• 제목/요약/키워드: time-temperature curve

검색결과 390건 처리시간 0.03초

은을 이용한 착색유리 제조에 관한 연구 (Study on Colour Development in Silver Containing Glass)

  • 이종근
    • 한국세라믹학회지
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    • 제11권2호
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    • pp.3-10
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    • 1974
  • For the manufacture of the silver-yellow glass, silver nitrate was used as a colorant in the base glass of $K_2O$-CaO-$SiO_2$ system. The latter in which the optimum condition was revealed showing beautiful yellow color had been selected among others after the preparatory studies to choose base glass. Other base glass systems considered were $Na_2O$-CaO-$SiO_2$, $R_2O$-PbO-$SiO_2$ and $R_2O$-PbO-BaO-$SiO_2$. The color developed on the specimen in various conditions was examined, using spectorphotometer, in term of the changes in absorbance with wavelength in the visible range. Experimental variables were the amount of the colorant and the additives, reheating temperature and time. The additives such as ZnO, BaO, $B_2O_3$ and $As_2O_3$ were added to increase the coloring action. It was observed that as the amount of silver increased in the base glass the absorbance around $410{\mu}m$ showed the increasing tendency, but the width of absorption curve was wider. Hence, the optimum amount of silver appeared to be 0.11~0.12%. It was found that ZnO was effective additive when present about 0.1%, while $As_2O_3$ ineffective rather retarding the coloration. Borax and $BaCO_3$ were proved effective when contained separately, but appeared ineffective when coexisted. Proper reheating temperature and time was ranged 550~$580^{\circ}C$ and 50~60 minutes. The higher the reheating temperature and the longer the reheating time, the absorbance was increased, while the width of absorption curve was wider. The colored glass prepared in the present experimental condition was found to have good water-resistance for the decorative purpose.

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초음속 비행체 구조재료에 대한 열기계적 특성 (Thermomechanical Characteristics for Structural Material of Supersonic Vehicle)

  • 김종환;이기범;이경용
    • 한국군사과학기술학회지
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    • 제8권2호
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    • pp.77-87
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    • 2005
  • The thermomechanical characteristics were evaluated for 17-4PH stainless steel widely used in supersonic airframe subjected to both aerodynamic loading and heating. The thermomechanical tests were conducted under both elevated temperature and rapid heating condition from $1^{\circ}C/sec\;to\;28^{\circ}C/sec$. The thermomechanical behaviors under rapid heating were compared with those of elevated temperature after 1/2 hour exposure in terms of yield stress to investigate the influence of heating rates. A heating rate-yield temperature parameter was suggested for rapid heating based on time-temperature parameters, and master yield stress curve was obtained by using these parameters. The experimental results and methodology from this study can be used as basic engineering data when designing supersonic vehicle structures subjected to aerodynamic loading and severe heating environment.

시분해 레이저 유도 백열법을 이용한 매연 입자 크기에 관한 수치적 연구 (Numerical Investigation on Soot Primary Particle Size Using Time Resolved Laser Induced Incandescence (TIRE-LII))

  • 이종호;김정용;정동수;장영준;전충환
    • 대한기계학회논문집B
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    • 제29권9호
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    • pp.1022-1031
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    • 2005
  • Temporal behavior of the laser induced incandescence (LII) signal is often used for soot particle sizing, which is possible because the cooling behavior of a laser heated particle is dependent on the particle size. In present study, LII signals of soot particles are modeled using two non-linear coupled differential equations deduced from the energy- and mass-balance of the process. The objective of this study is to obtain an appropriate calibration curve for determining primary particle size by comparing the gated signal ratio and double-exponential curve fitting methods. Not only the effects of laser fluence and gas temperature on the cooling behavior but also heat transfer mechanisms of heated soot particle have been investigated. The second-order exponential curve fitting showed better agreements with the LII signals than the gated signal ratio method which was based on the lust-order exponential curve fit. And the temporal decay rate of the LII signal and primary particle size showed nearly linear relationship, which was little dependent on the laser fluence. And it also could be reconfirmed that vaporization was dominant process of heat loss during first loons after laser pulse, then heat conduction played most important role while thermal radiation had little influence all the time.

