• 한국생산제조학회지
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• 제22권2호
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• pp.263-267
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• 2013

The continuing demand for increasingly slimmer and brighter liquid crystal display (LCD) panels has led to an increased focus on the role of light guide panels (LGPs) or optical films that are used to obtain diffuse, uniform light from the backlight unit (BLU). The most basic process in the production of such BLU components is the micromachining of V-shaped grooves. Thus, given the current trend, micromachining of V-shaped grooves is expected to play increasingly important roles in today's manufacturing technology. LCD BLUs comprise various optical elements such as a LGP, diffuser sheet, prism sheet, and protector sheet with V-shaped grooves. High-aspect-ratio patterns are required to reduce the number of sheets and enhance light efficiency, but there is a limit to the aspect ratio achievable for a given material and cutting tool. Therefore, this study comprised a series of experimental evaluations conducted to determine the machining limit in microcutting V-shaped grooves on electroless nickel plated die materials when using single-crystal diamond tools with point angles of $20^{\circ}-80^{\circ}$. Cutting performance was evaluated at various cutting speeds and depths of cut using different machining methods and machine tools. The experimental results are that V-shaped patterns with angles of $80^{\circ}$ or up can be realized regardless of the machining conditions and equipment. Moreover, the feed rate has little effect on machinability, and it is thought that the fly-cut method is more efficient for shallow patterns.

• 대한기계학회논문집A
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• 제38권12호
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• pp.1373-1377
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• 2014

핫스탬핑 공정은 고강도의 강을 얻을 수 있는 방법으로써, 일반적으로 보론강을 오스테나이트 온도까지 가열한 후, 성형과 냉각을 통해 제품을 생산한다. 열처리된 보론강은 1500MPa 이상의 강도를 가지기 때문에 경량화와 안전성을 동시에 향상시킬수 있는 특징이 있다. 뿐만아니라 우수한 성형성으로 인한 치수정밀도가 기존 강판대비 90 % 이상 향상되어 우수한 성형품질을 확보할 수 있는 장점도 있다. 따라서 본 연구에서는 디스크 레이저를 사용하여 핫스탬핑 강판의 맞대기 및 겹치기 용접을 실시하여 용접특성을 파악하였다. 실험결과, 맞대기 용접에서는 맞댄면의 갭에 영향으로 인해 겹치기 용접과 비교하여 더 빠른 속도에서도 완전 용입을 얻을 수 있었으며, 모든 용접부에서 열영향부에서 화이트밴드가 관찰되었다.

• 대한본초학회지
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• 제30권3호
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• pp.19-24
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• 2015

Objectives : HPL-1, a novel herbal medicine which is composed of five herbs such as Kalopanacis Cortex, Chaenomelis Fructus, Raphani Semen, Atractylodis Rhizoma and Pulvis Aconiti Tuberis Purificatum, was developed for treatment of osteoarthritis. This study is aimed to develop analytical method for consistent quality control of HPL-1 and validate chromatographic method. Methods : Chromatographic analysis was performed using ultra-high performance liquid chromatography - diode array detector (UHPLC-DAD) equipped with RP-amide column, column oven, and auto sampler. Marker compounds [protocatechuic acid, chlorogenic acid, liriodendrin, 3,5-dicaffeoylquinic acid, ${\beta}$-D-(3-O-sinapoyl)-fructofuranosyl-$\alpha$-D-(6-O-sinapoyl)glucopyranoside and benzoylmesaconine] were separated by step gradient elution of acetonitrile and 0.1% phosphoric acid/water. The method validation was evaluated by quantitative validation parameters of linearity, accuracy, precision, limit of detection (LOD) and limit of quantification (LOQ) according to KFDA guideline.Results : An optimized method for six marker compounds in HPL-1 was established by UHPLC-DAD. The correlation coefficient (R²) with each calibration curve was greater than 0.99. The LOD and LOQ were within the range of 0.008-0.090 and $0.023-0.274{\mu}g/mL$, respectively. The relative standard deviation (RSD) of intra- and inter-day variability were less than 4.0%. The result of recovery test was range from 93.3-106.3% with RSD < 4.0%.Conclusions : These results suggest that the quantitative UHPLC method is precise, accurate, effective for quality evaluation of HPL-1. The method may also contribute to improve quality of crude drug preparations used for treatment of various diseases.

