• 한국레이저가공학회지
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• 제18권2호
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• pp.1-4
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• 2015

This study is related to the surface hardening treatment to spheroidal graphite cast iron for die by using high power diode laser. Laser device used in this experiment is capable of real-time laser power control. This is because the infrared temperature sensor (two color pyrometer) attached to the optical system measures the surface temperature of specimen and adjusts the laser power in real time. The surface treatment was carried out with the change of heat treatment temperature at the beam travel speed 3 mm/sec. Hardened width and depth was measured and hardened zone was analyzed by micro vickers hardness test in order to research the optimum condition of heat treatment. The changes in microstructure of the hardened zone also was examined. As a result of hardness measurement and observations on microstructure of hardened zone, hardness increased over three times as compared with base metal because the martensite was formed on the matrix structure.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2002년도 추계학술대회 논문집 전기물성,응용부문
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• pp.176-178
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• 2002

Surface states of silicone polymer treated by plasma were investigated by the analysis by x-ray photoelectron spectroscopy(XPS) and surface voltage decay after corona charging. Plasma treatment causes the silica -like oxidative layer, which was confirmed with XPS, and lowers surface resistivity with increasing the plasma treatment time. Using the decay time constant of surface voltage, the calculated surface resistivity was compared with the value directly measured by voltage-current method using three electrodes system. A good agreement between two methods was obtained. In addition, we estimated the thermal activation energy for surface conduction, Based on our results, we could understand the relationship between surface chemical states and surface electrical properties.

• 열처리공학회지
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• 제36권2호
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• pp.86-95
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• 2023

This paper explained the equipment and process development to secure the source technology of controlled nitrification technology. The nitriding potential in the furnace was controlled only by adjusting the flow rate of ammonia gas introduced into the furnace. In addition, a control system was introduced to automate the nitriding process. The equipment's hardware was designed to enable controlled nitriding based on the conventional gas nitriding furnace, and an automation device was attached. As a result of measuring the temperature and quality uniformity for the equipment, the temperature and compound uniformity were ±1.2℃ and 14.3 ± 0.2 ㎛, respectively. And, it was confirmed that nitriding potential was controlled within the tolerance range of AMS2759-10B standard. In addition to parts for controlled nitriding, it was applied to products produced in existing conventional nitriding furnaces, and as a result, gas consumption was reduced by up to 80%.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2001년도 가을 학술발표회 논문집
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• pp.1225-1228
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• 2001

The purpose of this study is to develop for finishing method of concrete structures applying metal spraying system. In the experiments, the pull out tests were conducted using the specimen which was applied by various surface treatment of concrete substrate. As a result, it was confirmed that the adhesion strength of metal spray was effected by surface condition of concrete and the construction of primer or the coarse surface agent to the concrete substrate is very effective to the new finishing method of concrete for the metal spraying system.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2010년도 제39회 하계학술대회 초록집
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• pp.96-96
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• 2010

To improve surface wettability, each sample was treated by atmospheric pressure plasma (APP) using dielectric barrier discharge (DBD) system. Argon and oxygen gases were used for treatment gas to modify the $TiO_2$ surface by APP with RF power range from 50 to 200 W. Water contact angle was decreased from $20^{\circ}$ to $10^{\circ}$ with argon only. However, water contact angle was decreased from $20^{\circ}$ to < $1^{\circ}$ with mixture of argon and oxygen. Water contact angle with $O_2$ plasma was lower than water contact angle with Ar plasma at the same RF power. It seems to be increasing the polar force of $TiO_2$ surface. Also, analysis result of X-ray photoelectron spectra (XPS) shows the increase of intensity of O1s shoulder peak, resulting in increasing of surface wettability by APP. Moreover, each water contact angle increased according to increase past time. However, contact angle increase with plasma treatment was lower than without plasma treatment. Additionally, the efficiency of $TiO_2$ photocatalyst was improved by plasma surface-treatment through the degradation experiment of phenol

• 대한치과기공학회지
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• 제44권4호
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• pp.111-117
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• 2022

Purpose: This study was conducted to compare the Vickers hardness on the denture acrylic resins using the glaze color system. Methods: The specimens (20×2 mm) were prepared by mixing according to the manufacturer's protocols through thermal polymerization and self-polymerization. The surface roughness was measured using a testing machine after water-soaking for 48 hours. For the Vickers hardness measurement, the completed specimen was soaked in water for 48 hours and then applied at 200 gf for 30 seconds. Was the specimen immersed after being soaked in water for 48 hours at temperatures of 5℃ and 55℃, respectively, for 30 seconds for the thermos-cycling treatment, and it was carried out 5,000 times. Results: Surface roughness was higher in the more glazing group than in the control group. A significant difference was observed in all groups, except for the Retec Don 2000 and Luciton 199 groups (p<0.05). As a result of measuring the Vickers hardness, the treatment by glaze color showed slightly lower but the thermo-cycling treatment group appeared higher than control group in all. Conclusion: Therefore, the glaze color was found to affect the surface roughness and showed a significant difference. The surface glaze color showed a very high Vickers hardness after the thermo-cycling treatment, indicating that the surface-strengthening effect is greater in the oral environment.

