• Title/Summary/Keyword: twin screw extruder

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Starch Liquefaction and Residence Time Distribution in Twin-Screw Extrusion of ${\alpha}$-Starch (호화전분의 쌍축형 압출성형에서 전분액화 및 체류시간 분포)

  • Kim, Sung-Uk;Lee, Seung-Ju
    • Korean Journal of Food Science and Technology
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    • v.41 no.4
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    • pp.369-373
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    • 2009
  • ${\alpha}$-Waxy corn starch was used as a feed for twin-screw extrusion in order to enhance starch liquefaction with added thermostable ${\alpha}$-amylase (derived from Bacillus licheniformis). The residence time distribution and starch liquefaction were investigated. The starch liquefaction was analyzed in terms of reducing sugar contents, molecular size from gel permeation chromatography (GPC), and microstructure from scanning electron microscopy (SEM). The use of ${\alpha}$-starch contributed to the production of more reducing sugar than the use of raw starch use alone. From GPC, the effect of ${\alpha}$- starch on the molecular size reduction was shown to be small. From SEM, irregular and damaged surface were observed on the extrudate from ${\alpha}$-starch, as compared to those from raw starch. The spread of residence time distribution curves was greater with feed of ${\alpha}$-starch than raw starch, indicating that ${\alpha}$-starch was hard to flow forward during extrusion. This could be improved by increasing the feed moisture content and barrel temperature of extruder.

Preparation and Dielectric Properties of Ceramic(BNT)-Polymer(LCP) Composite (세라믹(BNT)-폴리머(LCP) 복합체 제조 및 유전특성)

  • Park, Myoung-Sung;Chun, Myoung-Pyo;Cho, Jung-Ho;Nam, Joong-Hee;Choi, Byung-Hyun;Nahm, Sahn
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.11
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    • pp.935-940
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    • 2009
  • In this research, the composites (100-x)LCP-xBNT (x = 0, 10, 20, 30, 40 vol.%) were fabricated with thermoplastic LCP(Liquid Crystal Polymer) and BNT($BaNd_2Ti_4O_{12}$) which is a high frequency dielectric material. Their dielectric properties, mechanical strength and microstructure were investigated by Impedance analyser, Instron and SEM. In order to fabricate LCP-BNT composites, LCP resin was put into the twin screw type mixer($310^{\circ}C$), melted by keeping for 10 min. After that, BNT filler was dispersed with melted LCP resin for 15 min. in the mixer. For measuring the dielectric properties and mechanical strength, Composite specimens were made by pressing composite granule (LCP-BNT) with 7 ton in the mold at $310^{\circ}C$. With increasing the BNT content (0~40 vol.%) of the composite, Its dielectric constant increased, dielectric loss and flexural strength decreased. The dielectric constant and flexural strength of composites with 20~30 vol.% of BNT filler are 4.1~6.0 and 35~55 MPa respectively. BNT/LCP composite is the potential substrate material for the high frequency application.

High-pressure rheology of polymer melts containing supercritical carbon dioxide

  • Lee Sang-Myung;Han Jae-Ro;Kim Kyung-Yl;Ahn Young-Joon;Lee Jae-Wook
    • Korea-Australia Rheology Journal
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    • v.18 no.2
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    • pp.83-90
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    • 2006
  • Supercritical carbon dioxide ($scCO_2$) has advantages of being incorporated in polymer with high solubility and of being recovered easily by depressurizing. $scCO_2$ reduces the viscosity of polymer melt and it is expected to be use as a plasticizing agent. In this work, we studied on the effect of $scCO_2$ on the rheological properties of polymer melts during extrusion process. Slit die attached to twin screw extruder was used to measure the viscosity of polymer melts plasticized by supercritical $CO_2$. A gas injection system was devised to accurately meter the supercritical $CO_2$ into the extruder barrel. Measurements of pressure drop within the die, confirmed the presence of a one phase mixture and a fully developed flow during the measurements. The viscosity measurement of polypropylene was performed at experimental conditions of various temperatures, pressures and $CO_2$ concentrations. We observed that melt viscosity of polymer was dramatically reduced by $CO_2$ addition.

