• 제목/요약/키워드: two sample testing

검색결과 249건 처리시간 0.024초

Specimen Geometry Effects on Oxidation Behavior of Nuclear Graphite

  • Cho, Kwang-Youn;Kim, Kyung-Ja;Lim, Yun-Soo;Chung, Yun-Joong;Chi, Se-Hwan
    • Carbon letters
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    • 제7권3호
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    • pp.196-200
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    • 2006
  • Graphite has hexagonal closed packing structure with two bonding characteristics of van der Waals bonding between the carbon layers at c axis, and covalent bonding in the carbon layer at a and b axis. Graphite has high tolerant to the extreme conditions of high temperature and neutron irradiations rather than any other materials of metals and ceramics. However, carbon elements easily react with oxygen at as low as 400C. Considering the increasing production of today of hydrogen and electricity with a nuclear reactor, study of oxidation characteristics of graphite is very important, and essential for the life evaluation and design of the nuclear reactor. Since the oxidation behaviors of graphite are dependent on the shapes of testing specimen, critical care is required for evaluation of nuclear reactor graphite materials. In this work, oxidation rate and amounts of the isotropic graphite (IG-110, Toyo Carbon), currently being used for the Koran nuclear reactor, are investigated at various temperature. Oxidation process or principle of graphite was figured out by measuring the oxidation rate, and relation between oxidation rate and sample shape are understood. In the oxidation process, shape effect of volume, surface area, and surface to volume ratio are investigated at $600^{\circ}C$, based on the sample of ASTM C 1179-91.

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Comparison of the bond strength of ceramics to Co-Cr alloys made by casting and selective laser melting

  • Lawaf, Shirin;Nasermostofi, Shahbaz;Afradeh, Mahtasadat;Azizi, Arash
    • The Journal of Advanced Prosthodontics
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    • 제9권1호
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    • pp.52-56
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    • 2017
  • PURPOSE. Considering the importance of metal-ceramic bond, the present study aimed to compare the bond strength of ceramics to cobalt-chrome (Co-Cr) alloys made by casting and selective laser melting (SLM). MATERIALS AND METHODS. In this in-vitro experimental study, two sample groups were prepared, with one group comprising of 10 Co-Cr metal frameworks fabricated by SLM method and the other of 10 Co-Cr metal frameworks fabricated by lost wax cast method with the dimensions of $0.5{\times}3{\times}25\;mm$ (following ISO standard 9693). Porcelain with the thickness of 1.1 mm was applied on a $3{\times}8-mm$ central rectangular area of each sample. Afterwards, bond strengths of the samples were assessed with a Universal Testing Machine. Statistical analysis was performed with Kolmogorov-Smirnov test and T-test. RESULTS. Bond strength in the conventionally cast group equaled $74.94{\times}16.06\;MPa$, while in SLM group, it equaled $69.02{\times}5.77\;MPa$. The difference was not statistically significant ($P{\leq}.05$). CONCLUSION. The results indicated that the bond strengths between ceramic and Co-Cr alloys made by casting and SLM methods were not statistically different.

용사 도막의 내식성에 관한 전기화학적 평가 (An Electrochemical Evaluation on the Corrosion Property of Metallizing Film)

  • 신중하;문경만
    • Corrosion Science and Technology
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    • 제9권6호
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    • pp.325-330
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    • 2010
  • Many surface protection methods have been developed to apply for constructional steels used under severe corrosive environment. Thermal spray coating has been known to be an attractive technique due to its relatively high coating speed. Furthermore high corrosion resistance of coated film with thermal spray is required to expand its application. Four types of coated films(DFT:300 um) such as pure zinc, pure aluminum and two Al-Zn alloy (Al:Zn=85:15 and Al:Zn=95:5) onto the carbon steel (SS401) were prepared with arc spray, and the corrosion behavior of their samples were evaluated by electrochemical method in this study. Pure aluminum sample showed high corrosion resistance behavior exposed to sea water solution and pure zinc and alloy (Al:Zn=95:5) samples followed pure aluminum sample. The other alloy(Al:Zn=85:15) so called galvalume coated onto the carbon steel ranks the 4th corrosion resistance in this study. The results of porosity ratio of those samples by observation are well matched with the electrochemical data.

