• Bulletin of the Korean Chemical Society
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• 제18권7호
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• pp.703-706
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• 1997

Response surface method was applied to the predicting optimum conditions of benzene synthesis for radiocarbon dating. The weight of carbon dioxide, the temperature of lithium container for producing acetylene and the activation temperature of catalyst which was used for the cyclization of acetylene to benzene were used as experimental factors. The yields of benzene synthesis were measured from twelve experiments which were carried out under various experimental conditions. The polynomial equation was obtained by using three experimental factors and yields. The validity of polynomial equation was confirmed by comparing the calculated yields with the experimental ones.

• 핵의학기술
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• 제12권3호
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• pp.176-180
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• 2008

Department of Nuclear Medicine in Seoul National University Hospital (SNUH) had developed $^{18}F$-Flumazenil as Benzodiazepine receptor imaging agent for PET diagnosis of Epilepsy. But production Activity of $^{18}F$-Flumazenil is decreased owing to this method has difficult synthesis procedures and pretty long synthesis time. In this study, we can modify synthesizing method to have more simple procedure and less spend time and help to increase production Activity. Old method: Radioactivity was produced by cyclotron was captured by QMA cartridge that was activated. Captured radioactivity was eluted into the reaction vial by using kryptofix solution and delivered. After evaporation of eluent, the azeotrophic drying step repeated two times. tosylflumazenil in anhydrous Acetonitrile was added to a reaction vial while bubbling. The reaction mixture was evaporated until the mixture volume was 0.5 mL. Reaction vial washed with 20 % Acetonitrile and that solution went into the reaction vial. The reaction mixture was loaded to the HPLC loop by hand and purified $^{18}F$-Flumazenil by HPLC column. New method: We used $TBAHCO_3$ solution as a eluent. After the eluent was evaporated, tosylflumazenil in anhydrous acetonitrile was added to a reaction vial and the reaction mixture was bubbled for 15 minutes. It was evaporated until the mixture volume became 0.5 mL. It was loaded to the HPLC loop. In old method, $^{18}F$-Flumazenil was synthesized via 6 steps synthesis procedures in 105 minutes with 30~35% synthesizing yield (non-decay correction) and specific activity was about $0.5{\sim}2{\times}10^5$ Ci/mole. In new method, It had 3 steps synthesis procedures in 53 minutes with 40~45% synthesizing yield and specific activity was about $3{\sim}8{\times}10^5$ Ci/mole. This method leads to improve of minimizing synthesis time, increasing synthesis yield and specific activity. While we can load reaction mixture to the HPLC loop, we can expose high radiation field thanks to used by hand.

• 소음진동
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• 제3권1호
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• pp.77-82
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• 1993

In general, the dynamic analysis with FEM(Finite Element Method) of large structures requires large computer memory space and long computational time. For the purpose of economical dynamic analysis of large structures, most of engineers want to use an efficient solution algorithm. This paper reports the modified CMS(Component Mode Synthesis) method which uses more efficient algorithm than the classical CMS method. In this paper, it is shown that Ritz vector sets can play the role of normal mode vector sets of substurctures in the CMS algorithm. The modified CMS method has good convergence performance compared with that of the classical CMS method.

• 대한기계학회논문집A
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• 제37권9호
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• pp.1069-1075
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• 2013

무인 국방 로봇의 실시간 해석을 위해서는 효과적인 해석기법이 필수적인 요소이다. 이러한 효과적인 해석을 위하여 부분시스템 합성방법이 개발되었다. 부분시스템 합성방법은 기준 물체의 운동방정식과 각 부분시스템들의 운동방정식을 독립적으로 계산함으로써 계산량의 이득을 볼 수 있다. 운동방정식은 미분방정식과 대수방정식이 혼합된 미분대수방정식으로 표현된다. 이러한 미분대수방정식의 정확하고 효과적인 해석을 위해서 직접 적분방법, 구속조건식 안정화기법, 일반 좌표 분할기법 등이 개발되었다. 본 논문에서는 무인 국방 로봇의 효과적인 해석을 위하여 부분시스템 합성방법을 적용하고 위에서 기술한 세 가지의 미분대수방정식 해석기법을 비교하는 연구를 수행하였다.

• 전자공학회논문지A
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• 제32A권11호
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• pp.94-104
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• 1995

In this paper, we present a new multi-level logic synthesis method for producing the multi-level circuits which can be easily tested by the pseudoexhaustive testing techniques. The method consists of four stages. In the first stage, it generates the minimum variable supports for each output of a multiple-output function. In the second stage, it removes the minimum variable supports which if used to implement the outputs, lead to inefficient pseudoexhaustive test. In the third stage, it determines the minimum variable support and logic (uncomplementary or complementary logic) for each output. In the fourth stage, it performs the multi-level logic synthesis so that each output. In the fourth stage, it performs the multi-level logic synthesis so that each output has the minimum variable support and logic determined in the third stage. To evaluate the performance and quality of the proposed method, we have experimented on the 56 benchmark examples. The results show that for 56 examples, our method obtains better results than MIS in terms of testability. Moreover, the method produces better results for 19 examples and the same results for 12 examples compared with MIS in terms of literal count although it has been developed to improve the testability.

