• Title/Summary/Keyword: synthetic temperature

Search Result 808, Processing Time 0.03 seconds

Electrical Machines and Drives for Potentially Explosive Atmospheres

  • Grantham, Colin
    • Journal of international Conference on Electrical Machines and Systems
    • /
    • v.1 no.1
    • /
    • pp.128-134
    • /
    • 2012
  • This paper gives an overview of the requirements for electrical equipment in potentially explosive atmospheres and describes how these are applied to electrical machines and drives in hazardous areas. The method by which equipment can be shown to be safe in a whole range of gases, by testing in a single test gas, is covered. It is shown how the more recently introduced methods of protection for hazardous areas, increased safety and nonsparking, are ideally suited to AC machines and drives. A novel method of measuring the fullload temperature rise of electrical machines for hazardous, and other areas, without the need to connect a mechanical load to the machine's drive shaft is explained.

Synthesis of Iron Oxide Using Ferrous Sulfate by Ozone Treatment (황산제일철 용액의 오존 처리에 의한 산화철 합성)

  • Kim Sam-Joong;Suhr Dong-Soo;Eom Tae-Hyoung;Song Kyung-Sub;Roh Jea-Seung
    • Korean Journal of Materials Research
    • /
    • v.14 no.5
    • /
    • pp.353-357
    • /
    • 2004
  • The influences of the ozone oxidation, reaction temperature and NaOH equivalent ratio on the iron oxide formation were studied with fixed ferrous sulfate concentration(0.5M $FeSO_4$$7H_2$O). Geothite($\alpha$-FeOOH) and/or Magnetite ($Fe_3$$O_4$) were synthesized depending on the reaction conditions. The characteristics of the synthesized powders were evaluated by XRD, SEM and quantitative phase analysis. The synthetic conditions to get Goethite were quite different from the results of Kiyama's and the Goethite was conveniently synthesized at low temperature and at low NaOH equivalent ratio.

Preparation of Sr-Ferrite Powders by Hydrothermal (수열합성법에 의한 Sr-Ferrite 분말합성)

  • 이경희;이병하;김상규
    • Journal of the Korean Ceramic Society
    • /
    • v.24 no.1
    • /
    • pp.17-22
    • /
    • 1987
  • This study is to detect the synthetic condition for the formation of Sr-Ferrite(SrFe12O19) by hydrothermally reaction. Mixed suspension of SrCl26H2O and FeCl3 6H2O were fixed on pH and were subjected to autoclavings at various temperature(150∼300$^{\circ}C$), reaction time(2hrs.∼48hrs.). The Sr-Ferrite powders were synthesized at 150$^{\circ}C$ for 36hrs, 200$^{\circ}C$ for 4hrs and 250$^{\circ}C$ for 2hrs. Synthesized powders were increased particle sizes at longer reaction time and higher reaction temperature. It has hexagonal ferrite M-type structure and has high purity of SrO.5.6 Fe2O3 composition.

  • PDF

Study for Synthetic Oil Performance Test Comparing with Mineral Gear oil in an Agitator Gear Box:Power consumption, Temperature, Oil & parts life for the Heavy load gear box in the Phosphoric Acid Plant (뉴스초점 - 광유와 합성유의 에너지 소비량, 온도변화 등의 성능시험 비교 고찰)

  • Lee, Jae Keun
    • Journal of the Korean Professional Engineers Association
    • /
    • v.45 no.6
    • /
    • pp.28-32
    • /
    • 2012
  • Namhae chemical is one of the largest fertilizer manufacturing company in Korea which company has operating 4 unit agitator gear boxes and producing variety kinds of fertilizer production. The gearbox operating temperature of agitator is approximated in $55^{\circ}C{\sim}90^{\circ}C$ and required to keep operating continuous without stopping. The system required high performance oil and longer oil drain interval as limited workforce in maintenance team. It was lubricated by mineral gear oil of ISO VG 320 and also need to change to new oil frequently. Namhae Chemical would expect to keep stable operating condition without shut down and consider, lower cost of operation and equipment protection.

