• Title/Summary/Keyword: swelling method

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The retrogradation and swelling power of modified potato starches (변성 감자 전분의 노화와 팽윤력)

  • Kim, Ji-Tae;Noh, Wan-Seob
    • Applied Biological Chemistry
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    • v.35 no.5
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    • pp.404-409
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    • 1992
  • Hydroxypropylated starches and acetylated starches were prepared by reaction of potato starch with propylene oxide and acetic anhydride, respectively and then degree of retrogradation and swelling power were investigated in different pHs and temperature. The extent of retrogradation determined by glucoamylase method during freeze-thaw treatment and storage in low temperature $(0{\sim}5^{\circ}C)$ showed that modified potato starches were slowly retrograded as the increase of degree of substitution. The order of the retrogradation tendencies in different pHs were pH 4>pH 6>pH 8>pH 10. Retrogradation of hydroxypropylated potato starches were less than that of acetylated potato starches. Swelling power of starches were influenced more by the temperature than by the pH. The order of the swelling power tendencies in different pHs were pH 10>pH 2>pH 8>pH 4>pH 6.

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Synthesis and characterizations of the non-swelling property micas by hydrothermal method (비팽윤성 운모의 수열합성 및 특성평가)

  • Park, Chun-Won;Park, Sun-Min;Kambayashi, Akira
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.16 no.3
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    • pp.95-100
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    • 2006
  • Synthesis of the non-swelling property micas was carried out by hydrothermal method. In order to artificially induce the diffusion of ions, a rotating system was attached to the hydrothermal apparatus and by adding 0.7 mm zircon beads, synthesis of the non-swelling property micas could be performed in a low temperature area. The hydrothermal conditions for the preparation of micas were a reaction temperature of $260^{\circ}C$, for 72 hrs, using $1K_2O,\;1Al(OH)_3,\;4Mg(OH)_2\;and\;6SiO_2$ as the starting materials and a 8M-KOH solution as the hydrothermal solvent. The micas obtained under these conditions were a plate shape with a size of $2.89{\mu}m$ and showed a whiteness of over 97 %. Also, through the FT-IR analysis, because the absorption peak of the $Mg_3OH$ vibration was observed at approximately $3700cm^{-1}$, it could be known that it was phlogopite of non-swelling property showing the chemical composition of $KMg_3AlSi_3O_{10}(OH)_2$. This result was very consistent with the EDS analysis where O (41.34 %), Mg (3.88 %), Al (11.45 %), Si (17.62 %) and K (25.71%) elements were detected.

추출조건 및 방법에 따른 인삼내의 panaxydol과 panaxynol의 추출율 비교

  • Park, Chan-Ell;Yun, Ji-Yong;Park, Chang-Ho
    • 한국생물공학회:학술대회논문집
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    • 2000.04a
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    • pp.493-496
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    • 2000
  • The extraction efficiencies of panaxynol and panaxydol according to extraction temperature were the highest at $80^{cdot}C$ among 65, 80, $95^{cdot}C$ with soxhlet and increased with shaking method when temperature increased from $25^{cdot}C$ to $45^{cdot}C$. The amounts of panaxynol and panaxydol were determined by gas chromatography. In time dependence of extracted amounts of panaxynol and panaxydol using shaking method, the efficiencies of panaxynol and panaxydol were increased during 12 hour. The effect of water swelling on panaxynol and panaxydol extraction efficiency using soxhlet and shaking methods, the efficiencies of panaxynol and panaxydol were decreased as swelling time was increased.

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The Comparative Study of Quality by Processing Methods of Liriope platyphylla (한국산(韓國産) 맥문동(麥門冬)의 포제방법(炮製方法)에 따른 품질(品質) 비교(比較) 연구(硏究))

  • Cho, Eun-Hwan;Roh, Seong-Soo;Seo, Young-Bae;Jeong, Gi-Hoon
    • The Korea Journal of Herbology
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    • v.25 no.4
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    • pp.95-102
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    • 2010
  • Objectives : Specifications by Processing Methods of Liriope platyphylla (LP) was not established in korea. We carried out method study for manufacture of LP. Above all, LP were purchased and were processed at four kinds. First group had hearts of swelling roots, not cut bodies(LP-A). Second group had not hearts of swelling roots, not cut bodies(LP-B). Third group had hearts of swelling roots, cut bodies(LP-C). Forth group had an aggregate of hearts of swelling roots(LP-D). Methods : We has gained losses on drying, contents of ethanol-soluble extracts, contents of water-soluble extracts and contents of spicatoside A. Results : 1. Losses on drying of all group were less than 18% that is a standard of chinese pharmacopoeia. 2. Contents of ethanol-soluble extracts at LP-C, LP-D were included more than contents of those in the other groups in significance levels. 3. Contents of water-soluble extracts at LP-A, LP-C were included more than contents of those in the other groups in significance levels. 4. Contents of spicatoside A in LP-B were included more than content of spicatoside A in the other groups in significance levels. Resultingly, standards of LP in korea were proposed compatible proposals suggested as below. 1. Losses on drying of LP were less than 15% that is less than that of chinese pharmacopoeia. 2. Form to boil in water must be cutting body with heart of swelling root. 3. Because there is no content of spicatoside A in heart of swelling root, it is not suited to purpose a index component. Conclusions : The subjects of loss on drying and form of LP to boil in water must be contained in korean pharmacopoeia. Moreover, because of much valuable LP in food and medicine, it is urgently required aspect of index component such as spicatoside B, spicatoside C, flavonoid, polysaccharide having medical actions and so on.

