• 제목/요약/키워드: tobacco analysis

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Studies on the Change of Nonvolatile Organic acids and Higher Fatty acids during the curing of Flue-cured tobaccos (황색종 잎담배의 건조과정중 비휘발성 유기산과 지방산의 변화에 관한 연구)

  • Rhee, Moon-Soo;Lee, Un-Chul
    • Journal of the Korean Society of Tobacco Science
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    • 제4권2호
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    • pp.75-80
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    • 1982
  • During the process of curing of the tobacco (Nicotiana tabacum L. ) leaves the concentration change of Nonvolatile organic acids and Higher fatty acids of the flue-cured tobacco leaves was observed. The contents of Nonvolatile organic acids in flue-cured tobacco leaves were as follows, malic> oxalic>malonic>citric>succinic acid. Higher fatty acids was linolenic>Palmitic>oleic >stearic$\geqq$linoleic acid, Citric acid content of last curing time was increased about 4~5 times in compare to before curing tobacco. It was concluded that significant changes of three variety flue-cured tobacco but a significant difference was observed in the composition of Daegu gold variety.

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Discrimination of Korean Tobacco's Aroma and Tastes using the Eloctronic Nose/Tongue and Their feasibility in Tobacco Sensory Evaluation

  • Lee Whan-Woo;Lee Seung-Yong;Shon Hyun-Joo;Kim Young-Hoh
    • Journal of the Korean Society of Tobacco Science
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    • 제27권1호
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    • pp.134-140
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    • 2005
  • The purpose of this study was the discrimination of different tobacco types by the E-Nose/tongue and the analysis of what human sensory attributes are correlated with e-instrument's sensors. Samples were made from five groups of Korean domestic tobacco leaves, aged burley and not aged, aged flue-cured and not aged and blending types of the four. Instrumental tests were conducted to discriminate characteristics among different tobacco samples by the E-Nose and the E-Tongue. Sensory attributes of tobacco tastes were impact, irritation, bitterness, hay-like, tobacco taste, smoke volume, smoke pungent and mouth cleanness. STATISTICA software was used to analyze correlation between the human sensory data and the raw data of e-instruments. Discrimination analysis can be achieved using principal components analysis (PCA) and discriminant factorial analysis(DFA). As a result, impact, bitterness, irritation, smoke volume and smoke pungent of human sensory attributes were correlated with data from the several clustered E-Nose sensors(p < 0.10). And bitterness, irritation, and smoke pungent of human sensory attributes were correlated with data from the E-Tongue sensors(p < 0.10). PCA plot by the E-Nose shows that aged tobacco and not aged were discriminated and DFA plot shows that three groups(aged burley, not aged burley and flue-cured) were discriminated. PCA plot by the E- Tongue shows that flue-cured tobacco was separated from burley. Our results indicated that the e-instruments are sensitive enough to distinguish among tobacco types and their several sensors are reacted to the human sensory attributes.

Studies on the Change of Chemical Components of Flue-cured Tobacco with Maturity (황색종 잎담배의 숙도에 따른 화학성분의 변화연구)

  • Hwang, Geon-Jung;Kim, Jeong-Hwan;Kim, Chan-Ho
    • Journal of the Korean Society of Tobacco Science
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    • 제3권1호
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    • pp.20-24
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    • 1981
  • This experiment was carried out to determine the relationships between maturity and content of the chemical components in flue-cured tobacco. The results were as follows : 1) Among the chemical components, the contents of total nitrogen, ammonia nitrogen, total alkaloids, nicotine, total volatile base, petroleum-ether extract, crude fiber, crude ash, water soluble ash, and chlorine decreased significantly, and those of total sugar, reducing sugar, and starch increased as leaf maturity progressed until the stage of ripeness, but, afterwards, a reverse tendency appeared. 2) There was a significant relationship between maturity and the contents of chemical components, such as total nitrogen, protein nitrogen, ammonia nitrogen, total volatile base, and the correlation coefficients of them were -0.743, -0.789, -0.797, and -0.642, respectively.