• Elastomers and Composites
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• 제34권3호
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• pp.222-228
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• 1999

본 연구에서는, 화학적 표면처리에 따른 카본블랙의 표면, 흡착, 그리고 미세구조의 성질과 물리적 표면 자유에너지를 고찰하였다. 실험적 결과를 통하여, 염기성 용액으로 표면 처리한 경우 pH와 비표면적의 변화 없이 표면 자유에너지의 비극성 또는 극성요소의 증가를 가져왔다. 반면에 산성표면처리의 경우에는 표면특성, 흡착성질과 미세구조의 큰 변화를 확인하였다. 특히, 염기성 처리된 카본블랙은 비극성이나 비표면적의 중요한 인자로 표면 자유에너지의 London 비극성 요소의 증가를 볼 수 있었다. 이는 카본블랙/고무 복합재료에 있어서, 카본블랙이 강화재의 역할 뿐 아니라 분산력 발달에 중요한 역할을 담당하고 있기 때문으로 사료된다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제40회 동계학술대회 초록집
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• pp.449-449
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• 2011

We reported the direct effect of intrinsic surface energy of dry adhesive material to the Van der Waals and capillary forces contributions of the total adhesion force in an artificial gecko-inspired adhesion system. To mimic the gecko foot we fabricated tilted nanohairy structures using both lithography and ion beam treatment. The nanohairy structures were replicated from Si wafer mold using UV curable polymeric materials. The control of nanohairs slanting angles was based on the uniform linear argon ion irradiation to the nanohairy polymeric surface. The surface energy was studied utilizing subsequent conventional oxygen ion treatment on the nanohairy structures which resulted in gradient surface energy. Our shear adhesion test results were found in good agreement with the accepted Van der Waals and capillary forces theory in the gecko adhesion system. Surface energy would give a direct impact to the effective Hamaker constant in Van der Waals force and the filling angle (${\varphi}$) of water meniscus in capillary force contributions of gecko inspired adhesion system. With the increasing surface energy, the effective Hamaker constant also increased but the filling angle decreased, resulting in a competition between the two forces. Using a simple mathematical model, we compared our experimental results to show the quantitative contributions of Van der Waals and capillary forces in a single adhesion system on both hydrophobic and hydrophilic surfaces. We found that the Van der Waals force contributes about 82.75% and 89.97% to the total adhesion force on hydrophilic and hydrophobic test surfaces, respectively, while the remaining contribution was occupied by capillary force. We also showed that it is possible to design ultrahigh dry adhesive with adhesion strength of more than 10 times higher than apparent gecko adhesion force by controlling the surface energy and the slanting angle induced-contact line of dry adhesive the materials.

• 한국기계가공학회지
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• 제20권3호
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• pp.100-106
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• 2021

Typical implants are not specified the screw structure and the surface process according to the bone quality of the human body. The purpose of this study is to complement the shortcomings of the existing implant surface processing method. It is to propose a surface processing method that increases the adhesion between the implant and bone tissue by increasing the surface area per unit area of the implant. It is very important to establish precise and systematic process parameters when surface treatment of implants using lasers. Therefore, we intend to develop a process so that the implant can be a biocompatible structure using a Q-switching Nd:YAG laser with a wavelength of 1.06um. Implant surface treatment technology through this study will be used in the industry.

• Elastomers and Composites
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• 제33권1호
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• pp.27-36
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• 1998

The surface of wiper blade(W/B) rubber was chlorinated by chemical treatment method using the hydrochloric acid(HCI) and sodium hypochlorite(NaOCl). From the results of contact angle measurement, friction coefficient measurement, and ATR-IR spectra, the surface characteristics of chlorinated W/B rubber with time of chlorination were studied. Contact angles for W/B rubber with increasing time of chlorination and chlorine concentration were measured for the water and ethylene glycol. From the results, contact angle fell rapidly with increasing time of chlorination and chlorine concentration, reaching a constant value after about 10min. And the wettability of W/B rubber surface by means of chlorination has been improved. For an unchlorinated W/B rubber, the friction coefficient with time of chlorination decreased from 1.27 to 0.20~0.23 on full chlorination. As the results it was considered that abrasion resistance of W/B rubber surface has been also improved. The values of pH and $Cl^-$ ion concentration in a chlorine treatment solution decreased as the extent of chlorination of W/B rubber surface increased. From the results of ATR-IR spectra, it was observed that C=C double band of W/B rubber surface transformed into C-Cl band, but quantitative determination of the extent of chlorination was not feasible because of the complexity of chlorination reactions.