Nuclide composition non-uniformity in used nuclear fuel for considerations in pyroprocessing safeguards

  • Woo, Seung Min;Chirayath, Sunil S.;Fratoni, Massimiliano
    • Nuclear Engineering and Technology
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    • 제50권7호
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    • pp.1120-1130
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    • 2018
  • An analysis of a pyroprocessing safeguards methodology employing the Pu-to-$^{244}Cm$ ratio is presented. The analysis includes characterization of representative used nuclear fuel assemblies with respect to computed nuclide composition. The nuclide composition data computationally generated is appropriately reformatted to correspond with the material conditions after each step in the head-end stage of pyroprocessing. Uncertainty in the Pu-to-$^{244}Cm$ ratio is evaluated using the Geary-Hinkley transformation method. This is because the Pu-to-$^{244}Cm$ ratio is a Cauchy distribution since it is the ratio of two normally distributed random variables. The calculated uncertainty of the Pu-to-$^{244}Cm$ ratio is propagated through the mass flow stream in the pyroprocessing steps. Finally, the probability of Type-I error for the plutonium Material Unaccounted For (MUF) is evaluated by the hypothesis testing method as a function of the sizes of powder particles and granules, which are dominant parameters to determine the sample size. The results show the probability of Type-I error is occasionally greater than 5%. However, increasing granule sample sizes could surmount the weakness of material accounting because of the non-uniformity of nuclide composition.

Testing Differences of Leisure Satisfaction by Demogrpahic Characteristics of MTB participants

  • MOON, Bo Ra;LEE, Hwan Yeol;SEO, Won Jae
    • Journal of Sport and Applied Science
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    • 제3권1호
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    • pp.27-34
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    • 2019
  • Purpose: Mountain biking as a sport and recreational activity has grown rapidly over the previous two decades. The purpose of this study is to analyze differences of leisure satisfaction by demographic characteristics of mountain bike participants. Research design, data, and methodology: To accomplish the purpose, the study employed purposive sample method among nonprobability sampling and collected data from 300 participants. Of collected data, 288 responses were analyzed excepted for uncompleted responses. To analyze data, study utilized statistical techniques including descriptive statistics, reliability analysis, independent-sample t-test, and one-way ANOVA, and to verify difference between individual groups in relation to significant results, Duncan's multiple range was conducted. Results: Findings indicated no differences of leisure satisfaction by gender. Similarly, education level and occupations have not influence leisure satisfaction. Yet, differences of leisure satisfaction by participation frequencies were observed. Of participation frequencies, participants riding 5 times a week were more satisfied with MTB participation than the other groups participating less 3 times a week. Conclusions: The findings provide a couple of insights in terms of promoting MTB participation. In specific, results indicated that MTB would be attractive sports that is able to appeal huge populations regardless of their education and occupation. Furthermore, consistent participation is judged an effective way to increase psychological, educational, and social satisfaction. In this sense, regional MTB clubs could play a salient role in motivating riders to more participate in MTB. Hence, establishing strategies for encouraging club activities are needed.

혈장 시료 풀링을 통한 신약 후보물질의 흡수율 고효율 검색기법의 평가 (Evaluation of a Sample-Pooling Technique in Estimating Bioavailability of a Compound for High-Throughput Lead Optimazation)

