• 대한화학회지
• /
• 제52권6호
• /
• pp.637-648
• /
• 2008

• 분석과학
• /
• 제15권1호
• /
• pp.87-90
• /
• 2002

The content of $SiHCl_3$ as a trace impurity in $SiCl_4$ was analyzed by Near IR spectrophotometer with optical fiber. The strong absorption bands of $5345{\sim}5116cm^{-1}$ and $4848{\sim}4349cm^{-1}$ were used for analysis of $SiHCl_3$, and the detection limit of impurity $SiCl_3$ was appeared to be 0.005 ％ in the spectrum. The quantitative analysis by Near IR spectrophotometry showed the analytical possibility of trace impurity in $SiCl_4$ without sample pre-treatment not only in the laboratory but also in the field.

• 분석과학
• /
• 제17권4호
• /
• pp.308-314
• /
• 2004

전자소재의 원료물질 혹은 보호물질에 사용되는 고분자수지내에 포함된 U, Th과 이들의 붕괴산물인 딸핵종과 같은 방사성 불순물이 있는 경우 전자소자의 오작동을 일으키는 주 요인으로 알려져 있으며, Na, Cl, Fe 등과 같은 이온성 불순물은 소자의 수명을 단축시키는 것으로 알려져 있어 극미량 무기불순물의 정확한 분석이 필요하다. NAA의 경우, 위와 같은 분석의 문제점인 시료전처리가 필요하지 않은 비파괴 분석이 가능하여 가장 적합한 분석법으로서 고분자수지중의 극미량 불순물 분석을 위한 시료 전처리법과 최적 분석방법을 개발하였다. 이 방법을 사용하여 전자소재의 밀봉보호재로 널리 이용되고 있는 에폭시수지와 페놀수지중의 극미량 무기 불순물을 분석기술을 개발하였으며, 그 결과 U, Th과 이온성 불순물인 Cl, Fe, Na 외에 20가지의 미량 무기불순물을 분석할 수 있었다.

• 한국환경보건학회지
• /
• 제28권3호
• /
• pp.64-71
• /
• 2002

Hair provides important information about the body's mineral status. Therefore, we have studied the trace elemental distribution in human hair under different inhalation and ingestion environment using neutron activation analysis (NAA). NAA is a powerful analytical method which can be used successfully to determine trace elements in environmental and biological materials. Total diet and six different herbal medicine were analysed to study ingestion environment. Airborne dust in foundry was analysed and compared with outdoor dust to study inhalation environment. Human hairs of common person, herbal medicine taker and foundry worker were analysed to estimate the trace elemental distribution of people under different inhalation and ingestion environment. Analytical results show that herbal medicines contain higher micronutrients such as Ca, Mg, Mn and Cu that total diet and airborne dust in foundry has high Cr. The concentration of Ca, Mg and Mn in hair of herbal medicine taker is two times higher than in hair of common person and Cr con-centration in hair of foundry worker is about three times higher than in hair of common person. These results show that NAA can be used importantly to monitor human health through biological and environmental samples.

• 한국대기환경학회지
• /
• 제18권5호
• /
• pp.363-372
• /
• 2002

PM$_{10}$ aerosols were collected using low volume air sampler every month intervals from September 1992 to August 1991 in Seoul. These samples were analyzed for 20 trace elements (Al, As, Ba, Br, Ca, Cl, Co, Cr, Fe, K, Mn, Na, Ni, Pb, Sc, Se, Si, Ti, V and Zn) by INAA (instrumental neutron activation analysis), XRF (x-ray fuorescence spectrometer), and ICP (inductively coupled plasma). PM$_{10}$ mass concentrations higher than 70 $\mu$g/m$^3$ were 32% of 60 samples and had significantly higher concentrations in spring and winter than in summer and fall (p-value<0.001). The elements of As, Br, Cl, Ni, Pb, Se, V, and Zn are enriched by factors of 20 to 2,000 relative to their natural abundance in crustal soil. To further identify common sources of pollution-related trace elements, factor analysis was applied to the trace elements concentration data. Major sources that contribute to the atmospheric loading of these elements were found to include fossil fuel combustion, automobile and waste incineration (33.2%), metal processing industry (18.2%), and soil(29.8%).8%).