• 전기전자학회논문지
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• 제3권1호
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• pp.150-160
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• 1999

본 논문에서는 기존의 레지스터 전송 단계 합성기들이 가지고 있는 단점을 개선하는 새로운 레지스터 전송 단계 합성 방법을 제안한다. 기존의 레지스터 전송 단계 합성기들은, 하드웨어 기술 언어로 기술된 설계 사양을 순서회로로 변환하는 과정에서 불합리한 변환을 수행하고 순서 회로를 최적화 하는 과정에서 순서회로를 구성하는 레지스터와 조합회로를 분리하여 조합회로부만을 최적화 한다. 본 논문에서는 이러한 방식의 레지스터 전송 단계 합성기들이 가지는 단점을 지적하고, 이런 단점을 극복하기 위한 새로운 레지스터 전송 단계 합성 방법을 제안한다. 또한, 제안된 방법을 감시용 시스템의 콘트롤러 설계 및 8 비트 부호화 곱셈기에 적용한 결과를 제시함으로써 본 논문에서 제안하는 방법의 유용성을 입증한다.

• 한국재료학회지
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• 제30권2호
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• pp.93-98
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• 2020

Effective control of the heat generated from electronics and semiconductor devices requires a high thermal conductivity and a low thermal expansion coefficient appropriate for devices or modules. A method of reducing the thermal expansion coefficient of Cu has been suggested wherein a ceramic filler having a low thermal expansion coefficient is applied to Cu, which has high thermal conductivity. In this study, using pressureless sintering rather than costly pressure sintering, a polymer solution synthesis method was used to make nano-sized Cu powder for application to Cu matrix with an AlN filler. Due to the low sinterability, the sintered Cu prepared from commercial Cu powder included large pores inside the sintered bodies. A sintered Cu body with Zn, as a liquid phase sintering agent, was prepared by the polymer solution synthesis method for exclusion of pores, which affect thermal conductivity and thermal expansion. The pressureless sintered Cu bodies including Zn showed higher thermal conductivity (180 W/m·K) and lower thermal expansion coefficient (15.8×10^-6/℃) than did the monolithic synthesized Cu sintered body.

• Advances in nano research
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• 제14권1호
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• pp.103-115
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• 2023

Recent developments in the synthesis of nanomagnesia of controlled sizes and shapes that are suitable for various applications are reviewed. Two main methods, based on liquid-phase synthesis, i.e., chemical methods and bio-based methods, are used to synthesize nanomagnesia. Conventionally, nanomagnesia was synthesized by chemical methods such as coprecipitation, sol-gel, combustion method, and so on using different chemical agents and stabilizers which later on become responsible for several biological risks because of the toxicity of used chemicals. Bio-based protocols are growing as another environmental friend method for the synthesis of various nanostructures especially nanomagnesia using biomass, plant extracts, alga, and fungi as a source of precursor material. The ideal method should offer better control of textural properties of nanostructures and decrease the necessity for purification of the synthesized nanoproducts, which sequentially removes the use of large amounts of chemicals and organic solvents and manipulation of products that are unsafe to the environment. Finally, the broad applicability of nanomagnesia in diverse areas is presented. Employment of nanomagnesia reported in several laboratory and industrial fields are valued from the standpoint of the significance of these issues for technological requests, as described in the literature. Nanomagnesia has various applications such as antimicrobial performance, removing pollutants, batteries application, and catalysis.

• ETRI Journal
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• 제44권1호
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• pp.85-93
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• 2022

We propose an efficient method for synthesizing mesh-based realistic computer-generated hologram (CGH). In a previous nonanalytic mesh-based CGH synthesis, the angular spectrum of the two-dimensional (2D) plane is calculated using the fast Fourier transform (FFT) with the same size as the resolution of the final hologram. Because FFT increases the computation time as the size of the input matrix increases, the previous method has a problem: The higher the resolution of the hologram, the greater the computational load, thereby delaying synthesis time. In this study, when calculating the angular spectrum of the 2D plane in mesh-based CGH synthesis, we propose a method to calculate the angular spectrum by defining the 2D plane with an arbitrary size smaller than the resolution of the final hologram. The resolution adjustment method reduces the computation time and can be applied to occlusion culling and texturing for the realistic effect of mesh-based CGH. We describe the principle, error analysis, application of realistic effect, and experimental results of the proposed method.

• 한국산학기술학회논문지
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• 제7권6호
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• pp.1175-1179
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• 2006

유성음원과 무성음원을 사용하는 음성부호화 방식에 있어서, 프레임 안에 모음과 무성자음이 있는 경우에 음성 파형에 일그러짐이 나타난다. 본 논문에서는 LMS를 적용한 새로운 TSIUVC 근사합성법을 제시하였다. 실험결과, LMS를 적용하여 양호한 TSRIVC 근사합성 파형을 얻을 수 있었으며, 오차신호가 일그러짐이 적은 근사합성 파형에 중요한 역할을 한다는 것을 알 수 있었다. 이 방법은 음성합성, 음성분석, 새로운 Voiced/Silence/TSIUVC의 음성부호화 방식에 활용할 수 있을 것으로 기대된다.