Effects of steam heat treatment conditions on the swelling and physical properties of PBS (polybutylene succinate) copolymer monofilament gill net (습식 열처리 조건이 PBS 공중합체 모노필라멘트 그물감의 부풀음 및 물성변화에 미치는 영향)

  • Park, Seongwook;Kim, Seonghun;Do, Choonho;Lim, Jihyun;Choi, Haesun
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.50 no.3
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    • pp.274-283
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    • 2014
  • Swelling of the heat-treated netting for gillnet was estimated through the netting height in square acrylic tank. Experimental Nylon netting and PBSAT netting were heat-treated by using the high-degree vacuum method in hot water after net making. Heat-treatment temperatures were conducted with Nylon netting $105^{\circ}C$ and PBSAT netting $62^{\circ}C$, $65^{\circ}C$, $66^{\circ}C$, $67^{\circ}C$. The swelling measurement method of a netting using the square tank was capable of the reduction measurement errors comparing with measurement methods of a mesh inner angle and the shortening rate of a mesh size. In addition, this method was available to comparison evaluation for each netting more easily. Wet type heat-treatment apparatus with high-degree vacuum was shown higher $7{\sim}8^{\circ}C$ inner side temperature than a setting temperature. The tensile strength and elongation of Nylon netting and PBSAT netting were shown higher wet condition than dry condition. The tensile strengths of PBSAT monofilaments in dry and wet condition were sharply decreased at heat-treatment temp. $75^{\circ}C$ than heat-treatment temp. $74^{\circ}C$.

Allergy Prevention Effect of Oral Administration of Quercetin on Picryl Chloride-induced Contact Dermatitis in BALB/c Mice (BALB/c mice에서 quercetin의 경구투여가 picryl chloride로 유발된 접촉성 피부 알레르기의 예방에 미치는 영향)

  • Kim, Hyeong-Jin;Jung, Ji-Youn
    • Journal of Life Science
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    • v.19 no.10
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    • pp.1444-1450
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    • 2009
  • The number of patients with immune- mediated dermatitis such as contact dermatitis is increasing year by year. Allergic contact dermatitis is a complex phenomenon that involves resident epidermal cells, fibroblasts, and endothelial cells, as well as invading leukocytes that interact with each other under the control of a network of cytokines and lipid mediators. It is a cell-mediated immune reaction, which occurs after susceptible individuals are exposed to sensitizing chemicals, and characteristic eczematous reaction is seen at the point of contact with an allergen. In this study, we investigated the allergy prevention effects of quercetin on mast cell-mediated allergic inflammation in BALB/c mice. BALB/c mice were sensitized with 40 ${\mu}l$ of 1.5% picryl choloride (PCL) to the left and right ear each. Total serum IgE levels and histamine levels were measured by the sandwich ELISA method using mouse IgE, histamine measuring kit. For histopathological examination, paraffin sections were stained with hematoxylin and eosin(HE) or toluidine blue(TB). Ear swelling responses were much weaker in the high-dose group (100 mg/kg) than the control group (0 mg/kg). The number of mast cells showed a significant decrease in the high-dose group (100 mg/kg) compared to the control group (0 mg/kg). Degranulation of mast cells was also confirmed by Toluidine Blue (TB) staining method. Both total serum IgE and histamine levels were significantly decreased in the high-dose group (100 mg/kg) compared to other groups. These findings suggest a certain relationship between the elevation of IgE, histamine levels and the degranulation of mast cells. These results show that the pharmacological actions of quercetin indicate its potential activity for prevention of allergic inflammatory diseases through the down-regulation of mast cell activation.

Electro-responsive Transdermal Drug Release of MWCNT/PVA Nanocomposite Hydrogels

  • Kim, Yeon-Yi;Yun, Ju-Mi;Lee, Young-Seak;Kim, Hyung-Il
    • Carbon letters
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    • v.11 no.3
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    • pp.211-215
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    • 2010
  • Multi-walled carbon nanotube (MWCNT)/poly(vinyl alcohol) (PVA) nanocomposite hydrogels were prepared by freezingthawing method for the electro-responsive transdermal drug delivery. MWCNTs were used as the functional ingredient to improve both mechanical and electrical properties of MWCNT/PVA nanocomposite hydrogels. The morphology of nanocomposites revealed the uniform distribution of MWCNTs and the good interfacial contact. The compression moduli of hydrogel matrices increased greatly from 40 to 1500 kPa by forming MWCNT/PVA nanocomposites. The swelling ratio of MWCNT/PVA nanocomposites decreased as the content of MWCNTs increased under no electric voltage applied. However, the swelling ratio of MWCNT/PVA nanocomposites increased as the content of MWCNTs increased under electric voltage applied and the applied electric voltage increased. The drug was released in the electro-responsive manner through the skin due to the electro-sensitive swelling characteristics of MWCNT/PVA nanocomposite hydrogels.

