• Title/Summary/Keyword: system separation method

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Determination of the Trace Elements in $UO_2$ Powder by ICP-AES Directyl Coupled with Extraction Chromatography (추출크로마토그래피와 유도결합플라스마 원자방출분광법을 이용한 이산화우라늄분말 중 미량금속불순물 분석)

  • Choi, Kwang-Soon;Lee, Chang-Heon;Pyo, Hyung-Yeal;Han, Sun-Ho;Suh, Moo-Yul;Eom, Tae-Yoon;Lee, Gae-Ho
    • Journal of the Korean Chemical Society
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    • v.37 no.9
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    • pp.813-819
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    • 1993
  • An ICP-AES system directly connected with a separation column was used in order to determine the trace elements in $UO_2$ powder promptly and reduce the volume of the waste solution. The outlet of a separation column, which was filled with Teflon powder ($330\;{\mu}m$) coated with tri-n-butyl phosphate (TBP) as extractant, was directly connected with sample injection tube of ICP-AES. Eleven elements including molybdenum in $UO_2$ powder were separated and determined simultaneously. Recoveries of these elements were $91{\sim}110%$ and these results were agreed with those of solvent extraction methods. This method was applicable to quality control in manufacturing nuclear fuel.

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PIV Measurements of the Flow characteristics around a single rudder in a backward state (역추진시 단동타 주위 유동특성에 대한 PIV계측)

  • Shon, Chang-Bae;Gim, Ok-Sok;Oh, Woo-Jun;Lee, Chang-Woo;Lee, Gyoung-Woo
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2010.04a
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    • pp.383-384
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    • 2010
  • The control surface on a ship is to control the motion of it in forward and backward states. In this paper, the measured results has been compared with each other to predict the backward flow characteristics of the single rudder's 2-dimensional section at $Re=2.0\times10^4$ using 2-frame grey level cross correlation PIV method especially, The separation region appears at 10 to 20 degrees angle of attack in a forward state. The separation point and boundary layer demonstrate in the same angle of attack compared it with the forward states.

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A Numerically Controlled Oscillator for Multi-Carrier Channel Separation in Cdma2000 3X (Cdma2000 3X 다중 반송파 채널 분리용 수치 제어 발진기)

  • Lim In-Gi;Kim Whan-Woo
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.29 no.11A
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    • pp.1271-1277
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    • 2004
  • We propose a foe phase tuner and a rounding processor for a numerically controlled oscillator (NCO), yielding a reduced phase error in generating a digital sine waveform. By using the fine Phase tuner Presented in this paper, when the ratio of the desired sine wave frequency to the clock frequency is expressed as a fraction, an accurate adjustment in representing the fractional value can be achieved with simple hardware. In addition, the proposed rounding processor reduces the effects of phase truncation on the output spectrum. Logic simulation results of the NCO for multi-carrier channel separation in cdma2000 3X multi-carrier receive system using these techniques show that the noise spectrum and mean square error (MSE) are reduced by 8.68 dB and 5.5 dB, respectively compared to those of truncation method and 2.38 dB and 0.83 dB, respectively, compared to those of Paul's scheme.

A Pd Doped PVDF Hollow Fibre for the Dissolved Oxygen Removal Process

  • Batbieri G.;Brunetti A.;Scura F.;Lentini F.;Agostino R G.;Kim, M.J.;Formoso V.;Drioli E.;Lee, K.H.
    • Korean Membrane Journal
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    • v.8 no.1
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    • pp.1-12
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    • 2006
  • In semiconductor industries, dissolved oxygen is one of the most undesirable contaminants of ultrapure water. A method for dissolved oxygen removal (DOR) consists in the use of polymeric hollow fibres, loaded with a catalyst and fed with a reducing agent such as hydrogen. In this work, PVDF hollow fibres loaded with Pd were characterized by means of perporometry, scanning electron microscopy (SEM), energy dispersive X-ray (EDX). The hollow fibre analyzed shows a five-layer structure with remarkable morphological differences. An estimation of pore diameters and their distribution was performed giving a mean pore diameter of 100 nm. The permeance and selectivity of the fibres were measured using $H_2,\;N_2,\;O_2$ as single gases, at different operating conditions. An $H_2$ permeance of $37 mmol/m^2s$ was measured and $H_2/O_2$ and $H_2/N_2$ selectivities of ca. 3 were obtained. $H_2$ permeance was 1/3 when a water stream flows in the shell side. Catalytic fibrebehaviour was simulated using a mathematical model for a loop membrane reactor, considering only $O_2$ and $H_2$ diffusive transport inside the membrane and their catalytic reaction. Dimensionless parameters such as the Thiele modulus are employed to describe the system behaviour. The model agrees well with the experimental reaction data.