• 해양환경안전학회:학술대회논문집
• /
• 해양환경안전학회 2007년도 추계학술발표회
• /
• pp.43-49
• /
• 2007

Al, Ag, Au, Cu, Cd, Co, Fe, Ni, Ph, Zn 등과 밀접한 금속은 일반적인 원소이며, 지속적인 오염물질에 속한다. 금속은 생명체의 생리활동에 필수원소인 경우도 있으나 경우도 있으나 그 중의 일부는 정해진 한계값을 초과할 때에는 독성을 가진다. 자연수 중의 미량금속 측정은 정확도와 정밀도에 있어서 큰 오차를 가지고 있음이 장기간 인식되어 왔다. 미국과 유럽에서는 1975 년 이후 미량금속의 해수 중 농도가 과거에 인지된 농도보다 $1/10{\sim}1/1,000$ 정도 낮아졌으며, 수직 분포는 알려진 생물, 물리, 지화학적인 과정들과 일치하고 있음이 밝혀졌다. 이와 같은 결과는 대부분 미량원소에 대한 분석방법과 기기의 발전에 기인하며, 시료 채취, 보관 및 분석 과정에 발생할 수 있는 오염을 제거해야 하는 세심한 주의 요구되어 진다.

• 대한임베디드공학회논문지
• /
• 제10권4호
• /
• pp.233-239
• /
• 2015

This paper describes a method that is integrated trace for real-time virtualization environment. This method has solved the problem that the performance trace may not be able to analyze integrated method between heterogeneous operating systems which is consists of real-time operating systems and general-purpose operating system. In order to solve this problem, we have attempted to reuse the performance analysis function in general-purpose operating system, thereby real-time operating systems can be analyzed along with general-operating system. Furthermore, we have implemented a prototype based on ARM Cortex-A15 dual-core processor. By using this integrated trace method, real-time system developers can be improved productivity and reliability of results on real-time virtualization environment.

• 한국식품위생안전성학회지
• /
• 제11권2호
• /
• pp.135-142
• /
• 1996

In order to grasp, status of trace metals contained and corelation analysis between cereal and soils, the samples which have been collected from four myeons in Ulju-ku Ulsan-city were 48 for cereal and 48 for soils. The average Hg containing level of samples is 0.006 ppm for cereal and 0.062 ppm for soil, Pb is 0.302 ppm for cereal and 0.885 ppm for soil, and Zn is 7.853 ppm for cereal and 2.366 ppm for soil. Corelation analysis between cereal and soils showed statistical significance for Hg, Pb and Cu, but it didn't show any significance for Cd and Zn.

• 한국조리학회지
• /
• 제14권1호
• /
• pp.21-38
• /
• 2008

This research aimed to analyze the differences in financial variables classifying chain restaurants. A total of 126 samples were drawn from financial statements for $2001{\sim}2006$. As a result of analysis, there was a significant difference in Pillai's Trace, Wilks' Lambda, Hotelling's Trace, and Roy's Largest Root values at the significant probability value(p<0.05) based on F value in terms of stability among chain restaurants. Difference was found only in current rate and liabilities in ANOVA. There was a great difference in current rate among institutional restaurants, fast food restaurants, and cafeterias. There was a significant difference in Pillai's Trace, Wilks' Lambda, Hotelling's Trace, and Roy's Largest Root values at the significant probability value(p<0.05) based on F value in terms of restaurants' profitability. In ANOVA, difference was found only in net profits to net sales. It was revealed that all factors showed no significant differences in multiple comparison. All multi-variant test statistics showed a significant difference in growth and turnover. ANOVA showed a significant difference in net sales growth rate, net profit growth rate, and total assets growth rate.

• Nuclear Engineering and Technology
• /
• 제27권2호
• /
• pp.234-247
• /
• 1995

Trace elements in airborne particulates were analyzed by instrumental neutron activation analysis (INAA) under the optimum analytical condition. Neutron irradiation for sample was done at the irradiation hole(neutron flux 1$\times$10$^{13}$ n/$\textrm{cm}^2$.s) of TRIGA MARK-III research reactor in the Korea Atomic Energy Research Institute. For the verification of the analytical method, NIST SRM-1648 and NIES CRM No.8 ore chosen and analyzed. The accuracy and precision of the analysis of 40 and 24 trace elements in the samples were compared with the certified and reported values, respectively. The analytical method was found to be reliable enough when the analytical data of NIES sample were compared with those of different counties. In the analytical result of two or both of standard reference materials, relative standard deviation wes within the 15％ except a few elements and the relative error was within the 10％. We used this method to analyze 30 trace elements in airborne particulates collected with the high volume air sampler(PM-10) at too different locations and also confirmed the possibility to use this method as a routine monitoring tool to find out environmental pollution sources.