• 대한기계학회논문집A
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• 제22권2호
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• pp.311-320
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• 1998

The cryogenic fracture behaviors of austenitic stainless steel HN2 developed for nuclear fusion reactor were evaluated quantitatively by using the small punch(SP) test. The electrochemical polarization test was applied to study thermal aging degradation of HN2 steel. The X-ray diffraction(XRD) analysis was conducted to detect carbides and nitrides precipitated on the grain boundary of the heat treated HN2 steel. The mechanical properties of the HN2 steel significantly decreased with increasing time and temperature of heat treatment or with decreasing testing temperature. The integrated charge(Q) obtained from electrochemical polarization test showed a good correlation with the SP energy(ESP) obtained by means of SP tests. From the results observed in the x-ray diffraction and anodic polarization curve, it was known that the material the grain boundary. Combining SP test and electrochemical polarization test, it could be useful tools to non-destructively evaluate the cryogenic fracture behaviors and the aging degradation for cryogenic structural material.

• 대한기계학회논문집A
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• 제21권3호
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• pp.519-527
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• 1997

AISI 316 steel has been used extensively for heater and boiler tube of the structural plants such as power, chemical and petroleum plants under severe operating conditions. Usually, material degradation due to microcrack or precipitation of carbides and segregation of impurity elements, is occured by damage accumulated for long-term service at high temperature in this material. In this study, the effect of aging time on fracture toughness was investigated to evaluate the measurement of material degradation. The elastic-plastic fracture toughness behaviour of AISI 316 steel pipe aged at $550^{\circ}C$for 1h-10000h (the aged material) was characterized using the single specimen J-R curve technique and eletric potential drop method at normal loading rate(load-line displacement speed of 0.2mm/min) in room temperature and air environment. The fracture toughness data from above experiments is compared with the $J_{in}$ obtained from predicted values of crack initiation point using potential drop method.

• 한국화재소방학회논문지
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• 제1권1호
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• pp.19-26
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• 1987

In this study, fire resistance of steel fiber reinforced concrete was investigated Cylindrical and prismatic specimens made of Ordinary Portland Cement plain concrete and steel fiber reinforced concrete were exposed to heating in accordance with a standard time-temperature curve as specified in KS·F22 57, method of fire resistance test for structural parts of buildings, the period of heating was 1 hour and 2 hours. After the fire resistance test, mechanical properties of specimens such as compressive and bending strength, stress-strain curve, static and dynamic modulus of elasticity and bending toughness were investigated. Also the cracks and spallings of the specimens were observed. From the test results, it was confirmed that steel fiber reinforced concrete has a excellent fire resistance than plain concrete in the view of higher residual strength of concrete and smaller crackings because of steel fibers in concrete.

• 한국철도학회논문집
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• 제8권1호
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• pp.57-62
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• 2005

The frost heaving pressure can be a problem for weakening of the railway roadbed material. This study was initiated to investigate the soils frost heaving pressure and physical characteristics(Liquid limit, permeability, SEM analysis) resulting from freezing and freezing-thawing cycle process. Therefore, upon freezing a saturated soil in a closed-system from the top, a considerable pressure was developed. Weathered granite soils, sandy soil were used in the laboratory freezing test which sometimes subjected to thermal gradients under closed-systems. The frost heaving pressure arising within the soil samples and the temperature of the samples inside were monitored with elapsed time. The degree of saturation versus heaving pressure curve is also presented for weathered granite soil and the maximum pressure is closely related to this curve. Based on the laboratory test results, fine-grained soils with strong attractive forces between soil grains md water molecules, and additional water is attracted into the pores leading to further volume changes and ice segregation.

• Journal of Pharmaceutical Investigation
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• 제23권3호spc1호
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• pp.9-18
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• 1993

Sugar spheres loaded with melatonin (MT) were coated with $Aquacoat^{\circledR}$ to control the release rate of MT over 8 hours. A zero-order release pattern over 8 hours was obtained with 20% coating on 8-10 mesh beads in USP basket dissolution studies. MT in 20% coated beads was quite stable at room temperature with less than 5% MT degraded during 6 months' storage. Dissolution profiles were also unchanged after 6 months. An oral preparation containing MT-loaded uncoated beads for immediate release and 20% coated beads with $Aquacoat^{\circledR}$ for controlled release over 8 hours was evaluated in six human subjects. When total 0.5 mg MT as low dose (immediate release portion of MT, 0.1 mg) was administered to four subjects, average peak plasma MT concentration was reached at about 600 pg/ml and maintained at about 10 pg/ml over 8 hours. Plasma MT concentration-time profiles were similar in shape to computer-simulated profiles. However, maximal plasma MT concentrations were three times greater compared to computer simulated curve. These results suggest that MT dose, ratio of immediate and controlled release MT, and pharmacokinetic parameters selected are adjusted to mimic endogenous MT concentration-time curve. In another study, 0.2 mg MT having 10% of immediate release portion and 80% controlled release portion produced plasma MT concentration-time curve which is more similar to endogenous profiles. A low bioavailability (<20%) may result from extensive first pass metabolism and remaining amounts of MT from controlled beads. A good correlation between plasma MT concentration and urinary excretion rate of 6-sulphatoxymelatonin (6-STMT), a major metabolite of MT was observed. As plasma MT concentration increased, urinary excretion rate of 6-STMT increased concomitantly. The linear relation between plasma MT and urinary excretion rate of 6-STMT was statistically significant. This result suggests that urinary 6-STMT may be used as an index of circadian rhythms of MT in humans.