  • PDF

Characteristics of Nickel-Diamond Composite Powders by Electroless Nickel Plating (무전해 니켈 도금법으로 제조된 니켈-다이아몬드 복합분체의 특성)

  • ;;Hoang Tri Hai
    • Journal of Powder Materials
    • /
    • v.11 no.3
    • /
    • pp.224-232
    • /
    • 2004
  • Ni-diamond composite powders with nickel layer of round-top type on the surface of synthetic diamond (140/170 mesh) were prepared by the electroless plating method (EN) with semi-batch reactor. The effects of nickel concentration, feeding rates of reductant, temperature, reaction time and stirring speeds on the weight percentage and morphology of deposited Ni, mean particle size and specific surface area of the composite powders were investigated by Atomic Adsortion Spectrometer, SEM-EDX, PSA and BET. It was found that nucleated Ni-P islands, acted as catalytic sites for further deposition and grown into these relatively thick layers with nodule-type on the surface of diamond by a lateral growth mechanism. The weight percentage of Ni in the composite powder increased with reaction time, feeding rate of reductant and temperature, but decreased with stirring speed. The weight percentage of Ni in Ni-diamond composite powder was 55% at 150 min., 200 rpm and 7$0^{\circ}C$ .

Control Effect on Root-knot Nematodes by Hot Water Dipping Treatment in Kiwifruit

  • Ma, K.;Cho, Y.;Jeong, B.;Choi, D.
    • Korean Journal of Organic Agriculture
    • /
    • v.19 no.spc
    • /
    • pp.255-258
    • /
    • 2011
  • When kiwifruit root system infected with nematodes was treated by hot water dipping treatment, the maximum temperature for this treatment was suggested as $50^{\circ}C$. The lowest killing temperature of internal root-knot in the root tissue was $48^{\circ}C$. Consequently, root-knot nematodes could be killed without damaging root tissues by the hot water dipping treatment at $48^{\circ}C$ for 10 minutes. This could be useful for organic production and distribution of kiwifruit seedlings by avoiding the synthetic nematicides which are not easily decomposed in soil once applied.

A Study on the Dyeing Properties of Chestnut Bur Extract on Silk and Cotton(I) (밤송이 추출액을 이용한 견 및 면직물 염색(I))

  • 장재철;전동원;김애순
    • Textile Coloration and Finishing
    • /
    • v.12 no.5
    • /
    • pp.280-287
    • /
    • 2000
  • For thousands of years, dyes were obtained from natural sources, such as plants and animals. Although synthetic dyes have replaced many natural dyes for commercial use but natural dyes with their fascinating color are still used extensively by some people. To investigate the dyeing properties of chestnut bur, which is most widely found in our country, some experiments were performed under the several dyeing conditions with silk and cotton fabrics. It was found that $\lambda_{max}$ of chestnut but extract was 410nm and the color of the fabric dyed is Yellow Red. The K/S value of silk and cotton fabrics increased when the dyeing temperature was higher than $60^\circ{C}$ and the dyeing time was more than 30 minutes. Optimal dyeing pH was between 5 and 6, and repetition of dyeing increased K/S value of the sample fabrics. K/S value of silk fabric dyed with chestnut bur extract was higher than that of cotton. Post-mordanting method showed higher color yield compared with pre-mordanting, and higher temperature and increased time in mordanting increased the dye-uptake.

  • PDF

A New Synthetic Route to Poly(benzimidazole) and the Related Model Reactions to Imidazoline and Benzimidazole

  • Shin, G. I.;Kim, Ji Heung
    • Bulletin of the Korean Chemical Society
    • /
    • v.17 no.1
    • /
    • pp.29-33
    • /
    • 1996
  • Mono-, or di-substituted chlorodicyanovinyl benzene compound was reacted with an excess amount of ethylenediamine to give corresponding imidazoline product with high reaction yield. This reaction occurs by stable imidazoline ring-forming process through nucleophilic attack of terminal amine on the enaminonitrile adduct, the reaction intermediate, toward electropositive enamine carbon, which is accompanied by the release of neutral malononitrile moiety. The similar reaction with 1,2-phenylenediamine produced stable enaminonitrile-amine adduct at lower temperature which could be cyclized intramolecularly to thermally stable benzimidazole at elevated temperature in solution or in solid state. From the difunctional compound of both reactants, poly(enaminonitrile-amine) could be prepared as a new soluble precursor polymer for well-known polybenzimidazole (PBI). The thermal cyclization reaction accompanying the release of malononitrile molecules was studied using thermalanalysis and infrared spectroscopy.