Stress Estimation of a Drain Current in Sub-threshold regime of amorphous Si:H

  • Lee, Do-Young;Lee, Kyung-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2007년도 7th International Meeting on Information Display 제7권2호
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    • pp.1172-1175
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    • 2007
  • We have investigated the threshold voltage shifts(${\Delta}Vth$) and drain current level shift (${\Delta}Ids$) in subthreshold region of a-Si:H TFTs induced by DC Bias (Vgs and Vds) - Temperature stress (BTS) condition. We plotted the transfer curves and the ${\Delta}Vth$ contour maps as Vds-Vds stress bias and Temperature to examine the severe damage cases on TFTs. Also, by drawing out the time-dependent transfer curve (Ids-Vgs) in the region of $10^{-8}\;{\sim}\;10^{-13}$ (A) current level, we can estimate the failure time of TFTs in a operating condition.

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고온 크리프 구조물의 장시간 한계응력강도 예측 (Prediction of Long-Term Stress Intensity Limit of High-Temperature Creep Structures)

  • 김우곤;류우석;김현희
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 춘계학술대회
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    • pp.648-653
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    • 2003
  • In order to predict stress intensity limit of high-temperature creep structures, creep work-time equation, defined as $W_ct^P=B$, was used, and the results of the equation were compared with isochronous stress-strain curve (ISSC) ones of ASME BPV NH Code. For this purpose, the creep strain tests with. time variations for commercial type 316 stainless steel were conducted with different stresses; 160 MPa, 150 MPa, 145 MPa, 140 MPa and 135 MPa at $593^{\circ}C$. The results of log $W_c$ and log t plots showed a good linear relation up to $10^5$ hr. The constants p, B and stress intensity limit values showed comparatively good agreement to those of ASME NH ISSC. It is believed that the relation can be simply obtained with only several short-term 1% strain data without ISSC which can be obtained by long-term creep data.

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WC-Co 초경합금의 산화거동 (Oxidation Behavior of WC-Co Hardmetal)

  • 이길근;권한상;하국현
    • 한국분말재료학회지
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    • 제11권2호
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    • pp.111-117
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    • 2004
  • The oxidation behavior of 91 WC-9Co hardmetal in weight percentage has been studied in the present work as a part of the development of recycling process. The morphological and compositional changes of the WC-Co hardmetal with oxidation time at 90$0^{\circ}C$ were analyzed by using surface observation and X-ray diffraction. respective]y. As the oxidation time increased, the WC-Co hardmetal was continuously expanded to form porous oxide mixtures of $CoWO_4$ and $WO_3$. The morphology of porous oxide mixture was basically dependent on initial shape of the WC-Co hardmetal. From thermo-gravimetric (TG) analysis, it was found that the oxidation rate was increased with increasing oxidation temperature and oxygen content in the flowing atmospheric gas. The fraction of oxidation versus time curves showed S-curve relationship at a given of oxidation temperature. These oxidation behaviors of the WC-Co hardmetal were discussed in terms of previously proposed kinetic models.

사출성형에서 캐비티압력과 인장강도에 관한 연구 (A Study on Cavity Pressure and Tensile Strength of Injection Molding)

  • 유중학;김희송
    • 한국자동차공학회논문집
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    • 제2권6호
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    • pp.110-116
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    • 1994
  • In this research, the tensile strength of molded parts and pressure distribution were analyzed to study the cavity filling stage and packing stage in injection molding. The measurement of cavity pressure was obtained by a data acquisition system with the installation of transducers in the cavity. Molded parts were tested by a universal testing machine to obtain the tensile strength. For the experimental work, the tensile strength of molded parts increased with longer packing time and exact freezing time of the gate was obtained by a cavity pressure curve. In addition, the effect of packing did not occur and tensile strength was almost constant after early 1.5 sec of the freezing time of gate. Density tended to be higher about 0.2% due to a larger degree of mold temperature and melt temperature. Also, changing pressure in the cavity was effectively sensed. Thereafter, the possibility of the development of pattern recognition expert system was confirmed on the basis of the experimental results.