The Effects of Extrusion Cooking and Milling on the Instant Properties of Wheat Powders

  • Tanhehco, E.J.;Ng, P.K.W.
    • Food Science and Biotechnology
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    • v.14 no.6
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    • pp.758-765
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    • 2005
  • Instant powders that only require mixing with water prior to consumption can be produced by extrusion for use in products such as instant beverages. Both extrusion processing conditions and particle size of powder are important to end-product characteristics. In this study, a twin-screw extruder was used under various processing conditions (feed moisture, barrel temperature, and screw speed) to produce extrudates from soft wheat flour, which were ground to powders with particle size ranges of less than 93, 93-145, and $145-249\;{\mu}m$. Effects of adding soy lecithin to wheat flour before extrusion were also investigated. Water absorption, solubility, suspension viscosity, and dispersibility of wheat powders were related to specific. mechanical energy measured during extrusion. Powder particle size was important to instant properties, especially ease of dispersal in water and stability to sedimentation. Addition of lecithin significantly improved dispersibility of powders.

Effects of Extrusion Conditions on the Physicochemical Properties of Extruded Red Ginseng

  • Gui, Ying;Gil, Sun-Kuk;Ryu, Gi-Hyung
    • Preventive Nutrition and Food Science
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    • v.17 no.3
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    • pp.203-209
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    • 2012
  • The effects of variable moisture content, screw speed and barrel temperature on the physicochemical properties of red ginseng powder extrudates were investigated. The raw red ginseng powders were processed in a co-rotating intermeshing twin-screw extruder. Primary extrusion variables were feed moisture content (20 and 30%), screw speed (200 and 250 rpm) and barrel temperature (115 and $130^{\circ}C$). Extruded red ginseng showed higher crude saponin contents (6.72~7.18%) than raw red ginseng (5.50%). Tested extrusion conditions did not significantly affect the crude saponin content of extrudates. Increased feed moisture content resulted in increased bulk density, specific length, water absorption index (WAI), breaking strength, elastic modulus and crude protein content and decreased water solubility index (WSI) and expansion (p<0.05). Increased barrel temperature resulted in increased total sugar content, but decreased reducing sugar content in the extrudate (p<0.05). Furthermore, increased barrel temperature resulted in increased amino acid content and specific length and decreased expansion and bulk density of extrudates only at a higher feed moisture content. The physicochemical properties of extrudates were mainly dependent on the feed moisture content and barrel temperature, whereas the screw speed showed a lesser effect. These results will be used to help define optimized process conditions for controlling and predicting qualities and characteristics of extruded red ginseng.

Mechanical Property of Cabon Nanofiber/Polypropylene Composites by Melt-mixing Process (압출공정에 의한 탄소나노섬유/폴리프로필렌 복합재료의 기계적 특성)

  • Byeon, Jun-Hyeong;Lee, Sang-Gwan;Eom, Mun-Gwan;Min, Gyeong-Sik;Song, Jae-Eun;Lee, Chang-Hun
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.125-128
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    • 2005
  • The dispersion of carbon nanofiber (CNF) was carried out by solution blending, mechanical mixing, and sonication. CNFs at levels of 5-50% fiber weight content were mixed with polypropylene (PP) powder, and then were melt-mixed using a twin-screw extruder. For the further alignment of fibers, extruded rods were stacked uni-directionally in the mold cavity for the compression molding. For the evaluation of mechanical properties of nanocomposites, tension, in-plane shear, and flexural tests were conducted. CNF/PP composites clearly showed reinforcing effect in the longitudinal direction. The tensile modulus and strength have improved by 100% and 40%, respectively for 50 % fiber weight content, and the flexural modulus and strength have increased by 120% and 25%, respectively for the same fiber weight content. The shear modulus showed 65% increase, but the strength dropped sharply by 40%. However, the property enhancement was not significant due to the poor adhesion between fiber and matrix. In the transverse direction, the tensile, flexural, and shear strength decreased as more fibers were added.

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Formation of Enzyme Resistant Starch by Extrusion Cooking of High Amylose Corn Starch (고아밀로즈 옥수수전분의 압출성형에 의한 난소화성화)

