• Title/Summary/Keyword: surface-modification technology

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Variation of Axial Tension-Compression Fatigue Characteristics by UNSM on Ti-6Al-4V (Ti-6Al-4V재의 UNSM처리에 의한 축인장압축피로특성변화)

  • Suh, Chang-Min;Cho, Sung-Am;Pyoun, Young-Sik;Suh, Min-Soo
    • Journal of Ocean Engineering and Technology
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    • v.25 no.6
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    • pp.42-48
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    • 2011
  • The present study makes three original contributions to nanoskinned Ti-6Al-4V materials. The nanoskins were fabricated on Ti-6Al-4V material using various surface treatments: deep rolling (DR), laser shot peening (LSP), and ultrasonic nanocrystal surface modification (UNSM). These surface treatments are newly developed techniques and are becoming more popular in industrial fields. A fatigue strength comparison at up to 106 cycles was conducted on these nanoskinned Ti-6Al-4V materials. Fatigue tests were carried out using MTS under axial loading tension-compression fatigue (R = -1, RT, 5 Hz, sinusoidal wave). The analysis of the crack initiation patterns in the nanoskinned Ti-6Al-4V materials found an interior originating crack pattern and surface originating crack type. Microscopic observation was mainly used to investigate the fatigue fractured sites. These surface modification techniques have been widely adopted, primarily because of the robust grade of their mechanical properties. These are mainly the result of the formation of a large-scale, deep, and useful compressive residual stress, the formation of nanocrystals by the severe plastic deformation (SPD) at the subsurface layer, and the increase in surface hardness.

Surface Modification of Iron Oxide Particle by Silica-contained Materials (실리카계 물질에 의한 산화철 입자의 표면개질)

  • Ryu, Beyong-Hwan;Lee, Jung-Min;Koh, Jae-Cheon
    • Applied Chemistry for Engineering
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    • v.8 no.5
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    • pp.830-836
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    • 1997
  • The surface modification of iron oxide particle produced from steel-pickled acid by sodium-contained materials was studied. The molar ratio of $SiO_2$ to $Na_2O$ of sodium silicate was 1, 2, 3.5, respectively. The dispersion stability of iron oxide suspension as functions of amount of silica and pH was evaluated by surface charge and sedimentation velocity of iron oxide particle. Then the amount of sodium silicate was determined to provide a dispersion stability of iron oxide particle above pH 7. Finally, the surface modification of iron oxide particle with sodium silicate as silica-contained materials was done by wet ball milling. In the results of study, the dispersion stability of silica modified iron oxide particle was largely depended on amount of silica and pH together. The untreated iron oxide was unstable at pH 8, i.e. isoelectric point, but, the surface modified iron oxide particle with 0.8wt% silica was stable above pH 5. The dispersion stability was enhanced with 0.2wt% of anionic polyelectrolyte.

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Investigation of Co-poly-para-aramid Fiber Dispersion in Chloroprene Rubber Matrix and Improvement of Dispersibility Through Fiber Surface Modification

  • Garam Park;Hyeri Kim;Gayeon Jeong;Dohyeong Kim;Seungchan Noh;Dajeong Gwon;Myung Chan Choi;Jaseung Koo
    • Elastomers and Composites
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    • v.57 no.4
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    • pp.175-180
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    • 2022
  • To produce a co-poly-para-aramid fiber (AF, Technora®)-reinforced neoprene rubber composite, dispersion of AF in a neoprene matrix is investigated. The AF is then surface-modified by mercerization and acetone, plasma, and silane treatments to improve dispersibility. Finally, an internal mixer process is used to disperse the surface-modified fibers in the neoprene rubber matrix.

