• 제목/요약/키워드: uniform grain size

검색결과 176건 처리시간 0.027초

대청도 지두리 해안의 모래 퇴적층의 특성과 매몰연대에 대한 연구 (A Study on the Characteristics and Burial Ages of Sediment Deposits at Jiduri, Daecheong Island)

  • 김종연
    • 한국지형학회지
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    • 제25권1호
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    • pp.1-17
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    • 2018
  • The characteristics and burial ages of sand sediments on the Jiduri coast in Daechung-myeon, Ongjin-gun, Incheon were investigated. Daecheong Island is the area where the characteristics of the rocky coast and sand coast are shown. Various studies have been conducted on the Okjukdong sand dune that appears in the north of the island. However, there has been no study on the sandy sedimentary topography of the Jiduri and Moraewul area in the south. The sandy sedimentary terrain of Jiduri is divided into sandy beaches, sand dunes and sand deposits along the slope including climbing dune. Overall, the depth of sandy sediments in Jiduri is not deep. The characteristics of sandy sediments and burial ages were investigated at an elevation of about 23 m above sea level at the back of Jiduli Beach and 46 m above sea level at the ridge line between Jiduri and Moraewol. From the Jiduri coast to the hillside behind, the average grain size decreases and the sorting becomes better as it moves from the intertidal zone to the beach and the foredune. This indicates the selective sand transport by the wind and can be judged by the terrain formed under the current sedimentation environment. The average grain size at the upper part of the section of JD-1 (elevation of about 23m MSL) was $1.6918{\varphi}$ of medium sand. The sorting was $0.4584{\varphi}$, skewness was -1.0491 and kurtosis was -1.2411, respectively. Particularly, the average particle size of the crosssection issomewhat uniform, but the color of the constituent material changes from brown to black. In the case of JD-2 (about 46 m MSL), the mean grain size of the section was $1.7943{\varphi}$, the sorting was 0.4931, the skewness was -1.1163, and the kurtosis was 1.2133. On the other hand, the brown and black layers of JD-1 exhibited a burial age of $0.1{\pm}0.0ka$ and the JD-2 had a burial age of $0.7{\pm}0.0ka$.

다공질 양극산화 피막을 이용한 고균일 다결정 살리콘의 성장 (Growth of High Uniform Polycrystalline Grain on the Highly Ordered Porous Anodic Alumina)

  • 김종연;한진우;김영환;김병용;서대식
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.375-375
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    • 2007
  • In the conventional crystallization method, thepoly-Si TFTs show poor device-to-device uniformity because of the random location of the grain boundaries. However, our new crystallization method introduced in this paper employed substrate-embedded seeds on the highly ordered anodic alumina template to control both the location of seeds and the number of grain boundaries intentionally. In the process of excimer laser crystallization (ELC), a-Si film deposited on the anodic alumina by low pressure chemical vapor deposition (LPCVD) is transformed into fine poly-Si grains by explosive crystallization (XC) prior to primary melting. At the higher energy density, the film is nearly completely melted and laterally grown by super lateral growth (SLG) from remained small part of the fine poly-Si grains as seeds at the Si/anodic alumina interface. Resultant grain boundaries have almost linear functions of the number of seeds in concavities of anodic alumina which have a constant spacing. It reveals the uniformity of. device can be enhanced prominently by controlling location and size of pores which contains fine poly~Si seeds under artificial anodizing condition.

