• Journal of Magnetics
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• v.4 no.1
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• pp.26-32
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• 1999

The HDDR process can be used as an effective means of processing of the coercive Nd-Fe-B-type or the Sm2Fe17Nx materials. The HDDR (hydrogenation, disproportionation, desorption, recombination) processed materials are feartured with a very fine microstructure. The thermomagnetic characteristics of the Nd-Fe-B-type or the Sm2Fe17Nx materials with fine microstructure due to the HDDR process were investigated. It has been found that the fine-microstructured hard magnetic materials showed an unusual TMA (Thermomagnetic analysis) tracting featured with a low and constant magnetization at lower temperature range and a peak just below their Curie temperatures when a low external field is applied. This thermomagnetic characteristic was immediate particularly in the TMA with a low applied field. This thermomagnetic characteristic was interpreted in terms of the competition between two counteracting effects; the decrease in magnetication due to the thermal agitation at an elevated temperature and the increase in magnetization resulting from the rotation of magnetization of the fine grains comparable to a critical single domain size due to the decreased magnetocrystalline anisotropy at an elevated temperature.

• Proceedings of the Korean Magnestics Society Conference
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• 2000.09a
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• pp.397-406
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• 2000

Hopkinson effect in the HDDR-treated Nd$\sub$15/Fe$\sub$77/B$\sub$8/ alloy was examined in detail by means of a thermomagnetic analysis with low magnetic field (600 Oe). The emergence and magnitude of maximum in magnetisation in the thermomagnetic curve due to the Hopkinson effect was correlated to the grain structure and coercivity of the HDDR-treated material. the HDDR-treated materials showed clear Hopkinson effect (maximum in magnetisation just below the Curie temperature of the Nd$\sub$2/Fe$\sub$14/B phase) on heating in the thermomagnetic curve. Magnitude of the magnetisation rise due to the Hopkinson effect became smaller as the recombination time increased. The magnetisation recovery at room temperature on cooling from above the Curie temperature became smaller as the recombination time increased. The HDDR-treated materials with shorter recombination time, finer grain size and higher coercivity showed larger magnetisation maximum due to Hopkinson effect in the thermomagnetic curve.

• Journal of Magnetics
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• v.3 no.4
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• pp.99-104
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• 1998

The $ Sm_2Fe_{17}N_x $materials were prepared by the combination consisting of the HDDR (hydrogenation, disproportionation, desorption, and recombination) process and nitrogenation or by the conventional way consisting of nitrogenation only, and the magnetic and thermomagnetic properties of the materials were investigated. The magnetic characterisation of the prepared $ Sm_2Fe_{17}N_x $ materials was performed using a VSM. Thermal stability of the materials was evaluated using a DTA under Ar gas atmosphere. The thermomagnetic characteristics of the materials were examined using a Sucksmith-type balance. The previously HDDR-treated Sm2Fe17parent alloy was found to be nitrogenated more easily compared to the ordinary $ Sm_2Fe_{17}N_x $alloy. The $ Sm_2Fe_{17}N_x $ material produced by the combination method showed a high coercivity (12.9 kOe) even in the state of coarse particle size (around 60 ${\mu}{\textrm}{m}$). It was also revealed that the $ Sm_2Fe_{17}N_x $ material produced by the material produced by the combination showed an unusual TMA tracing featured with a low and constant magnetisation at lower temperature range and a peak just before the Curie temperature. This thermomagnetic characteristic was interpreted in terms of the competition between two counteracting effects; the decrease in magnetisation due to the thermal agitation at an elevated temperature and the increase in magnetisation resulting from the rotation of magnetisation of the fine grains comparable to a critical single domain size due to the decreased magnetocrystalline anisotropy at an elevated temperature.

• Proceedings of the Korean Magnestics Society Conference
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• 1991.05a
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• pp.23-24
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• 1991

• 한국전산유체공학회:학술대회논문집
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• 2008.08a
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• pp.68.4-68.4
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• 2008

• Proceedings of the Optical Society of Korea Conference
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• 1989.02a
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• pp.235-241
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• 1989

Static according tests were carried out on a series of amorphous TbFe thin films of various composition under a constant laser irradiation condition. Examination of recorded domain configurations by using polarizing microscope led to the categorization of domain characteristics into 3 distinctly different types; i.c., type A: circular domains with smooth boundaries, the size not sensitive to variation of bias field, type B: domains of irregular shape at low bias, the size increasing and the boundaries getting smoother and more circular with increasing bias field and type C: not recordable. Critical factor which distinguishes among each types was fond to be the relative magnitude of H and H of the film near T, regardless of constituent atomic species. Micromagnetical process of thermomagnetic recording cycle was analyzed scheniatically for each type.

• Proceedings of the Korean Magnestics Society Conference
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• 2003.12a
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• pp.283-283
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• 2003

• Proceedings of the Korean Magnestics Society Conference
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• 1994.03a
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• pp.62-63
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• 1994

• Proceedings of the Materials Research Society of Korea Conference
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• 1998.08a
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• pp.126.1-126
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• 1998

• Journal of Magnetics
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• v.11 no.1
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• pp.36-42
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• 2006

In this report, we demonstrate a comprehensive analysis of the effects of Au addition on the microstructure and magnetic properties of $Fe_{73.5}Si_{13.5}B_{9}Nb_{3}Au_1$ Finemet-type alloy. It was found that the as-quenched alloys were the amorphous state and turned into nanocrystalline state under heat treatments. The DSC analysis indicates that the sharply exothermal peak corresponding to the crystallization of the $\alpha-Fe(Si)$ was observed at $547-579^{\circ}C$ depending on the heating rates, which is little higher than that of original Finemet (542-$570{^{\circ}C}$, respectively). Besides, the thermomagnetic result confirmed that the full substitution of Cu by Au with the single phase structure in the M(T) curve along cooling cycle. Ultrasoft magnetic properties of the nanocrystallized samples were significantly enhanced by the proper annealing such as the increase of permeability and the decrease of the coercivity. The optimum annealing condition was found at the annealing temperature of $540^{\circ}C$ and the increase of the annealing time up to 90 min.