  • Kim, Ji-Yong;Lee, Cherl-Ho
    • Korean Journal of Food Science and Technology
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    • v.30 no.5
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    • pp.1128-1133
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    • 1998
  • Extrusion cooking treatment was compared with autoclaving/cooling treatment for formation of enzyme resistant starch of high amylose corn starch (HACS). Effects of barrel temperature $(100^{\circ}C,\;120^{\circ}C,\;140^{\circ}C)$ and feed moisture content (25%, 35%, 45%) on extrusion processing in a co-rotating twin-screw extruder under fixed screw speed (100 rpm) were investigated by measuring enzyme resistant starch (RS) yield. RS yield were estimated by in-vitro pancreatin digestion method and enzymatic-gravimetric method using termamyl. Barrel temperature and yield of RS were negatively correlated and feed moisture content and yield of RS was positively correlated as determined by in-vitro pancreatin method. The highest yield (38.4%) of RS was obtained from HACS extrudate processed at the barrel temperature of $100^{\circ}C$ and the feed moisture content of 45%, while the yield of RS by 5 times of autoclaving/cooling was 25%. The yield of RS by in vitro pancreatin digestion method was 20.7% with high amylose corn starch and 8.2% with ordinary corn starch (CS), respectively, under the same extrusion condition (barrel temperature $120^{\circ}C$, feed moisture content 35%). At the same condition, the yields of RS by enzyme-gravimetric method were 14.6% with HACS and 6.8% with CS, respectively. The yield of RS increased during the storage at $4^{\circ}C$ for 4 weeks and the highest yield (60%) was obtained by the storage of HACS extrudates extruded at $100^{\circ}C$ and 45% feed moisture content.

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Physicochemical Properties of Rice-based Expanded Snacks according to Extrusion Conditions (Extrusion 제조 조건에 따른 쌀 스낵 제품의 이화학적 품질특성)

  • Eun, Jong-Bang;Hsieh, Fu-Hung;Choi, Ok-Ja
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.43 no.9
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    • pp.1407-1414
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    • 2014
  • Physicochemical properties of rice-based expanded snacks extruded with rice flour, high amylose starch, and isolated soy protein were investigated using a twin-screw extruder. The ingredients were extruded at various feed moisture contents (19~23%) and screw speeds (200~400 rpm) at a constant feed rate (43.4 kg/hr). Bulk density and apparent density of rice snacks were 0.06~0.21, and 0.55~0.65 respectively. Bulk density, apparent density, water absorption index, and breaking strength of rice snacks increased with increasing feed moisture content and decreasing screw speed. However, expansion and water solubility index of rice snacks increased with decreasing feed moisture content and increasing screw speed. Hunter's color L values of rice snacks was lower with increasing screw speed at feed moisture contents of 19% and 21%, but was not significantly different from a feed moisture content of 23%. On the other hand, a and b values of rice snacks were higher with increasing screw speed a feed moisture content of 19%. X-ray diffraction intensity of rice snacks decreased with decreasing feed moisture content and increasing screw speed. X-ray diffraction of rice snacks was V-type at feed moisture contents of 19% and 21% and screw speeds of 300, and 400 rpm. In the microstructure of the cross section of rice snacks, air cells in rice snacks were not well formed, and cell walls were thicker with increasing feed moisture content and decreasing screw speed.

Electrical Properties and Crosslinking Characteristics of XLPE/SXLPE Blends (XLPE/SXLPE 블렌드의 전기적 성질 및 가교 특성)

  • Ko, Jung-Woo;Ha, Nam-Kyu;Suh, Kwang-S.
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1602-1604
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    • 1999
  • Crosslinked polyethylene/silane crosslinked polyethylene (XLPE/SXLPE) blends were prepared by a twin screw extruder and their water tree and crosslinking characteristics were investigated. The water tree characteristics of XLPE were improved by the addition of SXLPE, when samples were cross- linked only by the thermorolysis of DCP (dicumyl peroxide). However, steam curing process was not good for water tree characteristics. It was also found that the degree of crosslinking of XLPE/SXLPE blends were higher than that of XLPE.

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Metal-Polymer Composites and their Characterization

  • Lebedev, S.M.;Gefle, O.S.;Semenikhin, M.V.
    • Journal of Powder Materials
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    • v.18 no.2
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    • pp.181-187
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    • 2011
  • PVDF was used as a polymeric matrix material in this work. Nickel powders with average particles size of 200 nm or 72 nm were used as fillers. PVDF/metal submicro- and nanocomposites were prepared by means of a mixing in twin screw extruder and planetary ball mill, respectively. All samples were prepared by hot pressing method. Their electrical, thermal and morphological properties were examined by dielectric spectroscopy, DSC, FTIR, XRD, optical microscopy and scanning electron microscopy. It was found that all properties of composites were strongly modified depending on the content of metal powders and filler particles size. Particularly, specific volume resistivity of PVDF/Ni composite with 0.2 wt.% of Ni was increased by factor of 1.5~4.