows greater erosion at 4 circumferential sections in line with grain slots due to the impingement of large particles, but that with the HTPB propellant shows uniform erosion with circumferential angle.

Evaluation of Effective Temperature for Estimate Design Thermal Loads in Steel Deck of Steel Box Girder Bridges (강상자형교의 강바닥판에서 설계온도하중을 위한 유효온도 산정)

  • Shin, Dong-Wook;Kim, Kyoung-Nam;Choi, Chul-Ho;Lee, Seong-Haeng
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.6
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    • pp.77-87
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    • 2013
  • A present LSD (limited state design) code for temperature load in the domestic bridge design has applied a uniform standard for various bridge types. In this study, in order to calculate the effective temperature, a specimen of steel box girder bridge section with real size dimension was manufactured. For a year, the temperature data were measured at the 18 point in steel deck of steel box girder bridges specimen. Effective temperature within the cross section according to atmospheric temperature was calculated by this experiment data. The analyzed results were very similar correlation when compared with the effective temperature of the Euro Code. Therefore, the effective temperature which calculated based on the present data could be used as the basic data in order to present to the appropriate design criteria for the thermal loads on the domestic bridge design.

Pharmacopuncture of Bauhinia variegata Nanoemulsion Formulation against Diabetic Peripheral Neuropathic Pain

  • Gupta, Pushpraj S;Singh, Sunil K;Tripathi, Abhishek K
    • Journal of Pharmacopuncture
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    • v.23 no.1
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    • pp.30-36
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    • 2020
  • Objectives: The objective of the study was to prepare Bauhinia variegata loaded nanoemulsion(formulation and determine the efficacy of herbal drug formulation against diabetic peripheral neuropathic pain through acupuncture technique. Methods: Nine different ba tches of nanoemulsion (NE1 NE9) of BVN was prepared by varying the Smix ratio and the concentration of oil. BVN was characterized to determine particle size, shape, zeta potential, polydispersity index, optical transmittance, drug release profile and stora ge stability. The optimized formulation was subjected to plantar test, behavioral tests of neuropathic pain and Von Frey filament stimulation test. Diabetes was induced by intraperitoneal injection of freshly prepared solution of Streptozotocin (60 mg/kg) to the experimental rats. Animals were made diabetic divided into four groups, Group I was untreated normal control group, Group II was diabetic control group, Group III was Bauhinia variegata extract ( treated group (100 mg/kg/day, p.o) and Group IV was BVN treated groups (100 mg/kg/day, p.o) acute and chronically. Results: The prepared B. variegata loaded nanoemulsion was nanosized (124 nm), spherical, uniform and stable over the period of 180 days with no change in physiochemical properties. The bl ood glucose and body weight of animals was normalizing after four weeks of treatment that was significant with BVN in comparison to diabetic control group. The chronic administration of BVN significantly (P<0.001) decreased hind paw withdrawal latency an d attenuated mechanical allodynia as compared with diabetic rats. Conclusion: Thus, BVN may be an effective drug formulation against diabetic peripheral neuropathic pain.

Blazed $GxL^{TM}$ Device for Laser Dream Theatre at the Aichi Expo 2005

  • Ito, Yasuyuki;Saruta, Kunihiko;Kasai, Hiroto;Nshida, Masato;Yamaguchi, Masanari;Yamashita, Keitaro;Taguchi, Ayumu;Oniki, Kazunao;Tamada, Hitoshi
    • Journal of Information Display
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    • v.8 no.2
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    • pp.10-14
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    • 2007
  • A blazed $GxL^{TM}$ device is described as having high optical efficiency (> 70% for RGB lasers), and high contrast ratio (> 10,000:1), and that is highly reliable when used in a large-area laser projection system. It has a robust design and precise stress control technology to maintain a uniform shape (bow and tilt) of more than 6,000 ribbons, a $0.25-{\mu}m$ CMOS compatible fabrication processing and planarization techniques to reduce fluctuation of the ribbons, and a reliable Al-Cu reflective film that provided protection against a high-power laser. No degradation in characteristics of the GxL device is observed after operating a 5,000- lumen projector for 2,000 hours and conducting 2,000 temperature cycling tests at $-20^{\circ}C$ and $+80^{\circ}C$. At the 2005 World Exposition in Aichi, Japan the world's largest laser projection screen with a size of 2005 inches (10 m ${\times}$ 50 m) and 6 million pixels (1,080 ${\times}$ 5,760) was demonstrated.

Development of Electrospun Cellulose Acetate Membranes using Carbon Nanotubes for Filtration of Particulate Matter in the Air (전기방사를 이용한 탄소나노튜브 폴리머 공기정화 멤브레인 개발)

  • Park, Soyeon;Kim, Jaehyuk;Han, Sangil
    • Korean Chemical Engineering Research
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    • v.55 no.1
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    • pp.68-73
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    • 2017
  • The removal of particulate matter ranging from $0.01{\mu}m{\sim}10{\mu}m$ can be performed by using membrane filters composed of fibers. Electrospinning techniques offer the production of very thin fibers with a uniform fiber diameter over conventional techniques including template synthesis, melt-blown, phase separation, etc. Air filtration will be improved with electrospun membranes due to the open pore structures, high porosity, and large surface area of the membranes. In the present study, filtration efficiency increased with pore size decrease and fiber density increase induced by carbon nanotube and the increased CA (cellulose acetate) concentration during electrospinning process.