• Title/Summary/Keyword: ultrasonic-assisted

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Morphology and mechanical properties of LDPE/PS blends prepared by ultrasound-assisted melt mixing

  • Ryu, Joung Gul;Kim, Hyungsu;Kim, Myung Ho;Lee, Jae Wook
    • Korea-Australia Rheology Journal
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    • v.16 no.3
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    • pp.147-152
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    • 2004
  • Ultrasound-assisted melt mixing was applied to blending polystyrene (PS) and low density polyethylene(LDPE). The influence of the ultrasonic irradiation on the morphology and mechanical properties of the blends was investigated. It was observed that the domain sizes of the blend were significantly reduced and phase stability was well sustained even after a thermal treatment. Such morphological feature was consistent with the improvements in mechanical performance of the blends. The desirable results of ultrasonic compatibilization are mainly attributed to the in-situ formation of PS-LDPE copolymers as confirmed by a proper separation experiment. An important relationship between ultrasonic irradiation time and mechanical properties is revealed and an issue on the thermal stability of the blend is discussed.

Development of Ultrasonication-assisted Extraction Process for Manufacturing Extracts with High Content of Pinosylvin from Pine Leaves (솔잎의 피노실빈 고함유 추출물 생산을 위한 초음파 추출 공정 개발)

  • 조용진;이상국;안용현;피재호
    • Journal of Biosystems Engineering
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    • v.28 no.4
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    • pp.325-334
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    • 2003
  • Pinosylvin, a stilbenoid phytoalexin, is a health ingredient to be extracted from pine leaves. In this study, ultrasonication-assisted extraction process for manufacturing extracts with high content of pinosylvin from pine leaves was investigated. As process and system variables, ultrasonic power, sonication time and solvent ratio were selected. According to the experimental results, the effective yield of pinosylvin increased with the increase of ultrasonic power and sonication time and the decrease of solvent ratio. When the ultrasonic power of 2400 W/L was added to the solution of pulverized pine leaves of 8 g per 1 L of a solvent for 10 minutes, yield of extracts and purity, effective yield and concentration ratio of pinosylvin were 0.3166 g/g, 0.7247 mg/g, 0.2294 mg/g and 23.0, respectively.

Ultrasound-Assisted Liquid-Liquid Extraction for Recovery of Paclitaxel from Plant Cell Cultures (식물세포배양으로부터 파클리탁셀 회수를 위한 초음파를 이용한 액-액 추출)

  • Ha, Geon-Soo;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.54 no.2
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    • pp.229-233
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    • 2016
  • In this study, an efficient ultrasound-assisted liquid-liquid extraction process was developed for recovering of paclitaxel from plant cell cultures. The optimal ultrasonic power and operating time were 250 W and 15 min at fixed ratio of bottom phase, methylene chloride to top phase, MeOH (25%, v/v). Under the optimal conditions developed in the present method, most of the paclitaxel (~92%) was recovered from crude extract by a single extraction step. Due to the synergistic effect of ultrasound by the addition of inorganic salt, an appropriate inorganic salt concentration and the ultrasonic power were found to be required for the effective recovery of paclitaxel using ultrasound-assisted liquid-liquid extraction.

Effect of Ultrasonic Microdroplet Generation in the Low-Temperature Plasma Ionization-Mass Spectrometry

  • Lee, Hyoung Jun;Yim, Yong-Hyeon
    • Mass Spectrometry Letters
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    • v.10 no.4
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    • pp.103-107
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    • 2019
  • Low-temperature plasma (LTP) ionization is one of the ambient ionization methods typically used in mass spectrometry (MS) for fast screening of chemicals with minimal or no sample preparation. In spite of various advantages of LTP ionization method, including simple instrumentation and in-situ analysis, more general applications of the method are limited due to poor desorption of analytes with low volatilities and low ionization efficiencies in the negative ion mode. In order to overcome these limitations, an ultrasonic vibrator of a commercial hand-held humidifier was interfaced with an LTP ionization source, which generated microdroplets from sample solutions and assisted with LTP ionization. Ionization behaviors of various chemicals in microdroplet-assisted LTP (MA LTP) were tested and compared with typical LTP ionization from dried samples applied on a surface. MA LTP efficiently ionized small organic, amino, and fatty acids with low volatilities and high polarities, which were hardly ionized using the standard LTP method. Facile interaction of LTP with ultrafine droplets generated by ultrasonic resonator allows efficient ionization of relatively non-volatile and polar analytes both in the positive and negative ion modes.

Study on the Effect of Thermal Property of Metals in Ultrasonic-Assisted Laser Machining (초음파 원용 레이저 가공에서 재료의 열적 물성이 표면상태에 미치는 영향에 관한 연구)

  • Lee, Hu Seung;Kim, Gun Woo;Park, Jong Eun;Yang, Min Yang;Cho, Sung Hak;Park, Jong Kweon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.8
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    • pp.759-763
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    • 2015
  • The laser machining process has been proposed as an advanced process for the selective fabrication of electrodes without a mask. In this study, we adapt laser machining to metals that have different thermal properties. Based on the results, the metals exhibit a different surface morphology, heat-affected zone (HAZ), and a recast layer around the machined surface according to their thermal conductivity, boiling point, and thermal diffusivity. Then, we apply ultrasonic-assisted laser machining to remove the recast layer. The ultrasonic-assisted laser machining exhibits a better surface quality in metals with higher diffusivity than those having lower diffusivity.