Enhanced High Contrast Image Rendering Method Using Visual Properties for Sharpness Perception (시각 선명도 감각 특성을 이용한 개선된 고명암 대비 영상 렌더링 기법)

  • Lee, Geun-Young;Lee, Sung-Hak;Kwon, Hyuk-Ju;Sohng, Kyu-Ik
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.38A no.8
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    • pp.669-679
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    • 2013
  • When an image is converted from HDR (high dynamic range) to LDR (low dynamic range), a tone mapping process is the essential component. Many TMOs (tone mapping operators) have been motivated by human vision which has lower physical luminance range than that in real scene. The representative of human vision properties which motivate TMOs is the local adaptation. However, TMOs are ultimately compressing image information such as contrast, saturation, etc. and the compression causes defects in image quality. In this paper, in order to compensate the degradation of the image which is caused by TMOs, the visual acuity-based edge stop function is proposed for applying the property of human vision to base-detail separation. In addition, using CSF (contrast sensitivity function) which represents the relationship among spatial frequency, contrast sensitivity, and luminance, the sharpness filter is designed and adaptively applied to the detail layer in regard to surround luminance.

Improvement of Hairy Vetch Seed Production by Mixture Cropping of Hairy Vetch and Triticale

  • Seo Jong Ho
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.50 no.2
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    • pp.73-78
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    • 2005
  • Demand for the domestic hairy vetch seed production will be increased with the increasing interest of environment-friendly agriculture in Korea. This study was conducted during from 2000 fall to 2003 spring at upland field of National Institute of Crop Science in Suwon, Korea to compare wheat and triticale (TC) as stake crop of hairy vetch (HV), and to know proper seeding rates and ratios between TC and HV for the maximum HV seed production. As supporting crop of HV, TC was superior to wheat at the points of higher HV seed yield, stronger TC stalk for supporting, consistence of ripening stage of two seeds. In seeding method, row seeding was superior to broadcast seeding at the points of less lodging and higher HV seed yield. HV seed yield decreased with the increase of TC seeding rate in mixture cropping (row seeding), particularly at TC seeding rates over 5kg/10a. HV seed yield increased with the increase of HV seeding rate at the condition of TC seeding rates under 5kg/10a in spite of higher lodging of mixed crops at higher HV seeding rate due to higher HV aboveground dry matter. Maximum HV seed yield was obtained at TC seeding rate of $1\~1.5kg/10a$ as indicating HV seed yield 176kg/l0a (CV. Madison) at seeding rate of TC 1kg/10a + HV 2 kg/10a in 2001, and HV seed yield 96kg/10a (CV. Common) at seeding rate of TC 1.5kg/10a + HV 4.5kg/10a in 2003. Use of all-purpose combine harvester for harvesting and appliance for separation of mixed seeds using centrifugal force, which are prerequisite for HV seed production, was excellent in the simultaneous seeds production system of HV and TC.

Qualitative Analysis of the Major Constituents in Traditional Oriental Prescription Bang-poong-tong-sung-san by Liquid Chromatography/Ultraviolet Detector/Ion-Trap Time-of-Flight Mass Spectrometry

