• Journal of Welding and Joining
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• v.18 no.2
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• pp.213-213
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• 2000

This study was performed to investigate types and formation mechanism of cracks in two Al alloy welds, A5083 and A7NO1 spot-welded by pulse Nd: YAG laser, using SEM, EPMA and Micro-XRD. In the weld zone, three types of crack were observed: center line crack($C_{C}$), diagonal crack($C_{D}$), and U shape crack($C_{U}$). Also, HAZ crack($C_{H}$), was observed in the HAZ region, furthermore, mixing crack($C_{M}$), consisting of diagonal crack and HAZ crack was observed.White film was formed at the hot crack region in the fractured surface after it was immersed to 10%NaOH water. In the case of A5083 alloy, white films in C crack and $C_D crack region were composed of low melting phases, Fe₂Si$Al_8$ and eutectic phases, Mg₂Al₃ and Mg₂Si. Such films observed near HAZ crack were also consist of eutectic Mg₂Al₃. In the case of A7N01 alloy, eutectic phases of CuAl₂, $Mg_{32}$ (Al,Zn) ₃, MgZn₂, Al₂CuMg and Mg₂Si were observed in the whitely etched films near $C_{C}$ crack and $C_{D}$ crack regions. The formation of liquid films was due to the segregation of Mg, Si, Fe in the case of A5083 alloy and Zn, Mg, Cu, Si in the case of A7N01 aooly, respectively.The $C_{D}$ and $C_{C}$ cracks were regarded as a result of the occurrence of tensile strain during the welding process. The formation of $C_{M}$ crack is likely to be due to the presence of liquid film at the grain boundary near the fusion line in the base metal as well as in the weld fusion zone during solidification. The $C_{U}$ crack is considered a result of the collapsed keyhole through incomplete closure during rapid solidification. (Received October 7, 1999)

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2005.05a
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• pp.216-227
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• 2005

The head penetrations for control rod drive mechanism and instrumentation systems are installed at the reactor pressure vessel head of PWRs. Primary coolant water and the operating conditions of PWR plants can cause cracking of these nickel-based alloy through a process called primary water stress corrosion cracking (PWSCC). Inspection of the head penetrations to ensure the integrity of the head penetrations has been interested since reactor coolant leakages were found at U. S. reactors in 2000 and 2001. The complex geometry of the head penetrations and the very low echo amplitude from the fine, multiple flaws due to the nature of the see made it difficult to detect and size the flaws using conventional pulse-echo UT methods. Time-of-flight-diffraction technique, which utilizes the time difference between the flaw tips while pulse-echo does the flaw response amplitude from the flaw, has been selected for this inspection for it's best performance of the detection and sizing of the head penetration see flaws. This study defines the limits of the detectable and accurately sizable minimum flaw size which can be detected by the General TOFD and the Delta TOFD techniques for circumferentially and axially oriented flaws respectively. These results assures the reliability of the inspection techniques to detect and accurately size for various kind of flaws, and will also be utilized for the future development and qualifications of the TOFD techniques to enhance the detecting sensitivity and sizing accuracy of the flaws of the reactor head penetrations in nuclear power plants.

• Journal of Pharmaceutical Investigation
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• v.12 no.4
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• pp.112-125
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• 1982

Sulfamethoxazole particles were microencapsulated using the gelatin-acacia complex coacervation method. Micromeritic properties and dissolution characteristics of the microcapsules were studied. The particle size distribution followed log-normal form. As the hardening time increased, the particle size and wall thickness increased ($45.3-52.0\;{\mu}m$, $2.02-5.12\;{\mu}m$, respectively). This is considered to be due to the cross-linked wall structure of formalized microcapsules which prevents shrinking of gelatin during the dehydration and drying processes. An increase of hardening time clearly delayed the release rate. The in vitro 50% dissolution time $(t_{50})$ for unencapsulated sulfamethoxazole powder was less than 3 min.; for microcapsules hardened for 30 min, the $t_{50}$ was 20.1 min.; for those hardened for 60 min. the $t_{50}$ was 25.0 min.; for those hardened for 120 min., the $t_{50}$ was 35.8 min. The surface of the unhardened microcapsules was smooth and had no cracking or pore penetration. However, the surface of the hardened microcapsules was folded and invaginated.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2001.05c
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• pp.62-65
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• 2001

The effects of accelerated UV radiation on EPDM used for a polymeric insulator were investigated by contact angle, surface voltage decay after corona charging, SEM-EDX, ATR-FTIR and XPS. EPDM occurs as loss of hydrophobicity by UV treatment, which followed by surface cracking and chalking. The surface voltage decay on UV-treated EPDM show that the shorter decay time corresponded to the treated samples with a longer UV exposure time. The surface oxygen and aluminum content were found to increase and carbon decrease, as is observed in EDX analysis. The ATR-FTIR and XPS indicated that C-C and C-H groups decreased and the highly oxidized carbon bonds such as C-O, C=O and O-C=O increase with time. Also, the effects of surface charges on hydrophobicity based on our results is discussed.