Effect of High Frequency Oscillation on Compression Tests of Aluminum Cylindrical Specimens (알루미늄 실린더 압축실험에서의 고주파 진동의 영향)

  • Kim, S.W.;Lee, Y.S.
    • Transactions of Materials Processing
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    • v.25 no.6
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    • pp.373-378
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    • 2016
  • Recent researches have reported that the superposition of ultrasonic vibrations in metal forming provides beneficial effects such as the reduction of forming load, flow stress and interfacial friction which improves the surface quality of end products. This paper presents experimental investigations on the effects of ultrasonic vibrations in upsetting tests of aluminum. The ultrasonic exciting system consists of piezoelectric transducer and resonator was designed and constructed to superimpose high frequency oscillation on the forming tools. Ultrasonic vibration-assisted upsetting tests were performed for three vibration modes five amplitudes, and the results were compared with those of conventional upsetting tests. The results showed that the superimposition of ultrasonic vibration reduces the upsetting load, and the load reduction is only dependent on the amplitude of the applied vibration regardless of deformation histories and vibration modes.

A Study on a Ultrasonic Vibration Assisted Grinding of Alumina Ceramic with Diamond Grinding Tool (초음파 진동을 하는 다이아몬드 연삭공구의 알루미나 세라믹 연삭 가공에 관한 연구)

  • Choi, Young-Jae;Song, Ki-Hyeong;Park, Kyung-Hee;Hong, Yun-Hyuck;Kim, Kyeong-Tae;Lee, Seok-Woo;Choi, Hon-Zong
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.1
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    • pp.13-19
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    • 2012
  • In this study, ultrasonic vibration tool designed and made by using FEM analysis. And machining test was carried out in various machining conditions using ultrasonic vibration capable CNC machine. For work material, alumina ceramic ($Al_2O_3$) was used while for tool material diamond electroplated grinding wheel was used. To evaluate ultrasonic vibration effect, grinding test was performed with and without ultrasonic vibration in same machining condition. In ultrasonic mode, ultrasonic vibration of 20kHz was generated by HSK 63 ultrasonic actuator. The two grinding speeds, 1.67m/s and 3.35m/s, were applied. On the other hand, grinding forces were measured by KISTLER dynamometer.

Study on Highly Accuracy Quality Evaluation of Spot Weld by use of Image Processing Technique

    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.5 no.4
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    • pp.38-46
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    • 1996
  • This paper discusses the feasibility of Ultrasonic Nondestructive Evaluation (UNDE) technique for sport weld quality. Ultrasonic c-scan image assisted by image processing technique was used for Nondestructive Evaluation(NDE) of spot weld quality. Ultrasonic testing results obtained were confirmed and compared by Optical Microscope and SAM(Scanning Acoustic Mircroscope) observation of the spot-weld cross section, The results show that the nugget dinameter can be successfully measured with the accuracy of 0.5mm. It was ascertained that ultrasonic c-scan technique is very effective method for the sake of the approach to the quantitative measurement of nugget diameter and the discrimination of the corona bond from nugget. Additional support for the above conclusions is provided by the results for galvanized steel. The ultrasonic results for galvanized welds generally correspond to the results for uncoated steel. Finally, it was found that the above-mentioned technique can be sufficiently applied to NDE method for securing the Quality Assurance(QA) of spot welded products in production line.

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Comparison of Sewage Sludge Solubilization through Different Pretreatment Methods (전처리 방법에 따른 하수슬러지 가용화 비교연구)

  • Kwon, Jae-Hyun;Kim, Bong-Jun;Kim, Min-Kyu;Yeom, Ick-Tae;Kim, Hyung-Soo
    • Journal of Korean Society of Water and Wastewater
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    • v.17 no.4
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    • pp.567-573
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    • 2003
  • The pretreatment process was carried out to solubilize the sewage sludge for enhancing its biodegradability using alkaline treatment, ultrasonic treatment(15kHz), ozone treatment and different combination of these three methods: alkaline followed by ultrasonic as well as ozone, and ultrasonic followed by alkaline. The solubilization efficiency was evaluated based on the SCOD/TCOD ratio and VSS/TS ratio. In results, the proper condition of alkaline treatment was shown as 30meq/l of NaOH, pH 12 and 3hours of reaction time. Solubilization efficiency increased to 17% from initial 2% based on SCOD/TCOD ratio under this condition. In ultrasonic treatment, the higher ultrasonic power, the longer treatment time and the lower sludge volume resulted in higher solubilization respectively. There was a rapid increase in solubilization efficiency after 20 minute, then it was measured as 32% of SCOD/TCOD ratio in 1 hour at a ultrasonic power of 1,300W with 1/sludge. Solubilization efficiencies in combined treatment using alkaline and ultrasonic were 47-53% higher than single treatment at a sonicated time of 1 hour. Ozone treatment followed by alkaline treatment also represented the enhanced solubilization compared to ozone treatment. Therefore, ultrasonic or ozone treatment assisted by alkaline could achieve the short treatment time as well as high solubilizetion efficiency.