• Title/Summary/Keyword: tensile adhesion strength

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Effect of carboxymethyl chitosan on postoperative intraperitoneal adhesion formation in the rat (Rat에서 carboxymethyl chitosan의 복강수술후 유착형성에 미치는 효과)

  • Jang, Kwang-ho;Kwon, Yong-sam;Kim, Jung-eun;Kwon, Eun-ju;Oh, Tae-ho;Lee, Keun-woo;Jang, In-ho
    • Korean Journal of Veterinary Research
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    • v.40 no.3
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    • pp.635-643
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    • 2000
  • The aim of this study was to determine the effectiveness of carboxymethyl chitosan(CMC) solution on preventing intraperitoneal adhesions. In this study, 44 rats were divided into four groups ; an untreated control group and three experimental groups that were treated with 3 ml of 1, 2 or 3% CMC solution, respectively. The anti-mesenteric serosa of the ileum was exteriorized and then abraded in a standard manner by scraping with a scalpel blade to create homogenous petechial hemorrhagic surface over a $0.5{\times}1cm$ area. The adhesions were blindly assessed 2 weeks later by using a computerized tensiometer. The mean tensile strength(Newton) of formed adhesions was $2.48{\pm}0.88$ in control group, $1.86{\pm}0.56$ in the 1% CMC-treated group, $1.75{\pm}0.71$ in the 2% CMC-treated group and $1.55{\pm}0.60$ in the 3% CMC-treated group. The most favorable prevention against adhesion was achieved in the 3% CMC-treated group(p<0.01). We could conclude that CMC was effective on preventing the formation of postoperative small intestinal adhesions in the rat.

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Bending Fatigue Reliability Improvements of Cu Interconnects on Flexible Substrates through Mo-Ti Alloy Adhesion Layer (Mo-Ti 합금 접착층을 통한 유연 기판 위 구리 배선의 기계적 신뢰성 향상 연구)

  • Lee, Young-Joo;Shin, Hae-A-Seul;Nam, Dae-Hyun;Yeon, Han-Wool;Nam, Boae;Woo, Kyoohee;Joo, Young-Chang
    • Journal of the Microelectronics and Packaging Society
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    • v.22 no.1
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    • pp.21-25
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    • 2015
  • Bending fatigue characteristics of Cu films and $8{\mu}m$ width Cu interconnects on flexible substrates were investigated, and fatigue reliability improvement was achieved through Mo-Ti alloy adhesion layer. Tensile bending fatigue reliability of Cu interconnects is 3 times lower than that of Cu films, and even compressive bending fatigue reliability of Cu interconnects is 6 times lower than that of Cu films. From these results, mechanical crack formation could be fatal in Cu interconnects. With Mo-Ti adhesion layer, fatigue reliability of Cu films and interconnects were enhanced due to the increase of adhesion strength and the suppression of slip induced crack initiation.

A Study on Improvement of Thermal and Adhesion Properties of Stone/Wood Composites for Stone Bed using CNT-epoxy Adhesive (CNT/Epoxy 접착제를 이용한 돌침대용 석재/목재 복합재의 열적특성 및 접착특성 개선 연구)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Kwon, Dong-Jun;Moon, Sun-Ok;Park, Joung-Man
    • Composites Research
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    • v.29 no.5
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    • pp.276-281
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    • 2016
  • Improvement of the thermal and adhesion properties of stone/wood composites was studied. Tensile test was performed for wood and stone to know the basic mechanical properties. Real-time temperature of stone and wood was measured when stone and wood was heated. To compare thermal transfer properties of stone/wood composites, two types of specimens were tested: one was stone upper whereas another was wood upper. Real time temperature measurement and lap shear test were performed to know thermal and adhesion properties by using CNT-epoxy adhesive in which CNT was dispersed in epoxy adhesive uniformly. The thermal transfer property was better for the wood upper case than stone upper case. Adding CNT improved the heat transfer as well as mechanical properties including lap shear strength.

Micro-tensile Bond Strength of Composite Resin Bonded to Er:YAG Laser-prepared Dentin (Er:YAG 레이저로 삭제된 상아질에 대한 컴포지트 레진의 미세인장결합강도에 관한 연구)