  • 이인경;구효정;정석재;이민화;심창구
    • Journal of Pharmaceutical Investigation
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    • 제30권3호
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    • pp.191-199
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    • 2000
  • Genomics is providing targets faster than we can validate them and combinatorial chemistry is providing new chemical entities faster than we can screen them. Historically, the drug discovery cascade has been established as a sequential process initiated with a potency screening against a selected biological target. In this sequential process, pharmacokinetics was often regarded as a low-throughput activity. Typically, limited pharmacokinetics studies would be conducted prior to acceptance of a compound for safety evaluation and, as a result, compounds often failed to reach a clinical testing due to unfavorable pharmacokinetic characteristics. A new paradigm in drug discovery has emerged in which the entire sample collection is rapidly screened using robotized high-throughput assays at the outset of the program. Higher-throughput pharmacokinetics (HTPK) is being achieved through introduction of new techniques, including automation for sample preparation and new experimental approaches. A number of in vitro and in vivo methods are being developed for the HTPK. In vitro studies, in which many cell lines are used to screen absorption and metabolism, are generally faster than in vivo screening, and, in this sense, in vitro screening is often considered as a real HTPK. Despite the elegance of the in vitro models, however, in vivo screenings are always essential for the final confirmation. Among these in vivo methods, cassette dosing technique, is believed the methods that is applicable in the screening of pharmacokinetics of many compounds at a time. The widespread use of liquid chromatography (LC) interfaced to mass spectrometry (MS) or tandem mass spectrometry (MS/MS) allowed the feasibility of the cassette dosing technique. Another approach to increase the throughput of in vivo screening of pharmacokinetics is to reduce the number of sample analysis. Two common approaches are used for this purpose. First, samples from identical study designs but that contain different drug candidate can be pooled to produce single set of samples, thus, reducing sample to be analyzed. Second, for a single test compound, serial plasma samples can be pooled to produce a single composite sample for analysis. In this review, we validated the issue whether the second method can be applied to practical screening of in vivo pharmacokinetics using data from seven of our previous bioequivalence studies. For a given drug, equally spaced serial plasma samples were pooled to achieve a 'Pooled Concentration' for the drug. An area under the plasma drug concentration-time curve (AUC) was then calculated theoretically using the pooled concentration and the predicted AUC value was statistically compared with the traditionally calculated AUC value. The comparison revealed that the sample pooling method generated reasonably accurate AUC values when compared with those obtained by the traditional approach. It is especially noteworthy that the accuracy was obtained by the analysis of only one sample instead of analyses of a number of samples that necessitates a significant man-power and time. Thus, we propose the sample pooling method as an alternative to in vivo pharmacokinetic approach in the selection potential lead(s) from combinatorial libraries.

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BioAPl기반 시스템 모듈을 검증하기 위한 적합성시험 방법 연구 (A Study on Conformance Testing Method to Verify the BioAPI Based System Module)

  • 이유영;권영빈
    • 정보처리학회논문지B
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    • 제11B권7호
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    • pp.759-768
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    • 2004
  • 생체인식기술을 응용한 제품이 다양해지면서 상호운용성의 문제가 제기되어 국제표준화가 진행중인 BioAPl(Biometric Application Pro-gramming Interface)를 기반으로 한 생체인식 제품의 개발이 증대되고 있다. 그러나 BioAPl를 적용하여 개발된 제품에 대한 성능 측정 및 표준규격의 적합성 여부에 대한 신뢰성 있는 평가 도구가 마련되어 있지 않은 상태이다. 본 논문은 생체인식시스템이 BioAPl 규격의 요구사항 및 기준에 얼마나 만족하여 개발하였는가를 검증하기 위한 적합성시험 방법을 연구하였다. 제안된 적합성 시험기술의 첫 번째는 BioAPl명세서가 제공하는 각 함수들을 제대로 구현하였는가에 대한 확인과 사용여부를 평가하는 것이다. 이것은 응용에서 APl(Application Provider Inter-face)함수를 호출하면 프레임워크를 통해 BSP(Biometric Service Provider)를 실행하는 것으로 이때 파라미터와 선행함수의 선택이 필요하다. 두 번째는 BioAPl의 해당 테스트케이스를 분석하여 모듈관리, 핸들기능, 검증기능에 대한 시나리오를 평가하는 것이다. 실험은 BioAPl 컨소시엄에서 제공하는 샘플프로그램과 상용 지문검증시스템의 BSP를 사용하여 제안하는 적합성 평가 방법에 대한 실험을 수행하였다. 이에 따라 BioAPl를 기반으로 한 BSP들이 요구사항에 적합하게 개발되었는지를 판단할 수 있었다.