• Bulletin of the Korean Chemical Society
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• 제5권4호
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• pp.154-158
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• 1984

In order to characterize the permeability of small unilamellar vesicles (SUV), efflux of 6-carboxyfluorescein (6-CF) from the vesicles was monitored spectrophotofluorometrically. Since the entrapped highly quenched 6-CF (200 mM) became fluorescent upon release from the vesicles, the 6-CF could be used as an efflux probe. SUV containing entrapped 6-CF was prepared from egg phosphatidylcholine and separated by gel filtration on Sepharose 4B. Observed change of relative fluorescent intensity with time was sigmoidal. From this curve, the parameter of permeability was determined either by half-time or a released amount per unit time from the initial slope. Half-time of efflux of prepared SUV having 302 ng phospholipid/ml in 10 mM Tris-HCl buffer pH 7.4 was 21.0 min at $37{\circ}C$. Various factors which could affect the half-time were examined including temperature, pH, salt, and vesicle concentration. In particular the effect of vesicle concentration on the efflux revealed that the permeability can be a function of the concentration.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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• pp.666-669
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• 2002

The differences of the effects of mechanical substance pre-activation in the mills with divers force effect schemes on the self-propagating high temperature synthesis (SHS) of the $SiO_2$ + 37.5% Al system were investigated. The power saturation of activated material state are estimated referring on the variations of dilatometry curve paths. The effects of activation time on the temperature of sample self-ignited in the furnace, combustion temperature and completeness of the quartz reaction with aluminium were determined. The enhancing effects of organic modifiers of quartz particle surfaces on the further SHS synthesis development were shown.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.231-236
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• 2001

A newly developed Advanced Indentation System (AIS), which is a portable and nondestructive system for evaluating tensile properties, was used to measure mechanical behavior of materials used under high temperature and pressure conditions. This test measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation and fracture. Aging effects of Cr-Mo and Cr-Mo-V steel at high temperature were simulated. Tensile properties including yield strength and tensile strength at various temperature are obtained from the test. For all test materials and conditions, the AIS-derived results were in good agreement with those from conventional standard test method. Examples of the test results ate given and potential applications of the AIS to assess the integrity of aging structures are briefly discussed.

• 한국초전도ㆍ저온공학회논문지
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• 제12권4호
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• pp.36-40
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• 2010

In this paper, a noble method for rapid cooldown of pulse tube refrigerator (PTR) was proposed and experimentally investigated. An orifice pulse tube refrigerator generates refrigeration effect by expansion PV work at the cold-end, and its amount is affected by the orifice valve opening. There exists the optimum valve opening for maximum cooling capacity and it varies as cold-end temperature. It is verified from simulation results using isothermal model that the optimum valve opening increases as the cold-end temperature increases. In the experiments, a single stage orifice pulse tube refrigerator is fabricated and tested. The fabricated PTR shows 97.5 K of no-load temperature and 10 W at 110 K of cooling capacity with the fixed orifice valve opening. From experiments, the initial cooldown curve with four cases of valve opening control scenario are obtained. And it is experimentally verified that the initial cooldown time can be reduced through the control of orifice valve opening.

• Nuclear Engineering and Technology
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• 제56권1호
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• pp.1-8
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• 2024

In this study, the influence of thermal aging on structural integrity is investigated for Gr. 91 steel. A commercial grade Gr. 91 steel is used for the virgin material, and service-exposed Gr. 91 steel is sampled from a steam pipe of a super critical plant. Time versus creep strain curves are obtained through creep tests with various stress levels at 600 ℃ for the virgin and service-exposed Gr. 91 steels, respectively. Based on the creep test results, the improved Omega model is characterized for describing the total creep strain curve for both Gr. 91 steels. The proposed parameters for creep deformation model are used for predicting the steady-state creep strain rate, creep rupture curve, and stress relaxation. Creep-fatigue damage is evaluated for the intermediate heat exchanger (IHX) in a large-scale sodium test facility of STELLA-2 by using creep deformation model with proposed creep parameters and creep rupture curve for both Gr. 91 steels. Based on the comparison results of creep fatigue damage for the virgin and service-exposed Gr. 91 steels, the thermal aging effect has been shown to be significant.