• Title/Summary/Keyword: surface properties

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Preparation and Characterization of IZO Thin Films grown by DC Magnetron Sputtering (DC 마그네트론 스퍼터링을 이용한 IZO 박막의 제조와 특성 연구)

  • Park Chang-Ha;Lee Hak-Jun;Kim Hyeon-Boum;Kim Dong-Ho;Lee Gun-Hwan
    • Journal of the Korean institute of surface engineering
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    • v.38 no.5
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    • pp.188-192
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    • 2005
  • Indium zinc oxide (IZO) thin films were deposited on glass substrate by dc magnetron sputtering. The effects of oxygen flow rate and deposition temperature on electrical and optical properties of the films were investigated. With addition of small amount of oxygen gas, the characteristic properties of amorphous IZO films were improved and the specific resistivity was about $4.8{\times}10^{-4}\Omega{\cdot}cm$. Change of structural properties according to the deposition temperature was observed with XRD, SEM, and AFM. Films deposited above $300^{\circ}C$ were found to be polycrystalline. Surface roughness of the films was increased due to the formation of grains on the surface. Electrical conductivity became deteriorated for polycrystalline IZO films. Consequently, high quality IZO films could be prepared by do sputtering with $O_{2}/Ar{\simeq}0.03$ and deposition temperature in range of $150\~200^{\circ}C$; a specific resistivity of $3.4{\times}10^{-4}{\Omega}{\cdot}cm$, an optical transmission over $90\%$ at wavelength of 550 nm, and a rms value of surface roughness about $3{\AA}$.

Filler-Elastomer Interactions. 1. Roles of Modified Carbon Black Surfaces to Enhance Mechanical Properties of Carbon Black/Rubber Vulcanizates (충전재-탄성체 상호작용. 1. 표면처리된 카본블랙이 카본블랙/고무 복합재료의 기계적 물성에 미치는 영향)

  • Kim, Jeong-Soon;Nah, Chang-Woon;Park, Soo-Jin
    • Elastomers and Composites
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    • v.35 no.2
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    • pp.98-105
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    • 2000
  • Using FT-IR and contact angle measurements it is observed that the chemical surface treatments on virgin carbon blacks lead to a change of the surface properties, including surface functionality and surface free energy It is found that the developments of surface functional groups on acidically and basically treated (ACB and BCB in this study, respectively) carbon blacks are largely correlated with the specific component of surface free energy of the carbon blacks. However, a significant advantage of compounding composites is gained by BCB or NCB (nonpolar chemical treatment) specimens, resulting in improving the hardness, elongation at break, and tensile strength. Particularly, it is seen that the tensile strength of the composites are greatly depended on the London dispersive component of surface free energy determined from the contact angle measurements. It is then concluded that the London dispersion component of carbon blacks plays an important role in an organic rubbers-based compounding composite system.

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A Study on Sintering and Mechanical Properties of $Si_3N_4$ (질화규소의 소결 및 기계적 성질에 관한 연구)

  • 이회동;이준근
    • Journal of the Korean Ceramic Society
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    • v.21 no.4
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    • pp.361-365
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    • 1984
  • This study has been carried out to sinter silicon nitride with additives and to show the effect of surface finishments on its strength and Weibull modulus which are two most important factors for its applications into structural ceramics. Silicon nitride was sintered with the additions of $Al_2O_3$ and $Y_2O_3$ under pressureless cond-ition. The optimum properties were obtained by sintering at 1, 75$0^{\circ}C$ for 3hrs under $N_2$ atmosphere and the strength showed 6, 500kg/$cm^2$ at room temperature and 3, 300kg/$cm^2$ at 120$0^{\circ}C$. The effects of surface treatment on the strength of sintered $Si_3N_4$ were studied and the results showed that fine surface treatment increased the strength by up to 50% The Weibull analysis showed that its modulus was increased with increasing fineness of surface finishments. It was concluded that the mechanical properties of sintered silicon nitride could be improved by fine surface grinding which implied the brittle-fracture nature of sintered silicon nitride.

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Detoxification Properties of Surface Aminated Cotton Fabric (아민화 표면 처리된 면직물의 제독 성능 연구)

  • Kim, Changkyu;Kwon, Woong;Jeong, Euigyung
    • Textile Coloration and Finishing
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    • v.32 no.2
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    • pp.73-79
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    • 2020
  • Pursuing the fabric materials for military chemical warfare protective clothing with the improved detoxification properties, this study investigated the simple and effective cotton treatment method using pad-dry-cure process and 3-aminopropyltrimethox ysilane(APTMS) solution for surface amination. Detoxification properties of the untreated and treated cotton fabrics were evaluated via decontamination of chemical warfare agent simulant, DFP(diisopropylfluorophosphate). The surface aminated cotton fabric increased the rate of the hydrolysis of DFP by the factor of 3 and the decontamination ratio reached 88.2% after 24h. Therefore, the surface amination of the cotton fabric with APTMS can be an effective pathway to prepare the material for protective clothing against chemical warfare agents.

Study on the Adhesive Properties of Polyesters Reinforcing Materials

  • Krump, H.;Hudec, I.;Cernak, M.;Janypka, P.
    • Elastomers and Composites
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    • v.37 no.3
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    • pp.192-194
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    • 2002
  • Polyester cord yarns have been treated in an atmospheric-pressure nitrogen plasma reactor in order to enhance their adhesion to rubber. A thin layer or the plasma was generated in the close vicinity of the yam surface using various types or surface discharge. To assess the effect of the plasma treatment on fiber surface properties, the cord thread/rubber matrix adhesion values measured using the untreated and threads cord threads were compared. The static and dynamic adhesion of the cord thread to rubber was characterized by using the standard Henley test. The dynamic adhesion values for the reference and plasma treated fiber were $7,3{\pm}1,2\;N$ and $83,5{\pm}3,5\;N$. The surface properties were investigated by scanning electron microscopy, infrared spectroscopy and electron spin resonance spectroscopy. It is concluded that both polar group interactions and increased surface area of the fibers are responsible for the improved adhesive strength.