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Studies on the Analysis of Tobacco Leaf Alkaloids (잎담배 Alkaloid분석에 관한 연구)

  • 장기철;한상빈;김용옥;이운철
    • Journal of the Korean Society of Tobacco Science
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    • 제13권2호
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    • pp.20-26
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    • 1991
  • This study was carried out to develop the method of alkaloids analysis and investigate the kinds and contents of alkaloids in flue-cured, burley and oriental tobacco leaves using developed analytical method. The developed analytical method of alkaloids was as followed : Tobacco sample was treated with acid(pH 2∼3) and extracted with chloroform to remove chemical components except alkaloids. Sample solution was treated with alkali(pH 12∼ 13) and was extracted with chloroform to obtain alkaloids from sample solution. After extraction of alkaloids from tobacco leaves, alkaloids were separated and identified by GC, GC/MS using SE-54 fused silica capillary column. Nicotine, nornicotine, myosmine, 9-nicotyline, anabasine, anatabine, 2, 3-bipyridyl, cotinine, formyl nornicotine, acetyl nornicotine and formal anatabine were isolated and identified from the extracts of tobacco leaves. The contents of alkaloids were burley > flue-cured > oriental tobacco leaves, but oriental tobacco leaves were higher nornicotine, cotinine, formyl nornicotine and acetyl nornicotine contents than those of flue-cured tobacco leaves. The burley tobacco harvested in Korea was higher nornicotine contents by 2-6 times in the portions of cutter, leaf and tips position than that of burley tobacco(B3F) harvested in V. S. A.

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Quality analysis of Reconstituted tobacco ( I ) - On the Physical and Structural properties - (판상엽 품질 특성 분석 (제1보) - 물리적ㆍ구조적 특성에 관하여 -)

  • 한영림;나도영;김삼곤;김근수;강영희
    • Journal of the Korean Society of Tobacco Science
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    • 제26권1호
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    • pp.57-63
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    • 2004
  • A comparative analysis of characteristics of domestic and foreign reconstituted tobacco based on papermaking was conducted to evaluate the quality of reconstituted tobacco and to utilize as basic data for improvement of domestic reconstituted tobacco. In the formation, which is key factor to quality and physical properties of product, foreign reconstituted tobacco has better uniform formation than those of domestic one. These result was attributed to distribution of large floc size in the domestic one unevenly. In the fiber morphology, domestic reconstituted tobacco has larger average fiber length and width than those of foreign one. They indicated that fiber morphology of domestic one will exert structural properties of paper such as formation and permeability. Tensile strength of domestic one has lower than those of foreign one by basis weight. In the air permeability, domestic one was remarkably reduced because base web was over sized. It also will affect the combustibility of reconstituted tobacco. In summary, we conclude that the physical and structural properties of domestic reconstituted tobacco result in quality deviations compared with foreign reconstituted tobacco.

A study on the sponsorship tactics of transnational tobacco companies in Korea: Review and analysis of tobacco industry internal documents (담배회사 내부문건분석을 통한 다국적 담배회사의 국내 후원 전략에 관한 연구)

  • Kim, Hyojin;Lee, Sungkyu;Kang, Eungjeong
    • Korean Journal of Health Education and Promotion
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    • 제33권3호
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    • pp.71-82
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    • 2016
  • Objectives: In this study, it was analyzed which marketing activity strategy multinational tobacco companies established against Republic of Korea through their internal documents and it was checked out how the marketing activities mentioned in the documents turned out to be actually. Methods: For that, analyzed the internal documents of tobacco companies after connecting Legacy Tobacco Documents Library(LTDL). Three documents were selected finally out of total searched 1,752 documents except the ones that did not include the theme or not appropriate. Results: Internal documents analysis showed that people smoke because the filter of cigarette shown in the movies looks nice. Tobacco companies carried out the marketing through sponsorship of soccer games, F1 Grand Prix was found in the internal documents. Conclusions: The legal restriction on marketing activities of tobacco companies should be enhanced by removing the articles of allowing advertisement and promotion for tobacco companies in Korean domestic law.

Statistical Evaluation of Smoke Analysis Technique through Asia Collaborative Study V.