  • Eom, Han Young;Kim, Hyung-Seung;Han, Sang Beom
    • Mass Spectrometry Letters
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    • v.5 no.1
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    • pp.24-29
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    • 2014
  • An advanced and reliable high performance liquid chromatography (HPLC)/ultraviolet detector (UV)/ion-trap time-of-flight (IT-TOF) mass spectrometry was developed for the simultaneous quantification of 19 marker compounds in Bang-poong-tong-sung-san (BPTS), a traditional oriental prescription. Various parameters affecting HPLC separation and IT-TOF detection were investigated, and optimized conditions were identified. The separation was achieved on a Capcell PAK C18 column ($1.5mm{\times}250mm$, $5{\mu}m$ particle size) using a gradient elution of acetonitrile and water containing 0.1% formic acid at a flow rate of 0.1 mL/min. The column temperature was maintained at $40^{\circ}C$ and the injection volume was $2{\mu}L$. IT-TOF system was equipped with an electrospray ion source (ESI) operating in positive or negative ion mode. The optimized electrospray ionization parameters were as follows: ion spray voltage, +4.5 kV (positive ion mode), or -3.5 kV (negative ion mode); drying gas ($N_2$), 1.5 L/min; heat block temperature, $200^{\circ}C$. Automatic $MS^n$ (n = 1~3) analyses were carried out to obtain structural information of analytes. Elemental compositions and their mass errors were calculated based on their accurate masses obtained from a formula predictor software. The marker compounds in BPTS were identified by comparisons between $MS^n$ spectra from standards and those from extracts. Moreover, the libraries of $MS^2$ and $MS^3$ spectra and accurate masses of parent and fragment ions for marker compounds were constructed. The developed method was successfully applied to the BPTS extracts and identified 17 out of 19 marker compounds in the BPTS extracts.

Preconcentration, Separation and Determination of lead(II) with Methyl Thymol Blue Adsorbed on Activated Carbon Using Flame Atomic Absorption Spectrometry (불꽃원자 흡수 분광법으로 활성탄소에 흡착된 메틸티몰 블루로 납(II)의 예비농축, 분리 및 측정)

  • Ensafi, Ali A.;Ghaderi , Ali R.
    • Journal of the Korean Chemical Society
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    • v.52 no.1
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    • pp.16-22
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    • 2008
  • on-line system for preconcentration and separation of lead(II) is presented. The method is based on the complex formation of Pb(II) with adsorbed Methyl thymol blue on activated carbon. The conditions of preparing the solid phase reagent and of quantitative recovery of Pb(II) from diluted solutions, such as acidity of aqueous phase, solid phase capacity, and flow variables were studied as well as effect of potential interfering ions. After preconcentration step, the metal ions are eluted automatically by 5 ml of 0.5 M HNO3 solution and the lead ions content was determined by flame atomic absorption spectrometry. Under the optimum conditions, the lead ions in aqueous samples were separated and preconcentrated about 1000-fold by the column. The detection limit was 0.001 g mL-1. Lead has been determined in river and tap water samples, with recovery of 98 to 102%.

A method for improving wear-leveling of flash file systems in workload of access locality (접근 지역성을 가지는 작업부하에서 플래시 파일시스템의 wear-leveling 향상 기법)

  • Jang, Si-Woong
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.12 no.1
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    • pp.108-114
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    • 2008
  • Since flash memory cannot be overwritten, new data are updated in new area. If data are frequently updated, garbage collection which is achieved by erasing blocks, should be performed to reclaim new area. Hence, because the count of erase operations is limited due to characteristics of flash memory, every block should be evenly written and erased. However, if data with access locality are processed by cost benefit algorithm with separation of hot block ad cold block though the performance of processing is hight wear-leveling is not even. In this paper, we propose CB-MB (Cost Benefit between Multi Bank) algorithm in which hot data are allocated in one bank and cold data in another bank, and in which role of hot bank and cold bank is exchanged every period. CB-MB shows that its performance is 30% better than cost benefit algorithm with separation of cold block and hot block its wear-leveling is about a third of that in standard deviation.

The Technological Method for Safe Processing of Sensitive Information in Network Separation Environments (망분리 환경에서 민감정보를 안전하게 처리하기 위한 기술적 방안)

  • Juseung Lee;Ilhan Kim;Hyunsoo Kim
    • Convergence Security Journal
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    • v.23 no.1
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    • pp.125-137
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    • 2023
  • Companies that handle sensitive information, led by public institutions, establish separate networks for work and the Internet and protect important data through strong access control measures to prevent cyber attacks. Therefore, systems that involve the junction where the Intranet(internal LAN for work purposes only) and the Internet network are connected require the establishment of a safe security environment through both administrative and technical measures. Mobile Device Management(MDM) solutions to control mobile devices used by institutions are one such example. As this system operates by handling sensitive information such as mobile device information and user information on the Internet network, stringent security measures are required during operation. In this study, a model was proposed to manage sensitive information data processing in systems that must operate on the Internet network by managing it on the internal work network, and the function design and implementation were centered on an MDM solution based on a network interconnection solution.