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Sol-Gel Processing에 의한 순수 $PbTiO_3$ Ceramics 제조 (Fabrication of Undoped PbTiO3 Ceramics via Sol-Gel Processing)

  • 김선욱;윤만순;임종인;김성숭;김남흥
    • 한국세라믹학회지
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    • 제29권3호
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    • pp.211-215
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    • 1992
  • Crack free PbTiO3 ceramics were produced by sol-gel processing using alkoxide, which has not been reported to be successful. The PbTiO3 gels were prepared from Ti alkoxide and lead acetate without any dopants. They were calcined at $600^{\circ}C$ and miled to produce fine PbTiO3 powder. It was pressed into discs and they were sintered at 110$0^{\circ}C$ for a few hours. The sintered ceramics were relativley hard and dense as having about 96% of theoretical density of PbTiO3. Fabrication of pure PbTiO3 ceramics by sol-gel processing is possibly due to their small grain size and uniform distribution of residual stress created during cubic-tetragonal transition over large number of small grains in fine grain PbTiO3 ceramics.

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순 Sn 도금에서의 Sn 휘스커 성장제어 기술 (Mitigation Methods of Sn Whisker Growth on Pure Sn Plating)

  • 김근수
    • Journal of Welding and Joining
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    • 제31권3호
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    • pp.17-21
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    • 2013
  • Sn whiskers are one of the serious causes of the failure of electronics. Sn whiskers grow spontaneously from Sn-based, lead-free finished surfaces, even at room temperature. A primary factor of these Sn whiskers growth is compressive stress, which enhances the diffusion of Sn or other elements. The sources of compressive stress are the growth of non-uniform large intermetallic compounds along the interface between the Sn grain boundary and Cu substrate. Recent studies revealed the methods for reducing Sn whisker growth. This paper gives an overview about recent researches for mitigation methods of Sn whisker growth during nearly room temperature storage.

수열반응에 의한 고순도 극미립자 BaTiO3 분말합성 (Preparationof High Purity, Submicron BaTiO3 Powder Prepared by Hydrothermal Reaction)

  • 김경용;김윤호;손용배
    • 한국세라믹학회지
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    • 제26권4호
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    • pp.493-498
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    • 1989
  • High purity, submicron BaTiO3 powder was prepared by a hydrothermal technique using Ba(OH)2.8H2O, TiCl4 and NH4OH as starting raw materials. The submicron BaTiO3 powder was synthesized at 130~23$0^{\circ}C$ for 2.5h to yield highly crystalline particles with a narrow particle distribution. The mole ratio of Ba(OH)2.8H2O/TiO(OH)2 was 1.5. It is possible to obtain BaTiO3 with Ba : Ti=1.00$\pm$0/01. The samples densified well at 13$25^{\circ}C$, showing a uniform and fine grain structure. The grain size ranged between 0.3 and 0.5${\mu}{\textrm}{m}$. The products obtained by hydrothermal treatment at various temperatures from 130 to 23$0^{\circ}C$ were characterized by XRD, DTA, BET and SEM etc.

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A Study of the Effect of Tungsten Oxide on W, WC Powder and Alloy Properties

  • Jiang, Cijin;Shen, Paul;Wang, Huan
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.654-655
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    • 2006
  • This is about the effects deoxidization, carbonization and alloying preparation on fine grain W, WC, and grade YG8 powder reduced by "yellow tungsten oxide" and "blue tungsten oxide". The result indicates that yellow tungsten has single composition and blue tungsten oxide has complex composition. With this feature, yellow tungsten oxide got better uniformity and concentration distribution on fine particle size W and WC powder than blue tungsten oxide's. The grade alloy YG8 that made of this W or WC powder has uniform alloy construction, concentrated WC grain distribution and better alloy properties.

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무전해 은도금층과 전기도금층의 형성에 관한 연구 (A Study on he Electroless Deposits and Electrodeposits)

  • 임종주;민병승;정원섭;김인곤
    • 한국표면공학회지
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    • 제33권4호
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    • pp.273-280
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    • 2000
  • Silver was deposited on glass by electroless plating and electroplating. Surface properties were investigated using the AFM. Crystal structure of deposit layers was confirmed by TEM and XRD. Electroplating is performed by DC plating and pulse plating, respectively. This study resulted in followings, first, deposit of electroless plating showed fine grain and was similar to the amorphous structure. Second, electrodeposit on the electroless layer was revealed following results ; (1) more uniform layer and finer grains were obtained with increasing frequency (2) more isotropic structure was obtained with increasing frequency (3) finer grains at 25% duty cycle was obtained (4) grain size and roughness of the silver deposit was decreased with increasing frequency.