  • Ra, Do-Young;Rhee, Moon-Soo;Kim, Yoon-Dong;Hwang, Keon-Joong
    • Journal of the Korean Society of Tobacco Science
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    • 제20권1호
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    • pp.108-114
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    • 1998
  • This study was conducted to evaluate the techniques or analyzing tobacco smoke by statistical treatment method for the analytical data through Asia Collaborative Study V. In addition to five smoke components analysis, consisting of TPM, water, nicotine, NFDPM, and puff count of four cigarettes samples, statistical parameters such as mean, standard deviation, box-and-whisker plots, h plots, k plots, regression coefficients, reproducibility (R), and repeatability (r) were also calculated. Analysis of water content of cigarette smoke was the most difficult task, whereas puff count analysis was the easiest as well recognized by all laboratories. Analysis of nicotine and puff count accounted for both the lowest and the highest variation among four parameters. The water coefficients indicated more randomness or variation in the slops. The NFDPM data exhibited both types of deviations from linearity. Water content of sample D indicated the highest difference between two single results and between two interlaboratory test results. As a whole, KGTRI ranked higher in the analytical techniques for statistical evaluation of results when compared with the practices of 28 other laboratories.

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Composition Studies on the Aromatic Tobacco Varieties (Nicotiana tabacum L.): 1. Characteristics of Less-Volatile Organic Components. (향끽미종 잎담배 성분조성에 관한 연구 1. 휘발성이 적은 유기성분의 특성조사)

  • Kim, Kyoung-Rae;Park, Jeen-Woo;Lee, Un-Chul;Heu, Il
    • Journal of the Korean Society of Tobacco Science
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    • 제2권2호
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    • pp.1-7
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    • 1980
  • Less-volatile organic components in leaves from aromatic tobaccos of different varieties, both Oriental and Korean types were isolated and concentrated using a simple apparatus with fewer manipulations. Each less-volatile concentrate was then subjected to spectrophotometric recording in the visible range, to thin-layer chromatographic group separation, and high-performance liquid chromatographic profile analysis. The methods allow detection of significant quantitative differences in visible absorption spectra, TLC patterns, and high resolution HPLC profiles among varieties.

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Uncertainty of Total Alkaloids and Reducing Sugar Determination in Flue-cured Tobacco (황색종 담배중 전알카로이드와 환원당 분석에 대한 불확도 측정)

  • 백순옥;장기철;이운철;한상빈
    • Journal of the Korean Society of Tobacco Science
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    • 제23권1호
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    • pp.45-52
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    • 2001
  • This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

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Determinants of Tobacco Cessation Behaviour among Smokers and Smokeless Tobacco Users in the States of Gujarat and Andhra Pradesh, India

  • Sarkar, Bidyut K.;Arora, Monika;Gupta, Vinay K.;Reddy, K. Srinath
    • Asian Pacific Journal of Cancer Prevention
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    • 제14권3호
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    • pp.1931-1935
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    • 2013
  • Background: This study was undertaken to identify the socio-demographic determinants of quit attempts among smokers and smokeless tobacco users to identify correlates of tobacco cessation behaviour in India Materials and Methods: This was a cross-sectional study for the outcome of quit attempts made by current tobacco users in last 12 months in twelve districts in two states. Simple and multivariable logistic regression analysis was used to obtain the odds ratios (ORs) of socio-demographic variables (age, gender, education, occupation, socio-economic status, community, area, type of family) and tobacco user status (smoker/smokeless). Results: In the combined analysis, a smoker had higher predicted probability of attempting quitting (OR-1.41,CI 1.14-1.90), in comparison to a smokeless tobacco user and a tobacco user in the state of Gujarat was less likely to attempt quitting than a user in Andhra Pradesh (OR-0.60, CI 0.47-0.78). The probability of making a quit attempt was higher among tobacco users who were more educated (OR-1.40, CI 1.04-1.94), having a higher socio-economic status (SES) (OR-2.39, CI 1.54-3.69), and belonging to non-agricultural labourer occupational group (OR-1.90, CI 1.29-2.78). The effects were maintained even after adjusting for all other variables. In disaggregated analysis, findings were similar except in smokeless as a separate group, education level was not significantly associated with quit attempts and with lower odds (OR-0.91, CI 0.58-1.42). Conclusions: This is one of the first studies to provide useful insight into potential determinants for quit attempts of tobacco users in India including smokeless tobacco users, exploring the socio-demographic patterning of correlates of quit attempts.