신용평가모형에서 두 분포함수의 동일성 검정을 위한 비모수적인 검정방법 (Nonparametric homogeneity tests of two distributions for credit rating model validation)

  • 홍종선;김지훈
    • Journal of the Korean Data and Information Science Society
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    • 제20권2호
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    • pp.261-272
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    • 2009
  • 신용평가모형에서 두 집단의 판별력 검정방법 중의 하나로 두 분포함수의 동일성 검정을 위한 비모수적인 Kolmogorov-Smirnov (K-S) 검정방법이 대표적으로 적용되고 있다. 본 연구에서는 신용평가모형에서 두 분포함수의 동일성 검정을 위하여 K-S 검정 방법 외에 Cramer-Von Mises, Anderson-Darling, Watson 검정방법들을 소개하고 Joseph (2005)의 기준에 대응하는 판단기준을 제안한다. 또한 신용평가 자료와 유사한 상황 하에서의 모의실험을 통해서 불량률, 표본크기 그리고 제II종 오류율을 고려한 대안적인 판단기준을 제시하고 그 적용방법에 대해서 살펴본다.

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가짜휘발유 판정을 위한 성분 분석 (Analysis of Component for Determining Illegal Gasoline)

  • 임영관;원기요;강병석;박소휘;정성;고영훈;김성수;정길형
    • Tribology and Lubricants
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    • 제36권3호
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    • pp.161-167
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    • 2020
  • Petroleum is the most used energy source in Korea with a usage rate of 39.5% among the available 1st energy source. The price of liquid petroleum products in Korea includes a lot of tax such as transportation·environment·energy tax. Thus, illegal production and distribution of liquid petroleum is widespread because of its huge price difference, including its tax-free nature, from that of the normal product. Generally, illegal petroleum product is produced by illegally mixing liquid petroleum with other similar petroleum alternatives. In such case, it is easy to distinguish whether the product is illegal by analyzing its physical properties and typical components. However, if one the components of original petroleum product is added to illegal petroleum, distinguishing between the two petroleum products will be difficult. In this research, we inspect illegally produced gasoline, which is mixed with methyl tertiary butyl ether (MTBE) as an octane booster. This illegal gasoline shows a high octane number and oxygen content. Further, we analyze the different types of green dyes used in illegal gasoline through high performance liquid chromatography (HPLC). We conduct component analyses on the simulated sample obtained from premium gasoline and MTBE. Finally, the illegal gasoline is defined as premium gasoline with 10% MTBE. The findings of this study suggest that illegal petroleum can be identified through an analytic method of components and simulated samples.

한국 가정생활 문화 관련 단원의 학습에서 ICT활용 수업이 가정교과에 대한 흥미, 전통문화의식, 학업성취 및 수행평가 미치는 효과 (The Effects of ICT Teaching Method on Interest in Home Economics, Consciousness on Traditional Culture, Achievement Test, and Performance Assessment in High School Borne Economics Instruction)

  • 하영희;유태명
    • 대한가정학회지
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    • 제41권11호
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    • pp.135-150
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    • 2003
  • This research was to verity the effects of ICT teaching method in high school home economics. The research questions for this study were as follows: 1. Is the ICT teaching method effective in increasing students' interest in home economics and consciousness on traditional culture in teaming the unit of ‘Korean traditional culture of home life’? 2. Is the ICT teaching method effective in improving students' achievement test and performance assessment in teaming the unit of ‘Korean traditional culture of home life’? This study is carried out with following procedure: developing the homepage and lesson plans for ICT teaching, constructing questionnaire, and testing its reliability, pre-testing, treatment for 8 weeks, and post-testing. Two groups were arranged for 8 weeks experiment from May 7,2001 through June 30,2001. Sixteen hours of ICT teaching and 8 hours of traditional lecture for experiment group whereas 8 hours of ICT teaching and 16 hours of traditional lecture for comparison group were input. SAS program was used for statistical analysis, and independent sample t-test and matched pairs t-test were peformed for answering research questions. The results of this study were as following: 1. Sixteen hours of ICT teaching and 8 hours of traditional lecture for experiment group was effective in increasing consciousness on traditional culture and performance assessment. 2. Eight hours of ICT teaching and 16 hours of traditional lecture for comparison group was not effective in learning home economics. This means that at least 2 hours of ICT teaching is demanding for effective learning. This study concluded that ICT teaching will be effectively applied in high school home economic with well developed ICT teaching materials. And home economics educators should continuously put effort in developing curricular, teaching materials, and teaching methods to raise students' interest in home economics.