Filler-Elastomer Interactions. 3. Microstructures and Mechanical Interfacial Properties of Anodized Carbon Black/Rubber Composites

  • Park, Soo-Jin;Kim, Jeong-Soon;Lee, Jae-Rock
    • Carbon letters
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    • v.1 no.3_4
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    • pp.138-142
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    • 2001
  • The effect of electrochemical surface treatments in KOH chemical solution on microstructures of carbon blacks was investigated in terms of surface functional values and XRD measurements. And their mechanical interfacial properties of the carbon blacks/rubber composites were studied by the composite tearing energy ($G_{IIIC}$). It was found that the development of basic-surface functional groups lead to the significant physical changes of carbon blacks, such as, decrease of the interlayer spacing ($d_{002}$), increase of the crystalline size along c-axis ($L_c$), and increase of degree of crystalline (${\chi}_c$). This treatment is possibly suitable for carbon blacks to be incorporated in a hydrocarbon rubber matrix, resulting in improving the hardness and tearing energy of the resulting composites.

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Benchmark Study on Surface Roughness and Mechanical Properties of Rapid Prototypes (쾌속조형부품의 표면거칠기와 기계적 물성치에 관한 비교)

  • Kim Gi-Dae;Kim Jung-Yun
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.15 no.4
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    • pp.56-62
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    • 2006
  • Various kinds of rapid prototyping processes are available, such as stereo-lithography apparatus(SLA), fused deposition modeling(FDM), selective laser sintering(SLS), 3 dimensional printing(3DP), and laminated object manufacturing(LOM). In this study, benchmark tests are carried out to obtain detailed informations about surface roughness and mechanical properties of those parts. Although the patterns and roughness averages of part surface are dependent on the surface direction, the roughness of SLA part is the best and that of FDM or 3DP part is the worst. It is shown that FDM part has an advantage in impact strength, SLS(or EOS) part in compressive strength, and LOM part has an advantage in tensile strength and heat resistance, but the change of building direction in FDM and LOM processes severely weakens the tensile and impact strengths.

Surface-Properties of Poly(Ethylene Terephthalate) Fabric by In-line Atmospheric Plasma Treatments (연속 대기압 플라즈마를 처리한 폴리에스테르 섬유의 표면 특성)

  • Kwon, Il-Jun;Park, Sung-Min;Koo, Kang;Song, Byung-Kab;Kim, Jong-Won
    • Textile Coloration and Finishing
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    • v.19 no.4
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    • pp.38-46
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    • 2007
  • Surface properties of the plasma treated fabric were changed while maintaining its bulk properties. Surface of plasma treated fabric take charge of enhanced adhesion by surface etching, surface activity. The water repellency coating Poly(Ethylene Terephthalate) fabric was treated with atmospheric pressure plasma using various parameters such as Argon gas, treatment time, processing power. Morphological changes by atmospheric pressure plasma treatment were observed using field emmission scanning electron microscopy(FE-SEM) and the zeta-potential measurement, contact angle measurement equipment. At the atmospheric pressure plasma treatment time of 150 sec, the power of 800W, the best wettability and peel strength were obtained. And we confirmed the possibility of industrial application by using atmospheric plasma system.

Development of the Program Road lighting Road Surface Property Measuring Apparatus (도로조명용 프로그램과 노면특성 장치의 개발)

  • ;金紀勳
    • The Proceedings of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.13 no.2
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    • pp.133-133
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    • 1999
  • Average illuminance and luminance can be calculated by graphical methods to a certain extent but to calculate for a wide place a suitable software is needed. Softwares suitable for this purpose have been already developed in foreign nations, but the appropriate softwares for domestic use have not been developed. Therefore a program is developed which is executable in Hangul Windows. The softwares LAPRoad, is developed to calculate luminance and illuminance distribution of road surface, as well as average luminance and illuminance, overall uniformity, longitudinal uniformity, threshold increment veilling luminance and glare. And an apparatus that measures road surface reflection properties is developed. Because the road surface reflection properties is very important in luminance calculation, then concrete road surface reflection properties were measured.

Magnetonic Resistance Properties of Semiconductor Thin Films by Plasmon Effect on Fabricated Si(100) Substrate (플라즈몬 효과에 의한 실리콘 기판위에 증착된 반도체 박막의 자기저항특성)

  • Oh, Teresa
    • Journal of the Semiconductor & Display Technology
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    • v.18 no.3
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    • pp.105-109
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    • 2019
  • Plasmons have conductive properties using the effect of amplifying magnetic and electric fields around metal particles. The collective movement of free electrons in metal particles induces and produces the generation of plasmon. Because the plasmon is concentrated on the surface of the nanoparticles, it is also called the surface plasmon. The polarizing effect of plasma on the surface is similar to the principle of surface currents occurring in insulators. In this study, it was found the conditions under which plasma is produced in SiOC insulators and studied the electrical properties of SiOC insulators that are improved in conductivity by plasmons. Due to the heat treatment temperature of thin film, plasma formation was shown differently, metal particles were used with normal aluminium, SiOC thin films were treated with heat at 60 degrees, conductivity was improved dramatically, and heat treatment at higher temperatures was found to be less conductivity.