  • Min, Suk-Jin;Ahn, Yong-Woo;Ko, Myung-Yun;Park, June-Sang
    • Journal of Oral Medicine and Pain
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    • v.31 no.3
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    • pp.211-221
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    • 2006
  • Purpose The aims of this study were to evaluate micro-tensile bond strength of composite resin bonded to dentin following high-speed rotary handpiece preparation or Er:YAG laser preparation with two different adhesive systems and to assess the influence of different Er:YAG laser energies on the micro-tensile bond strength. Materials and Methods In this study, 40 third morlars were used. Flat dentin specimans were obtained and randomly assigned to eight groups. Dentin surfaces were prepared with one of four cutting types: carbide bur, Er:YAG laser (2 W, 3 W and 4 W) and conditioned with two bonding systems, Scotchbond Multipurpose Plus (SM), Clearfil SE bond (SE) and composite resin-build ups were created. After storage for 24 hours, each specimen was serially sectioned perpendicular to the bonded surface to produce more than thirty slabs in each group. Micro-tensile bond strength test was performed at a crosshead speed of 1.0 mm/min. Micro-tensile bond strengths (${\mu}TBS$) were expressed as means$\pm$SD. Data were submitted to statistical analysis using two-way ANOVA, one-way ANOVA, Student-Newman-Keuls' multiple comparison test and t-test. Results and Conclusion 1. Regardless of bonding systems, the ${\mu}TBS$ according to cutting types were from highest to lowest : 3 W, 2 W, Bur, and 4 W. In addition, there was no significant difference between Bur and 4 W (p<0.001). 2. Regardless of cutting types, SM showed significantly higher ${\mu}TBS$ than SE (p<0.001). 3. Bonding to dentin conditioned with SM resulted in higher ${\mu}TBS$ for 3 W compared to Bur, 2 W, and 4 W. There was no significant difference between 2 W and Bur (p<0.001). 4. Bonding to dentin conditioned with SE resulted in higher ${\mu}TBS$ for 3 W compared to 2 W, 4 W, and Bur. Bur exhibited significant lower ${\mu}TBS$ than all other cutting types. There were no significant differences between 3 W, 2 W and between 4 W and Bur (p<0.001). 5. The ${\mu}TBS$ of laser cutting groups were shown in order from highest to lowest: 3 W, 2 W and 4 W in two bonding systems. There was no significant difference between 2 W and 3 W in SE (p<0.001). : The ${\mu}TBS$ of composite resin bonded dentin was significantly affected by interaction between the cutting type and bonding system. In the range of 2 W-3 W, cavity preparation of the Er:YAG laser seems to supply good adhesion of composite resin restoration no less than bur preparation. In particular, if you want to use the self-etching system, including Clearfil SE bond for the purpose of a simplification of the bonding procedures and prevention of adverse effects by excessive etching, an Er:YAG laser may offer better adhesion than a bur.

A Study on the Joint Tensile Strength of EVA Waterproofing Sheet According to Hot Air Welding Speed and Chemical Attack in Low Temperature (저온 환경에서의 열풍융착 속도별 화학적 침식이 EVA 방수시트의 접합부 인장강도에 미치는 영향에 대한 연구)

  • Park, Jin-Sang;Choi, Su-Young;Park, Wan-Goo;Jung, Hae-Choon;Kim, Byoung-Il;Oh, Sang-Keun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.3
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    • pp.320-326
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    • 2017
  • This study is based on the hot air welding application method of EVA sheet to test the tensile strength performance changes due to the hot air welding speed, temperature and chemical attack. For the parameters of the study, the hot air welding method that directly heats the overlap between the sheets and the adhesion surface was controlled, and the maximum temperature for application was set to $20^{\circ}C$, $0^{\circ}C$, $-5^{\circ}C$, $-10^{\circ}C$. According to the results of the testing, the tensile strength of the overlap area was the highest between the temperatures of 20 at 5~6m/min and between the low temperatures at 3~4m/min of hot air welding speed.

Effect of Silane Coupling Agent on Adhesion Properties between Hydrophobic UV-curable Urethane Acrylate and Acrylic PSA (소수성 UV 경화형 우레탄 아크릴레이트와 아크릴 점착제 사이의 계면 부착력 향상을 위한 에폭시 실란의 영향)

  • Noh, Jieun;Byeon, Minseon;Cho, Tae Yeun;Ham, Dong Seok;Cho, Seong-Keun
    • Applied Chemistry for Engineering
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    • v.31 no.2
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    • pp.230-236
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    • 2020
  • In this study, an adhesive tape with water and impact resistance for mobile devices was developed using a UV-curable urethane acrylate based polymer as a substrate. The substrate fabricated by UV-curable materials shows hydrophobicity and poor wettability, which significantly deteriorates the interface-adhesions between the substrate and acrylic adhesive. In order to improve the interface adhesion, 3-glycidoxy-propyl trimethoxysilane (GPTMS), a silane coupling agent having epoxy functional groups, was selected and incorporated into UV-curable urethane acrylate based polymer resins in various contents. The changes of the chemical composition according to the contents of GPTMS was studied with Fourier-transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS) to know the surface bonding properties. Also mechanical properties of the substrate were characterized by tensile strength, gel fraction and water contact angle measurements. The peel strengths at 180° and 90° were measured to compare the adhesion between the substrate and adhesive according to the silane coupling agent contents. The mechanical strength of the urethane acrylate adhesive tape decreased as the silane coupling agent increased, but the adhesion between the substrate and adhesives increased remarkably at an appropriate content of 0.5~1 wt%.

