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Fracture Toughness Measurement of the Semiconductor Encapsulant EMC and It's Application to Package (반도체 봉지수지의 파괴 인성치 측정 및 패키지 적용)

  • 김경섭;신영의;장의구
    • Electrical & Electronic Materials
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    • v.10 no.6
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    • pp.519-527
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    • 1997
  • The micro crack was occurred where the stress concentrated by the thermal stress which was induced during the cooling period after molding process or by the various reliability tests. In order to estimate the possibility of development from inside micro crack to outside fracture, the fracture toughness of EMC should be measured under the various applicable condition. But study was conducted very rarely for the above area. In order to provide a was to decide the fracture resistance of EMC (Epoxy Molding Compound) of plastic package which is produced by using transfer molding method, measuring fracture is studied. The specimens were made with various EMC material. The diverse combination of test conditions, such as different temperature, temperature /humidity conditions, different filler shapes, and post cure treatment, were tried to examine the effects of environmental condition on the fracture toughness. This study proposed a way which could improve the reliability of LOC(Lead On Chip) type package by comparing the measured $J_{IC}$ of EMC and the calculated J-integral value from FEM(Finite Element Method). The measured $K_{IC}$ value of EMC above glass transition temperature dropped sharply as the temperature increased. The $K_{IC}$ was observed to be higher before the post cure treatment than after the post cure treatment. The change of $J_{IC}$ was significant by time change. J-integral was calculated to have maximum value the angle of the direction of fracture at the lead tip was 0 degree in SOJ package and -30 degree in TSOP package. The results FEM simulation were well agreed with the results of measurement within 5% tolerance. The package crack was proved to be affected more by the structure than by the composing material of package. The structure and the composing material are the variables to reduce the package crack.ack.

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Analytical, experimental and numerical study of timber-concrete composite beams for bridges

  • Molina, Julio C.;Calil, Carlito Junior;de Oliveira, Diego R.;Gomes, Nadia B.
    • Computers and Concrete
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    • v.24 no.2
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    • pp.103-115
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    • 2019
  • In this study, the strength and stiffness (EI) of wood-concrete composite beams for bridges with T-shaped cross section were evaluated. Two types of connectors were used: connectors bonded with epoxy adhesive and connectors attached to the wood just by pre-drilling (without adhesive). The connectors consisted of common steel bars with a diameter of 12.5 mm. Initially, the strength and stiffness (EI) of the beams were analyzed by bending tests with the load applied at the third point of the beam. Subsequently, the composite beams were evaluated by numerical simulation using ANSYS software with focus on the connection system. To make the composite beams, Eucalyptus citriodora wood and medium strength concrete were used. The slip modulus K and the ultimate strength values of each type of connector were obtained by direct shear tests performed on composite specimens. The results showed that the connector glued with epoxy adhesive resulted in better strength and stiffness (EI) for the composite beams when compared to the connector fixed by pre-drilling. The differences observed were up to 10%. The strength and stiffness (EI) values obtained analytically by $M{\ddot{o}}hler^{\prime}$ model were lower than the values obtained experimentally from the bending tests, and the differences were up to 25%. The numerical simulations allowed, with reasonable approximation, the evaluation of stress distributions in the composite beams tested experimentally.

Effect of a Coil Shape on an Impulse Velocity of the Electromagnetic Welding (전자기 용접의 충돌 속도에 대한 코일 형상의 영향)