• Tribology and Lubricants
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• 제33권2호
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• pp.52-58
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• 2017

An ultra-high precise ejection process is essential in a dispensing system for fabricating various precision parts such as a semiconductor, LED, and camera module. The size of such parts has been decreasing, which implies that a precise ejecting technique is required. A phosphor-containing liquid is ejected via a dispenser using dual piezoelectric actuators that are used for generating a high-speed dispensing mechanism. The rod and nozzle continuously contact in high speed to eject the liquid. However, the high-strength filler or phosphor in the liquid causes wear on the surfaces of the rod and nozzle during the dispensing process. As a result, the ejection reliability decreases as the wear on the surfaces increases. Therefore, it is necessary to estimate the wear characteristics of the rod and nozzle via an experiment and FE analysis. Reliability rests up to 1,000 cycles are conducted under relatively severe conditions. The flow rate and surfaces roughness of the rod and nozzle are measured in each ejection cycle. The surface images and wear volume are obtained before and after the tests and the ejection reliability is confirmed by measuring the flow rate of the liquid. The experimental results show that the ejection reliability is maintained up to 1,000k cycles; these results are validated by the simulation results.

• 대한기계학회논문집A
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• 제39권8호
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• pp.759-763
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• 2015

레이저 가공 공정은 마스크 없이 전극을 가공할 수 있다는 장점 때문에 우수한 공정들 중의 하나로 제안되고 있다. 본 논문에서는, 서로 다른 열적 물성을 가지는 금속들에 레이저 가공을 수행하였다. 이 금속들은 서로 다른 표면형상, 열영향부, 그리고 재융착층을 나타내었고 이는 열전도도, 끓는점, 그리고 열확산계수에 의존하였다. 또한 재융착층을 제거하기 위하여 초음파 원용 레이저 가공을 적용, 높은 열확산계수를 가지는 재료에서 그 초음파 가진에 의한 표면 품질의 향상을 발견하였다.

• Natural Product Sciences
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• 제26권1호
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• pp.64-70
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• 2020

Citrus junos seeds (CS) have been traditionally used for the treatment of cancer and neuralgia. They are also used to manufacture edible oil and cosmetic perfume. A large amount of CS shells without oil (CSS) are discarded after the oil in CS is used as foods or herbal remedy. To efficiently utilize CSS as a by-products, it needs to be studied through chemical analysis. Therefore, we developed an ultra-performance liquid chromatography (UPLC)-diode array detection (DAD) method for simultaneous determination and quantitative analysis of five components (two flavonoids and threes limonoids) in CSS. A Waters Acquity UPLC HSS T3 column C18 (2.1 × 100 mm, 1.8 ㎛) was used for this separation. It was maintained at 40 ℃. The mobile phase used for the analysis was distilled water and acetonitrile with gradient elution. To identify the quantity of the five components, a mass spectrometer (MS) with an electrospray ionization (ESI) source was used. The regression equation showed great linearity, with correlation coefficient ≥ 0.9912. Limits of detection (LOD) and limits of quantification (LOQ) of the five compounds were 0.09 - 0.13 and 0.26 - 0.38 ㎍/mL, respectively. Recoveries of extraction ranged from 97.45% to 101.91%. Relative standard deviation (RSD) values of intra- and inter-day precision were 0.06 - 1.15% and 0.19 - 0.25%, respectively. This UPLC-DAD method can be validated to simultaneously analyze quantities of marker flavonoids and limonoids in CSS.

• Journal of Ginseng Research
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• 제40권4호
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• pp.382-394
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• 2016

Background: Ginsenosides are the characteristic and principal components which manifest a variety of the biological and pharmacological activities of the roots and rhizomes of Panax ginseng (GRR). This study was carried out to qualitatively and quantitatively determine the ginsenosides in the cultivated and forest GRR. Methods: A rapid and sensitive ultra-high-performance liquid chromatography coupled with diode-array detector and quadrupole/time of flight tandem mass spectrometry (UPLC-DAD-QTOF-MS/MS) was applied to the qualitative analysis of ginsenosides and a 4000 QTRAP triple quadrupole tandem mass spectrometer (HPLC-ESI-MS) was applied to quantitative analysis of 19 ginsenosides. Results: In the qualitative analysis, all ingredients were separated in 10 min. A total of 131 ginsenosides were detected in cultivated and forest GRR. The method for the quantitative determination was validated for linearity, precision, and limits of detection and quantification. 19 representative ginsenosides were quantitated. The total content of all 19 ginsenosides in the forest GRR were much higher than those in the cultivated GRR, and were increased with the growing ages. Conclusion: This newly developed analysis method could be applied to the quality assessment of GRR as well as the distinction between cultivated and forest GRR.