Leachability of Zinc Borate-Modified Oriented Strandboard (OSB)

  • Lee, Sun-Young;Wu, Qinglin
    • Journal of the Korean Wood Science and Technology
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    • v.35 no.5
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    • pp.46-57
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    • 2007
  • The leachability of boron in zinc borate (ZB)-modified oriented strandboard (OSB) from southern wood species was investigated in this study. The leaching experiments were conducted by exposing edge-sealed OSB samples under running water at $31^{\circ}C$ for 8, 24, 72, and 216 h. The results from leached samples were compared with those from the unleached controls. Boron leaching of the modified OSB occurred upon the initial water exposure, and the leaching rate decreased as the leaching time increased. Initial boric acid equivalent (BAE) level, wood species, and sample thickness swelling significantly influenced the leachability. There was no consistent effect of polyethylene glycol (PEG) on zinc borate leaching. The glue-line washing within OSB due to thickness swelling of the test samples under water and decomposition of the borate to form water-soluble boric acid were thought to be two possible causes for the observed leaching. The relationship between assayed BAE and leaching time followed a decaying exponential function for zinc borate treated OSB. From the boron/zinc ratio after each leaching period, boron element in ZB was more or less leachable. The material constant of the regression models allowed comparing the leachability of the modified OSB for various wood species. An unified leaching method for treated wood composite materials is needed.

Rheological Studies on the Aqueous Suspension of Korean Bentonite (국산벤토나이트 현탁액의 유동학적 성질)

  • Kim, Eun-Hee;Rhee, Gye-Ju
    • YAKHAK HOEJI
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    • v.34 no.5
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    • pp.302-310
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    • 1990
  • A study has been made of the Korean bentonite aqueous suspension contrast with American bentonite by means of XRD IR swelling, gel formation and rheogram at various conditions such as concentration, temperature and pH. The Korean bentonite was identified as montmorillonite clay containig a small proprotion of crystoballite and mordenite, and its swelling power were acceptable for requirements of Korean pharmacopeia regulations though its values were not satisfied. Korean bentonite swelled to 10 times and American one did to 15 times compared to its bulkiness of powder. The rheogram of Korean bentonite suspension reveals bulged pseudoplatic flow with yield value at higher concentration and pseudoplastic flow without yield value at lower concentration. The higher the concentration, the greater were the apparent viscosity and hysteresis loop. Korean bentonite suspension showed insignificant temperature dependence on both apparent viscosity and hysteresis loop and it was more temperature dependent on viscosity but less on hysteresis loop than those of American sample. The pH dependence was so high on viscosity that apparent minimum value was near pH 7 and maximum value at pH 3 or 7. The hysteresis loop appeared minimum over the pH range 5-7 and maximum near pH 3 or 11. The Korean bentonite was inferior to the American bentonite in swelling volume, gel formation, thioxotropy, however, it would be possible to improve the quality of Korean bentonite by developing the method of purification for bentonite clay.

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Treatment of Patients With Elephantiasis Lymphedema - Case Report - (상피성 임파부종 환자의 치료 -증례보고-)

  • Kim, Seng-Jung
    • Physical Therapy Korea
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    • v.6 no.3
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    • pp.110-120
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    • 1999
  • Lymphedema, regardless of etiology, is essentially incurable but different treatment approaches which serve to contain swelling exist. The objectives of treatment are to reduce swelling, restore shape, educate about the self-maintenance methods, and prevent inflammatory episodes, eg, recurrent cellulitis. The purpose of this report is to provide therapists and other medical staff with a general guideline through the example treatment procedure of two patients with lymphedema admitted to Samsung Medical Center. This study demonstrates the effects of the various treatments used and how they helped to achieve improvement in mobility and reduction in swelling of the lower limbs. The basic conservative treatments were sequential intermittent pneumatic pumps, elevation, and CDP (complex decongestive physiotherapy). The surgical procedures (Homan's operation) were carried out after maximal volume reduction through conservative programs. In these cases, we can see greater than 50% reduction in the lymphedema in those treated by conservative and surgical procedures. This presents a simple, reliable, variable method yielding satisfactory cosmetic and functional results for patients suffering from chronic both-leg lymphedema. Futhermore, I suggest that the outcomes are best when treatment is administered by a multidisciplinary team including a physiotherapist, surgeon, nurse, et al.

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