  • Park, H.;Lee, K.;Lee, J.;Lee, Y.;Kim, D.
    • Transactions of Materials Processing
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    • v.28 no.3
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    • pp.135-144
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    • 2019
  • Electromagnetic impulse welding (EMIW) is a type of solid state welding using the Lorentz force generated by interaction between the magnetic field of the coil and the current induced in the workpiece. Although many experimental studies have been investigated on the expansion and compression welding of tube using the EMIW process, studies on the EMIW process of lap joint between flat sheets are uncommon. Since the magnetic field enveloped inside the tube can be controlled with ease, the electromagnetic technique has been widely used for tube welding. Conversely, it is difficult to control the magnetic field in the flat sheet welding so as to obtain the required welding velocity. The current study analyzed the effects of coil shape on the impulse velocity for suitable flat one-turn coil for the EMIW of the flat sheets. The finite element (FE) multi-physics simulation involving magnetic and structural field of EMIW were conducted with the commercial software LS-DYNA to evaluate the several shape variables, viz., influence of various widths, thicknesses, gaps and standoff distances of the flat one-turn coil on the impulse velocity. To obtain maximum impulse velocity, the flat one-turn coil was designed based on the FE simulation results. The experiments were performed using an aluminum alloy 1050 sheets of 1.0mm thickness using the designed flat one-turn coil. Through the microscopic interfacial analysis of the welded specimens, the interfacial connectivity was observed to have no defects. In addition, the single lap joint tests were performed to evaluate the welding strength, and a fracture occurred in the base material. As a result, a flat one-turn coil was successfully designed to guarantee welding with bond strength equal to or greater than the base material strength.

Microstructure and High-Cycle Fatigue Properties of High-Speed-Extruded Mg-5Bi-3Al Alloy (Mg-5Bi-3Al 마그네슘 고속 압출재의 미세조직과 고주기피로 특성)

  • Cha, J.W.;Jin, S.C.;Park, S.H.
    • Transactions of Materials Processing
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    • v.31 no.5
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    • pp.253-260
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    • 2022
  • In this study, the microstructural characteristics of a high-speed-extruded Mg-5Bi-3Al (BA53) alloy and its tensile, compressive, and high-cycle fatigue properties are investigated. The BA53 alloy is successfully extruded at a die-exit speed of 16.6 m/min without any hot cracking using a large-scale extruder for mass production. The homogenized BA53 billet has a large grain size of ~900 ㎛ and it contains fine and coarse Mg3Bi2 particles. The extruded BA53 alloy has a fully recrystallized microstructure with an average grain size of 33.8 ㎛ owing to the occurrence of complete dynamic recrystallization during high-speed extrusion. In addition, the extruded BA53 alloy contains numerous fine lath-type Mg3Bi2 particles, which are formed through static precipitation during air cooling after exiting the extrusion die. The extruded BA53 alloy has a high tensile yield strength of 175.1 MPa and ultimate tensile strength of 244.4 MPa, which are mainly attributed to the relative fine grain size and numerous fine particles. The compressive yield strength (93.4 MPa) of the extruded BA53 alloy is lower than its tensile yield strength, resulting in a tension-compression yield asymmetry of 0.53. High-cycle fatigue test results reveal that the extruded BA53 alloy has a fatigue strength of 110 MPa and fatigue cracks initiate at the surface of fatigue test specimens, indicating that the Mg3Bi2 particles do not act as fatigue crack initiation sites. Furthermore, the extruded BA53 alloy exhibits a higher fatigue ratio of 0.45 than other commercial extruded Mg-Al-Zn-based alloys.

Effects of Reaction pH and Hardener Type on Reactivity, Properties, and Performance of Urea-Formaldehyde (UF) Resin

  • Park, Byung-Dae;Kim, Yoon Soo;So, Won Tek;Lim, Kie Pyo
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.3
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    • pp.1-11
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    • 2002
  • This study was conducted to investigate the effects of reaction pH conditions and hardener types on the reactivity, chemical structure and adhesion performance of UF resins. Three different reaction pH conditions, such as traditional alkaline-acid (7.5 → 4.5), weak acid (4.5), and strong acid (1.0), were used to synthesize UF resins which were cured by adding three different hardeners (ammonium chloride, ammonium citrate, and zinc nitrate) to measure adhesion strength. Fourier transform infrared (FT-IR) and carbon-13 nuclear magnetic resonance (13C-NMR) spectroscopies were employed to study chemical structure of the resin prepared under three different reaction pH conditions. Adhesion strength of the resins cured with three different hardeners was determined with lap shear specimens in tension. The gel time of UF resins decreased with an increasing in the amount of both ammonium chloride and ammonium citrate added in the resins. However, the gel time increased for zinc nitrate. Both FT-IR and 13C-NMR spectroscopies showed that the strong reaction pH condition produce uronic structures in UF resin, while both alkaline-acid and weak acid conditions produce quite similar chemical species in the resins. The maximum adhesion strength was occurred with the resin prepared under strong acid pH condition. However, this study indicated that the weak acid reaction condition provide a balance between increasing resin reactivity and improving adhesion strength of UF resin. The measurement of formaldehyde emission from the panels bonded with the UF resins prepared is planned for future work.