• 대한기계학회논문집B
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• 제35권11호
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• pp.1147-1156
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• 2011

CLECDiS 는 면적변화형 정전용량 센서의 단점을 극복하고 나노미터 수준의 분해능으로 밀리미터 이상의 큰 변위를 측정하도록 개발된 접촉식 변위센서이다. 그러나 접촉구동 특성으로 인하여 표면평탄도와 마찰에 의해 작은 접촉상태의 변화에도 출력 신호는 크게 왜곡될 수 있어 실제 이를 활용하기 위해서는 전극간 접촉상태를 안정적으로 유지하는 것이 중요하다. 이에 본 연구에서는 전극간 접촉상태의 변화에 따른 신호의 왜곡 특성을 실제 출력 신호와 비교하여 분석하고, 접촉면 내 압력 분포와 센서의 운동 오차 측정을 통해 접촉상태의 변화를 파악하였다. 이를 통하여 센서의 운동 오차와 마찰력의 영향을 최소화하기 위한 접촉 유지 기구를 설계하고 제작하였으며 이를 이용한 구동실험을 통해 보다 안정적인 센서 출력 신호를 획득하였다.

• 한국산업정보학회논문지
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• 제12권3호
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• pp.124-131
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• 2007

3 Megapixel, 2.5배 Zoom 카메라폰 모듈용 광학계 중 비구면과 평면으로 설계된 평볼록형 비구면 Glass렌즈를 고온압축성형법으로 제작하였다. 제작된 비구면 Glass 성형렌즈의 성능은 성형렌즈의 형상정도(PV) 전사성과 해상도로 평가하였다. Glass렌즈 성형용 몰드의 형상정도(PV)는 비구면의 경우 $0.127\;{\mu}m$, 평면의 경우 $0.168\;{\mu}m$이었고, 성형된 렌즈의 형상정도(PV)는 비구면의 경우 $0.205\;{\mu}m$, 평면의 경우 $0.223\;{\mu}m로 $90{\sim}95%$의 전사정도를 보였다. 성형렌즈의 해상도 평가를 위해 렌즈의 MTF[Contrast]를 측정하였다. 공간주파수 80 lp/mm에서 Contrast가 32.9%을 보였으며, 이 값은 렌즈 광학설계의 전산모사에서 얻어진 Contrast 33%에 근사한 값으로 성형렌즈의 해상도 특성이 우수함을 알 수 있었다.

• Journal of Applied Biological Chemistry
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• 제59권2호
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• pp.165-169
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• 2016

The quantitative analytical method for the bioactive substance, 3-cyano-4-methoxy-N-methyl-2-pyridone (ricinine) and an index compound, ricinoleic acid in castor plant (Ricinus communis) extract or oil was developed. For the determination of a pyridone alkaloid compound, ricinine, successive cartridge cleanup method combined with ultra-performance liquid chromatography was set up with $ENVI-Carb^{TM}$ (0.5 g) and $C_{18}$ SPE cartridges. Accuracy and precision were evaluated through fortification studies of one biopesticide (PE) at 10 and $100mg\;kg^{-1}$. Mean recoveries of ricinine were 98.7 and 96.0 % associated with less than 10 % RSD, respectively. For the determination of ricinoleic acid in castor extract and oil, saponification and methylation were optimized using gas chromatography-time of flight mass spectrometry. Recovery was more than 84.8 % associated with 6.2 % RSD after derivatization procedure. Both methodologies developed were applied to analyze real samples including three castor oil products and six commercially available biopesticides containing R. communis, collected at Korean market. The contents of ricinine and ricinoleic acid in most commercial biopesticides were less than the oil or extract contents indicated by label.