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유기화학적 방법에 의한 제조된 ZnO 바리스터의 특성 (Characteristics of ZnO Varistors Prepared by Organiz Process)

  • 안충선;심영재;조성걸;조병두
    • 한국세라믹학회지
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    • 제29권4호
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    • pp.253-258
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    • 1992
  • ZnO varistors were prepared by the organochemical method which used citric acid and ethylene glycol as gelling agents. The microstructure of the sintered specimens exhibited small grains, uniform grain size distribution, and few intragranular pores. Thermal decomposition of the organic resin formed during the powder preparation process was completed around 450$^{\circ}C$. No significant changes were observed in microstructure and current voltage characteristic with respect to calcination temperatures. A major advantage of the organochemical method used in this experiment is a possible uniform mixing of trace amounts of dopants. Therefore, this powder preparation method seems promising in investigating the effect of Li or In ion, which is added in ppm level to ZnO varistors, on the pulse respose characteristic.

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Enhanced Exchange Coupling of $Nd_2Fe_{14}B/Fe_3B$ Magnet Via Magnetic Field Treatment

  • Choong Jin Yang;Con Byung Park
    • Journal of Magnetics
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    • 제1권1호
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    • pp.31-36
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    • 1996
  • An externally applied magnetic field during heat treating the $Nd_2Fe_{14}B/Fe_3B$ based spring magnet was found to enhance the exchange coupling between the hard and soft magnetic grains. More than 30% increase in $M_r/M_s$ values for melt-spun $Nd_2Fe_{73.5}Co_3$$(Hf_{1-x}Ga_x)B_{18.5}$ (x=0, 0.5, 1) alloys was resulted from a uniform distribution of $Fe_3B, \alpha-Fe$ and $Nd_2Fe_{14}B$ phases, and also from a reduced grain size of those phases by 20%. The externally applied magnetic field induced a uniform distribution of fine grains. A study of Mossbauer effect also report that the enhancement of total magnetization of nanocomposite $Nd_2Fe_{14}B/Fe_3B$ alloys is attributed to an increased formation of $Fe_3$B after magnetic annealing.

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다축단조와 다축대각단조로 제조된 순동의 미세조직 및 경도 비교 (Comparison of Microstructure and Hardness of Pure Copper Fabricated by Multi-Axial Forging and Multi-Axial Diagonal Forging)

  • 이재근;권상철;김순태;정효태;김용관;박성혁
    • 소성∙가공
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    • 제28권5호
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    • pp.257-265
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    • 2019
  • Multi-axial forging (MAF), a severe plastic deformation technique, is known to be difficult to obtain materials with homogeneous microstructures. Recently, multi-axial diagonal forging (MADF) process has been developed to solve this problem. In this study, in order to compare the microstructural and mechanical homogeneities of the MAFed and MADFed samples, oxygen-free copper (OFC) cubes measuring 25 mm in length were deformed through MAF and MADF processes and the average grain size and hardness were measured at the edge, face, and center regions of the samples. In the MAFed samples, ultrafine grains were formed at the center region, but a considerable amount of coarse grains remain at the face region. Therefore, the MAFed samples showed a high inhomogeneity in regards to grain size and hardness. On the contrary, in the case of the MADFed sample, the grain sizes at the edge, face, and center regions were similar and the hardness in all the regions are almost similar. This indicates that the MADFed sample has a homogeneous microstructure and uniform mechanical properties, which can be attributed to the homogeneous distribution of the effective strain throughout the material. The results of this study suggests that the MADF is a suitable process in the fabrication of high-strength copper materials with a homogeneous and ultrafine grain structure.