• Proceedings of the Korea Concrete Institute Conference
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• 1996.10a
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• pp.473-479
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• 1996

Until now, we assumed in the time-dependent analysis of concrete structure that tensile creep has same characteristics as compressive creep has. But, in according to results of researches, it appears that tensile creep is different from compressive creep in quantity and in mechanics because tensile creep is affected significantly by micro cracking. The test results indicate that the creep behavior of concrete in compression and tension is rather different. The test data shows that the amount of creep under tensile loading is larger than that under compressive loading. In this paper, a realistic tensile creep model is suggested and incorporated in the formulation. In order to get more accurate results of time-dependent analysis. The present study indicates that the long-term deflection of concrete structures under realistic tensile creep model is somewhat larger than that under ordinary compressive creep model.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.28 no.5
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• pp.610-616
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• 2004

The aim of this study was to investigate the hydride embrittlement when the LBB evaluation was carried out for the integrity of PHWR Pressure Tubes. The transverse tensile and CCT toughness tests were performed at three hydrogen concentrations while the test temperatures were changed (RT to 30$0^{\circ}C$). Both the transverse tensile and the fracture toughness tests showed the hydrogen embitterment clearly at RT but this phenomenon was disappeared while the test temperature arrived at 25$0^{\circ}C$. Using the DHC test results, the CCL and LBB time were calculated and compared. The hydride embrittlement at the LBB evaluation made the LBB time short definedly. If the operating temperature, DHCV and LBB deterministic parameters such as A and m were known, LBB time could be estimated without the calculation of CCL.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2002.05a
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• pp.173-178
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• 2002

Fourier transform has been one of the most common tools to study the frequency characteristics of signals. With the Fourier transform alone, it is difficult to tell whether signal's frequency contents evolve in time or not. Except for a few special cases, the frequency contents of most signals encountered in the real world change with time. Time-frequency methods are developed recently to overcome the drawbacks of Fourier transform, which can represent the information of signals in time and frequency at the same time. In this study, heat damage process of a carbon fiber reinforced plastic(CFRP) and glass fiber reinforced plastic(GFRP) under monotonic tensile loading was characterized by acoustic emission. Different kinds of specimens were used to determine the characteristics of Strength and AE signals. Time-frequency analysis methods were employed for the analysis of fracture mechanism in CFRP such as matrix cracking, debonding and fiber fracture.

• Geomechanics and Engineering
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• v.34 no.1
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• pp.1-15
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• 2023

This study conducts uniaxial compression tests on intact and single crack-contained rocks to investigate the time-frequency domain characteristics of acoustic emission (AE) signals monitored during the deformation failure process. A processing approach, short-time Fourier transform (STFT), is performed to obtain the evolution characteristics of time-frequency domain of AE signals. The AE signal modes at different deformation stages of rocks are different. Five modes of AE signal are observed during the cracking process of rocks. The evolution characteristics of time-frequency domain of AE signals processed by STFT can be utilized to evaluate the damage process of rocks. The difference of time-frequency domain characteristics between intact and cracked rocks is comparatively analyzed. The distribution characteristics of frequency changing from a single band-shaped cluster to multiple band-shaped clusters can be regarded as an early warning information of damage and failure of rocks. Meanwhile, the attenuation of frequency enables the exploration of rock failure trends.

• Corrosion Science and Technology
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• v.6 no.6
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• pp.316-321
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• 2007

The effect of annealing on the pitting corrosion resistance of anodized Al-Mg alloy (AA5052) processed by equal-channel angular pressing (ECAP) was investigated by electrochemical techniques in a solution containing 0.2 mol/L of $AlCl_3$ and also by surface analysis. The Al-Mg alloy was annealed at a fixed temperature between 473 and 573 K for 120 min in air after ECAP. Anodizing was conducted for 40 min at $100-400A/m^2$ at 293 K in a solution containing 1.53 mol/L of $H_2SO_4$ and 0.0185 mol/L of $Al_2(SO_4)_3$. The internal stress generated in anodic oxide films during anodization was measured with a strain gauge to clarify the effect of ECAP on the pitting corrosion resistance of anodized Al-Mg alloy. The time required to initiate the pitting corrosion of anodized Al-Mg alloy was shorter in samples subjected to ECAP, indicating that ECAP decreased the pitting corrosion resistance. However, the pitting corrosion resistance was greatly improved by annealing after ECAP. The time required to initiate pitting corrosion increased with increasing annealing temperature. The strain gauge attached to Al-Mg alloy revealed that the internal stress present in the anodic oxide films was compressive stress, and that the stress was larger with ECAP than without. The compressive internal stress gradually decreased with increasing annealing temperature. Scanning electron microscopy showed that cracks occurred in the anodic oxide film on Al-Mg alloy during initial corrosion and that the cracks were larger with ECAP than without. The ECAP process of severe plastic deformation produces large internal stresses in the Al-Mg alloy; the stresses remain in the anodic oxide films, increasingthe likelihood of cracks. It is assumed that the pitting corrosion is promoted by these cracks as a result of the higher internal stress resulting from ECAP. The improvement in the pitting corrosion resistance of anodized AlMg alloy as a result of annealing appears to be attributable to a decrease in the internal stresses in anodic oxide films

• Journal of Hydrogen and New Energy
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• v.26 no.2
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• pp.114-119
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• 2015

Nowdays, fossil fuels have been used as an important resource in development of industry. But it is limited and caused climate change such as pollution and global warming. So nuclear fusion research is being issued with tritium to develop eco-friendly and sustainable energy. Republic of Korea is in charge of Storage and Delivery System (SDS) in the International Thermonuclear Experimental Reactor (ITER), weld present in the SDS bottles are easily exposed to the hydrogen embrittlement of special characteristics of the hydrogen in hydrogen atmosphere, When the hydrogen embrittlement is rapidly progresses, the cracking is generated in the weld zone. Due to this cracking, the risk of leakage of tritium into the atmosphere occurs. In this study, hydrogen heat treatment was processed through the Pressure-Composition-Temperature (PCT) device according to the time variation. Also mechanical properties such as rupture strength test, three point bend test and hardness test in accordance with the respective time have been conducted and the fracture was observed by scanning electron microscopy(SEM) after the mechanical properties evaluation.