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연소관 내열고무의 내열성능평가를 위한 시험장치 개발 (A Development of Test Equipment for Thermal Protection Performance on Insulator used in Rocket Motor Chamber)

  • 강윤구;박종호
    • 한국추진공학회지
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    • 제20권3호
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    • pp.32-36
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    • 2016
  • 고체로켓추진기관 연소관 내열고무의 열반응 특성을 평가하기 위한 모사시험장치를 개발하였다. 시험장치는 연소실 압력 2,500 psi, 연소시간 100 s까지 시험할 수 있으며, 여러 시편을 동시에 상대 비교 할 수 있다. 시편 부는 사각 패널로 되어 있으며, 마주보는 두 면에서는 연소시간 동안 시편 내부의 온도 변화를 측정할 수 있다. 시험장치의 안전성을 확인하기 위하여 연소실 유효평균압력 1,000 psi, 유효연소시간 10 s 시험을 수행하였으며, 내열고무의 열특성 분석에 필요한 기본 데이터들, 즉 연소실의 압력-시간 선도, 재료 내부에서의 온도-시간 선도, 재료의 열파괴 두께를 획득하였다.

초내열합금 Nimonic 80A의 미세조직 변화에 관한 연구 (Microstructure Evolution of Superalloy Nimonic 80A)

  • 정호승;조종래;박희천
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2004년도 춘계학술대회 논문집
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    • pp.174-177
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    • 2004
  • The nickel-based alloy Nimonic 80A possesses strength, and corrosion, creep and oxidation resistance at high temperature. These products are used for aerospace, marine engineering and power generation, etc. The control of forging parameters such as strain, strain rate, temperature and holding time is important because the microstructure change in hot working affects the mechanical properties. It is necessary to understand the microstructure variation evolution. The microstructure change evolution occurs by recovery, recrystallization and grain growth phenomena. The dynamic recrystallization evolution has been studied in the temperature range $950-1250^{\circ}C$ and strain rate range $0.05-5s^{-1}$ using hot compression tests. The metadynamic recrystallization and grain growth evolution has been studied in the temperature range $950-1250^{\circ}C$ and strain rate range 0.05, $5s^{-1}$, holding time range 5, 10, 100, 600 sec using hot compression tests. Modeling equations are developed to represent the flow curve, recrystallized grain size, recrystallized fraction and grain growth phenomena by various tests. Parameters of modeling equation are expressed as a function of the Zener-Hollomon parameter. The modeling equation for grain growth is expressed as a function of initial grain size and holding time.

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두께감육 평가를 위한 SH-EMAT파의 모드특성 분석 (Mode Characteristics Analysis of the SH-EMAT Waves for Evaluating the Thickness Reduction)

  • 박익근;김용권
    • 한국생산제조학회지
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    • 제19권2호
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    • pp.198-203
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    • 2010
  • In this paper, study on the mode characteristics analysis of the SH-EMAT (shear horizontal, electromagnetic acoustic transducer) waves for evaluating the thickness reduction in plates such as corrosion and friction is presented. Noncontact methods for ultrasonic wave generation and detection have been a great concern and highly demanded due to their capability of wave generation and reception on surface of high temperature or on rough surface. Mode identification of the SH-EMAT wave is carried out in an aluminum plate with thinning defects using time frequency analysis method such as wavelet transform, compared with theoretically calculated group velocity dispersion curve. The changes of various wave features such as the amplitude and the time-of-flight have been observed and the correlations with the thickness reduction have been investigated. Firstly, experiments have been conducted to confirm that it is possible to selectively generate and receive specific desired SH modes. These modes have then been analyzed to select the parameters that are sensitive to the thickness change. The results show that the mode cutoff and the time-of-flight changes are feasible as key parameters to evaluate the thickness reduction.