Evaluation of Fluidity Over Time and Mechanical Properties of Cement-based Composite Materials for 3D Printing (3D 프린팅용 시멘트계 복합재료의 경시변화 및 역학적 특성평가)

  • Seo, Eun-A;Lee, Ho-Jae;Yang, Keun-Hyeok
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.26 no.4
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    • pp.73-80
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    • 2022
  • This study evaluated changes in fluidity and rheological properties over time for 3D printed composite materials, and evaluated compressive strength and splitting tensile strength properties for laminated and molded specimens. The composite material for 3D printing starts to change rapidly after 30 minutes of extrusion, and the viscosity of the material tends to be maintained up to 90 minutes, but it was confirmed that construction within 60 minutes after mixing is effective. The compressive strength of the laminated test specimen showed equivalent or better performance at all ages compared to the molded test specimen. In the stress-strain curve of the laminated specimen, the initial slope was similar to that of the molded specimen, but the descending slope was on average 1.9 times higher than that of the molded specimen, indicating relatively brittle behavior. The splitting tensile strength of the P-V laminated specimen was about 6% lower than that of the molded specimen. It is judged that this is because the interfacial adhesion force against the vertical load is affected by the pattern direction of the laminated test specimen.

Interfacial Evaluation of Flax and Hemp Fibers/Polypropylene Composites Using Micromechanical Test and Acoustic Emission (Micromechanical 시험법과 음향방출을 이용한 Flax 와 Hemp섬유 강화된 Polypropylene 복합재료의 계면 물성 평가)

  • Son, Tran-Quang;Hwang, Byung-Sun;Park, Joung-Man
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.04a
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    • pp.42-45
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    • 2005
  • Interfacial evaluation of various combinations of both Flax and Hemp fibers/polypropylene were performed by using micromechanical test and nondestructive acoustic emission (AE). It can be because interfacial adhesion between the natural fiber surface and matrix plays an important role in controlling the overall mechanical properties of polymer composite materials by transferring the stress from the matrix to the fiber. It is necessary to characterize the interphase and the level of adhesion to understand the performance of the composites properly. Microfailure mechanism of single Flax fiber bundles were investigated using the combination of single fiber tensile test and nondestructive acoustic emission. Microfailure modes of the different natural fiber/polypropylene systems were observed using optical microscope and determined indirectly by AE and their FFT analysis.

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A study on the EVA reforming processes transparency sheet and nonwoven warm air point adhesion using of tunnel waterproofing method. (EVA개질 투명시트와 부직포를 열풍 점융착한 일체형 방수시트를 이용한 터널방수공법에 관한 연구)

  • Seon Yun-Suk;Kim Jaun-Sull;Kim Su-Ryon;Oh Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.05a
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    • pp.185-190
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    • 2005
  • Safe, economical and environment-friendly tunnel construction are required again along with social continuous development, the importance of waterproof work that is portion that actually all of user and builder can find that is embossed by tunnel construction's one of important construction. Also, ECB (Ethylen Copolymer Bitumen) sheet that is used in existing tunnel waterproofing method (ECB waterproofing method) being black because asphalt (Bitumen) is added, by purpose that make illumination of tunnel interior brightly and scar discovery eases in sheet with coating white film, but ECB that is used present according as ECB that asphalt is added does not satisfy high tensile strength of construction field, quality standard of extension. Also ECB denigrates color of black M/B that asphalt is excepted.

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Interfacial Evaluation of Modified Jute and Hemp Fibers/Polypropylene (PP)-Maleic Anhydride Polypropylene Copolymers (PP-MAPP) Composites Using Micromechanical Test and Nondestructive Acoustic Emission (Micromechanical 시험법과 음향방출을 이용한 Flax 와 Hemp 섬유 강화 에폭시 복합재료의 계명 물성 평가)

  • Son, Tran Quang;Hwang, Byung-Sun;Park, Joung-Man
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.157-160
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    • 2005
  • The surface energies and acid-base interaction between the untreated and treated Jute or Hemp fibers and different matrix compositions of polypropylene-maleic anhydride polypropylene copolymers (PP-MAPP) were investigated using dynamic contact angle measurement. The contribution of the acid-base property into the interfacial adhesion of the natural fibers/matrix systems were characterized by calculating the work adhesion coming from the acid-base interaction. On the other hand, microfailure mechanism of both single Jute and Hemp fiber bundles were investigated using the combination of single fiber tensile test and acoustic emission. Distinctly different micro failure modes of the different natural fiber/polypropylene systems wet ε observed using optical microscope and determined indirectly by AE and their FFT analysis.

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