Syntrophic Propionate Degradation Response to Temperature Decrease and Microbial Community Shift in an UASB Reactor

  • Ban, Qiaoying;Li, Jianzheng;Zhang, Liguo;Jha, Ajay Kumar;Zhang, Yupeng;Ai, Binling
    • Journal of Microbiology and Biotechnology
    • /
    • v.23 no.3
    • /
    • pp.382-389
    • /
    • 2013
  • Propionate is an important intermediate product during the methane fermentation of organic matter, and its degradation is crucial for maintaining the performance of an anaerobic digester. In order to understand the effect of temperature on propionate degradation, an upflow anaerobic sludge blanket (UASB) reactor with synthetic wastewater containing propionate as a sole carbon source was introduced. Under the hydraulic retention time (HRT) of 10 h and influent propionate of 2,000 mg/l condition, propionate removal was above 94% at 30-$35^{\circ}C$, whereas propionate conversion was inhibited when temperature was suddenly decreased stepwise from $30^{\circ}C$ to $25^{\circ}C$, to $20^{\circ}C$, and then to $18^{\circ}C$. After a long-term operation, the propionate removal at $25^{\circ}C$ resumed to the value at 30- $35^{\circ}C$, whereas that at $20^{\circ}C$ and $18^{\circ}C$ was still lower than the value at $35^{\circ}C$ by 8.1% and 20.7%, respectively. Microbial community composition analysis showed that Syntrophobacter and Pelotomaculum were the major propionate-oxidizing bacteria (POB), and most POB had not changed with temperature decrease in the UASB. However, two POB were enriched at $18^{\circ}C$, indicating they were low temperature tolerant. Methanosaeta and Methanospirillum were the dominant methanogens in this UASB and remained constant during temperature decrease. Although the POB and methanogenic composition hardly changed with temperature decrease, the specific $COD_{Pro}$ removal rate of anaerobic sludge (SCRR) was reduced by 21.4%-46.4% compared with the control ($35^{\circ}C$) in this system.

Synthetic Conditions of an Aspartame Precursorby Immobilized Thermolysin (고정화 Thermolysin을 사용한 아스파탐 전구체의 최적 합성조건 선정)

  • Han, Min-Su;Kim, Woo-Jung
    • Korean Journal of Food Science and Technology
    • /
    • v.27 no.4
    • /
    • pp.564-570
    • /
    • 1995
  • N-Benzoyl-L-aspartyl-L-phenylalanine methyl ester(BzAPM), a novel aspartame precursor, was investigated for its enzymatic synthesis by immobilized thermolysin using a water-miscible organic solvent system. The substrate used were N-benzoyl-L-aspartic acid(BzAsp) and L-phenylalanine methyl ester (PheOMe). Synthetic conditions such as substrates concentration, temperature, pH, and some metallic ions were varied to study their effects on BzAPM synthesis. The synthetic reaction rate increased linearly as the PheOMe concentration increased at a constant concentration of BzAsp(100 mM), and the maximum reaction rate was obtained at BzAsp concentration of 200 mM when 300 mM PheOMe was used. The optimum pH and temperature were found to be 6.1 and $40^{\circ}C$, respectively. The metallic ions such as $Zn^{2+},\;Mg^{2+},\;Mn^{2+},\;Fe^{2+},\;Pb^{2+}\;and\;Cu^{2+}$ at 5 mM level showed inhibitory effect on BzAPM synthesis, while $Co^{2+}$ and $Ca^{2+}$ ion increased synthesis. $Co^{2+}$ ion was also found to have synergistic effect with $Ca^{2+}$ ion. Benzoic acid, L-phenylalanin and NaCl showed inhibitory effect.

  • PDF