Effect of process pressure and nitrogen addition ratio on the uniformity of hardening depth and surface properties of Cr-Mo low alloy steel in vacuum carburizing (Cr-Mo 저합금강의 진공침탄 공정 압력 및 질소 첨가 비율에 따른 경화깊이 균일도 및 표면 특성 효과)

  • Gi-hoon Kwon;Hyunjun Park;;Young-Kook Lee;Kyoungil Moon
    • Journal of the Korean institute of surface engineering
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    • v.56 no.1
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    • pp.94-103
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    • 2023
  • The effects of carburizing pressure and gas ratio on vacuum carburizing properties (uniformity and surface characteristics) have been studied through the analyses of carbon concentration, hardness, surface color, surface roughness and type of carbon bonding. AISI 4115 steel specimens were carburized with various pressures (1, 5, and 10 Torr) at different locations (P1, P2, P3, P4, P5, and P6) inside a furnace held at 950 ℃. Since the carburizing pressure represents the density of the carburizing gas, it plays an important role in improving the carburizing uniformity according to locations in the furnace. As the carburizing pressure increased, the carburizing uniformity according to the sample location was improved, but the surface of the carburized specimen was discolored due to the residual acetylene gas, which does not contribute to the carburizing reaction. Therefore, the carburizing uniformity and surface discoloration have been improved by injecting acetylene gas (carburizing gas) and nitrogen gas (non-reactive gas) in a specific ratio.

Resistance to Root Penetration of Root Barrier for Green Roof System (옥상녹화용 방근층 구성재료의 방근성능에 관한 실험적 연구)

  • Kim, Hyun-Soo;Jang, Dae-Hee;Choi, Soo-Kyung
    • Journal of the Korea Institute of Building Construction
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    • v.8 no.6
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    • pp.123-129
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    • 2008
  • The purpose of this study is to test performances of 14 types of root barrier materials by applying testing plant: and soils suitable for weather and natural features of Korea. For testing Plants, Plioblastus pygmaed Mitford A and Pyracantha angustifolia have been selected. For testing soil, mixture of pearlite and peat moss in 3:1 ratio Testing container has been fabricated with duplicated structure having inner and outer containers. And the outer container has 2 hinges on its side wall to allow opening and closing. Wet rock wool with 50mm in thickness has been inserted between inner and outer containers to allow root to penetrate through root barrier material and continue to grow. We planted 12 Plioblastus pygmaed Mitford A. and 4 Pyracantha angustifolia per one testing container. Three testing samples have been made for 1 type of root barrier material, which become a total 42 specimens. Planted testing samples have been installed within the greenhouse, which will be observed regularly for 2 years from now on. We started test from July 11, 2008 and had performed intermediate observations every month for initial 3 months. From the 3rd intermediate observation on Sept. 18, we confirmed that 6 types of roe barrier materials have penetrated roots. Even though two types of them have been generally used as root barrier materials for roof planting system, all of three testing samples have a lot of penetrated roots. This result proves that it is not reasonable to introduce testing methods of root barrier from Europe. USA or Japan.

Pasteurella anatipestifer infection in ducklings in Korea (오리의 Pasteurella anatipestifer 감염증 발생)