Effects of Atmospheric Pressure Microwave Plasma on Surface of SUS304 Stainless Steel

  • Shin, H.K.;Kwon, H.C.;Kang, S.K.;Kim, H.Y.;Lee, J.K.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.268-268
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    • 2012
  • Atmospheric pressure microwave induced plasmas are used to excite and ionize chemical species for elemental analysis, for plasma reforming, and for plasma surface treatment. Microwave plasma differs significantly from other plasmas and has several interesting properties. For example, the electron density is higher in microwave plasma than in radio-frequency (RF) or direct current (DC) plasma. Several types of radical species with high density are generated under high electron density, so the reactivity of microwave plasma is expected to be very high [1]. Therefore, useful applications of atmospheric pressure microwave plasmas are expected. The surface characteristics of SUS304 stainless steel are investigated before and after surface modification by microwave plasma under atmospheric pressure conditions. The plasma device was operated by power sources with microwave frequency. We used a device based on a coaxial transmission line resonator (CTLR). The atmospheric pressure plasma jet (APPJ) in the case of microwave frequency (880 MHz) used Ar as plasma gas [2]. Typical microwave Pw was 3-10 W. To determine the optimal processing conditions, the surface treatment experiments were performed using various values of Pw (3-10 W), treatment time (5-120 s), and ratios of mixture gas (hydrogen peroxide). Torch-to-sample distance was fixed at the plasma edge point. Plasma treatment of a stainless steel plate significantly affected the wettability, contact angle (CA), and free energy (mJ/$m^2$) of the SUS304 surface. CA and ${\gamma}$ were analyzed. The optimal surface modification parameters to modify were a power of 10 W, a treatment time of 45 s, and a hydrogen peroxide content of 0.6 wt% [3]. Under these processing conditions, a CA of just $9.8^{\circ}$ was obtained. As CA decreased, wettability increased; i.e. the surface changed from hydrophobic to hydrophilic. From these results, 10 W power and 45 s treatment time are the best values to minimize CA and maximize ${\gamma}$.

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Rapid Surface Modification via Mussel-Inspired Polymer Coating

  • Hong, Sang-Hyeon;Gang, Seong-Min;Lee, Hae-Sin
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.11a
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    • pp.88-88
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    • 2012
  • 도파민은 홍합 모방물질로 표면개질 가능한 표면의 다양성과 편리한 개질 방법으로 인해 여러 분야에서 각광받고 있다. 본 연구에서는 이러한 도파민 표면개질 방법을 최적화 시켜 수분 안에 기존의 특성에 변화를 주지 않고 표면개질이 가능 하도록 개선시켰다.

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Polymer surface modification by plasma reaction

  • Park, Jang-Sick;Kim, Tae-Woo;Kim, Eun-Ju;Lee, Young-Kil;Jeong, Won-Sang;Park, Sang-Won;Kim, Sung-Kuk;Ahn, Won-Sool
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2003.10a
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    • pp.40-41
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    • 2003
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Pervaporation Separation of Water-isopropanol Mixtures through Modified Asymmetric Polyetherimide Membrane: the Effect of NaOH Concentration and Modification Reaction Times on the Morphology of the Morphology of the Modified Membranes (개질 비대칭 폴리에테르이미드막을 통한 물-이소프로판올 혼합물 투과증발 분리: NaOH용액의 농도와 개질반응 시간에 따른 몰폴로지 변화)

  • Kim, Sang-Gyun;Jegal, Jonggeon;Lee, Kew-Ho
    • Applied Chemistry for Engineering
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    • v.10 no.4
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    • pp.515-522
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    • 1999
  • Asymmetric polyetherimide membrane were prepared by phase inversion method, and the effects of NaOH concentration and reaction time on the morphology change of the polyetherimide membranes were studied. The morphology of skin layers varied from dense structure to sphere structure with increasing concentration of modification solution. The thickness of dense layer increased with increasing reaction time. However, when either the concentration of modifying solution was very high or the reaction time was very long, the dense layers of the asymmetric membrane were disappeared. From these results, it was found that the surface morphology of the asymmetric polyetherimide membranes depended strongly on the modification conditions such as concentration of modification solution and reaction time. These results might be explained by the hydrolysis reaction of polyetherimide into polyamic acid by the NaOH solution.

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