  • Choi, Chung-ok;Kim, Gyoung-nyoun
    • Korean Journal of Veterinary Research
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    • v.33 no.1
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    • pp.93-99
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    • 1993
  • This study was conducted to investigate the cause of a new duck disease occured in southern part of Korea. A meat type duck farm located in Kangjin, Chonnam Province had experienced outbreaks of septicemic disease at around 20 days of age in nearly every batch of ducklings from early spring to early summer in 1989. Main symptoms of the birds were eye and nasal discharge, depression, inappetence, diarrhea and nervous signs such as tremor and ataxia. Some birds died suddenly without any signs. Mortality reached from 20% to 80% in severe cases. The autopsy findings of the affected ducklings revealed consistantly severe airsacculitis, fibropericarditis, perihepatitis and occasionaly enteritis and distended ureter with urate deposit. A rod shaped gram-negative bacterium was isolated purely from brain and liver of the diseased ducks by culturing the specimens on blood agar for 48 hours in candle jar. The isolate neither produced hemolysis nor grew on MacConKey Agar. It formed colony relatively slowly being recognizable at least 36 hours after culturing, reaching colony size of about 1mm in diameter at 48 hours culture. The colony looked iridescent under oblique light and had muddy odor. The isolate did not ferment carbohydrates tested but produced gelatinase, hippuricase and oxidase which were considered as characteristics of P anatipestifer. The isolate induced similar signs and lesions when infected experimentally into ducks of 3 to 38 days age via intraperitoneum or intratrachea. However it did not produce any clinical signs wen inoculated via intranasal route. It produced only mild signs in chicken just injected with a very large dose. The bacteria did not produce any signas or lesions in mice. It was concluded through biochemical and physiological tests and animal inoculation tests that the new disease was caused by P anatipestifer.

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Bending Capacity Evaluation of the Infilled Composite Beam with Semi-slim Closed Section (반슬림 폐단면 충전형 합성보의 휨성능 평가)

  • Lim, Hwan Taek;Choi, Byong Jeong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.3
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    • pp.130-140
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    • 2018
  • An AU-composite beam based on U-shaped steel beams and steel plate anchors of type A was developed. The composite beam reduced the height of the building floor and construction cost. In addition, it decreased the length of construction work, and improved the flexural strength and stiffness as a form of tubes. In this study, AU-composite beams were tested directly and their performance was evaluated through bending experiments. The strength of the specimens was increased initially by linear loads and reached a maximum strength due to destruction of the concrete slab. All of the experiments showed more than 85% of the maximum stress and performed gentle movement. In addition, there was good composite behavior with the steel plate anchor that had excellent composite effects and reached full strength until the maximum strength was reached. When the thickness of the steel plate was increase, the flexural stiffness and strength of the specimen were improved. Therefore, the flexural strength of AU-composite beams can be estimated using the flexural strength formula according to the KBC 2016.

Low Temperature Sintering of PNN-PZT Ceramics and Its Electrical Properties (PNN-PZT 세라믹스의 저온 소결 및 전기적 특성 평가)

  • Lee, Myung-Woo;Kim, Sung-Jin;Yoon, Man-Soon;Ryu, Sung-Lim;Kweon, Soon-Yong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.12
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    • pp.1077-1082
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    • 2008
  • To fabricate a multi-layered piezoelectrics/electrodes structure, the piezoelectrics should be sintered at the temperature lower than $950^{\circ}C$ to use the silver electrode, which is cheaper than the electrodes containing noble metals such as Pd and Pt. Therefore, in this study, we modified the composition of $Pb(Zr,Ti)O_3$-based material as $(Pb_{0.98}Cd_{0.02})(Ni_{1/3}Nb_{2/3})_{0.25}Zr_{0.35}Ti_{0.4}O_3$ to lower the sintering temperature and to improve the piezoelectric properties. Small amount of $MnCO_3$, $SiO_2$, and $Pb_3O_4$ were also added to lower the sintering temperature of the ceramic. The prepared raw powders were mixed by using a ball mill for 24 hours. And then the mixed powders were calcinated for 2 hours at $800^{\circ}C$. The calcinated powders were again crushed with the ball mill for 72 hours. The final powders were pressed for making the shape of ${\emptyset}15\;mm$ disk. The disk-type samples were sintered at temperature range of $850{\sim}950^{\circ}C$. The crystal phases of the sintered specimens were perovskite structure without secondary phases. All of the measured electrical properties such as electromechanical coupling coefficients ($k_p$), mechanical quality factors ($Q_m$), and piezoelectric charge constants ($d_{33}$) were decreased with decreasing the sintering temperatures. The electrical properties measured at the sample sintered at $950^{\circ}C$ were 54% of $k_p$, 503 of $Q_m$, and 390 pC/N of $d_{33}$, respectively. These properties were considered to be fairly good for the application of multi-layered piezoelectric generators or actuators.