• Title/Summary/Keyword: surface modulus

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The Rheological Behaviors of Solid-Liquid Transfer Emulsion (고상-액상 전이형 에멀젼의 레올로지 거동)

  • Park, Byeong-Gyun;Han, Jong-Sub;Lee, Sang-Min;Lee, Cheon-Koo;Yoon, Moung-Seok
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.31 no.2 s.51
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    • pp.135-140
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    • 2005
  • A solid state emulsion haying high velocity gradient shows two important transition ranges in the plot of storage modulus(G') as a function of shear strain, when the state is changed from solid to liquid. However, a solid state emulsion having low velocity gradient shows only one apparent transition range when the change from solid to liquid state takes place. The result implies the importance of the surface properties in the solid state emulsion. The addition of water phase in the solid state emulsion reduces the modulus in the modulus in the surface transition range by increasing interfacial friction and weakening the matrix. The addition of pigments increases the modulus in the modulus in the surface transition range by reinforcing the matrix, when there is no wafer phase in the solid state emulsion. When the solid state emulsion has water phase, however, the addition of pigments decreases the modulus in the modulus in the surface transition range.

Effect of Distance Between Filler Particles on the Tensile Properties (충진 입자 계면간 거리가 물성에 미치는 영향)

  • 돈윤승;심미자;김상욱
    • Journal of the Korean institute of surface engineering
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    • v.25 no.4
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    • pp.165-172
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    • 1992
  • Filler, popularly used in the polymer materials, was dispersed randomly and irregularly. For the study of dispersed behavior, the specimen which have two particles in polystyrene was prepared. And the tensile strength, modulus and SEM picture were measured. When the distance between particles increased, the tensile strength and modulus increased, but particle size did not affect the values. And when the am-bient temperature increased, the tensile strength and modulus decreased, but the distance did not affect the tensile strength and modulus.

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High-speed Microcantilever Resonance Testing on the Young's Modulus of a Nanoscale Titanium Film (고속 마이크로 외팔보 공진시험을 통한 나노스케일 티타늄 박막의 탄성계수 평가)

  • Kim, Yun Young
    • Journal of the Korean institute of surface engineering
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    • v.50 no.5
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    • pp.392-397
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    • 2017
  • The Young's modulus of a nanoscale titanium (Ti) thin-film was evaluated using a high-speed microcantilever resonating at the megahertz frequency in the present study. A 350 nm thick Ti film was deposited on the surface of a silicon microcantilever, and the morphology of the film was analyzed using the atomic force microscopy. The microcantilever was excited to resonate using an ultrasonic pulser that generates tone burst signals and the resonance frequency shift induced by the deposition of Ti was measured using a Michelson interferometer. The Young's modulus was determined through a modal analysis using the finite element method and the result was validated by the nanoindentation testing, showing good agreement within a relative error of 1.0%. The present study proposes a nanomechanical characterization technique with enhanced accuracy and sensitivity.

Determination of Mechanical Properties of Equal Channel Angular Pressed Aluminum Alloys in Nano-surface Region (나노표면 영역에서의 ECAP 변형된 알루미늄합금의 기계적 물성변화 측정)

  • An, SeongBin;Kim, ChungSeok
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.3
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    • pp.113-117
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    • 2019
  • The effects of severe plastic deformation and heat treatment on the mechanical properties of Al 5052 and 6005 alloys were investigated using the metallurgical technique and nano-indentation technique in nano-surface region. Equal channel angular pressing (ECAP) was used to apply severe plastic deformation to the aluminum alloys in order to obtain fine grain sized materials. The elastic modulus was measured and interpreted in relation to the metallurgical observation. The elastic modulus increased after ECAP process due to evolution of the fine grains. However, the elastic modulus decreased after heat treatment due to generation of coarsened precipitates on the grain boundaries.

A Study on Normal Range of Surface Deflection for Epoxy Asphalt Pavement using Light Weight Deflectormeter (LWD를 활용한 에폭시 아스팔트 포장의 정상 표면처짐 범위 연구)

  • Park, Ki Sun;Kim, Kyung Nam;Kim, Nak Seok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.35 no.1
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    • pp.229-236
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    • 2015
  • In this study, the resilient modulus test and Light Weight Deflectormeter (LWD) test were conducted to simulate the moving vehicle load for the evaluation of the internal failure of epoxy asphalt pavement. The Measured displacement in the resilient modulus test of epoxy asphalt concrete showed very little residual deformation under repeated loads unlike the conventional asphalt. Therefore, the test results were evaluated as a normal state due to its similarity with elastic deformation. The deflection results from the resilient modulus tests were converted to the surface deflection modulus and the normal range of surface deflection modulus was estimated applying LWD measurement of 1 SIGMA level. Internal failure of pavements were estimated using the suspicious failure range at $60^{\circ}C$ and hysteresis. Internal moisture penetration and a decrease in bonding were observed in partial areas at $140{\mu}m$ of surface deflection. However, the areas showed inflection points in the hysteresis. Field investigation by suggested criterion indicated a high degree of accuracy.

Effect of the Elasticity Modulus of Jig Material on Blade Edge Shape in Grinding Process of Sapphire Medical Knife (사파이어 의료용 나이프의 연삭가공에서 지그의 탄성계수가 날 부 형상에 미치는 영향)

  • Shin, Gun-Hwi;Lee, Deug-Woo;Kwak, Tae-Soo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.2
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    • pp.102-107
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    • 2017
  • This study focuses on the effect of the elasticity modulus of jig material on blade edge shape in the grinding process of a sapphire medical knife. The ELID grinding process was applied as the edge-grinding method for sapphire material. Carbon steel and copper have been selected as the hard and soft jig materials, respectively. The blade edge created by ELID grinding was measured by a surface roughness tester and optical microscope. The shape of the ground edge and surface roughness were compared using the measurement results. As a result, it was found that chipping in the blade edge of the sapphire knife occurred more than in the case of jig material with a high-elasticity modulus because of the high normal force in the grinding process. Moreover, the maximum height surface roughness, $R_{max}$,of the ground surface was higher in the case of the jig material with a high-elasticity modulus due to the difference in elasticelongation. It was considered to lead to chipping from the notch effect.

Mechanical parameters detection in stepped shafts using the FEM based IET

  • Song, Wenlei;Xiang, Jiawei;Zhong, Yongteng
    • Smart Structures and Systems
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    • v.20 no.4
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    • pp.473-481
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    • 2017
  • This study suggests a simple, convenient and non-destructive method for investigation of the Young's modulus detection in stepped shafts which only utilizes the first-order resonant frequency in flexural mode and dimensions of structures. The method is based on the impulse excitation technique (IET) to pick up the fundamental resonant frequencies. The standard Young's modulus detection formulas for rectangular and circular cross-sections are well investigated in literatures. However, the Young's modulus of stepped shafts can not be directly detected using the formula for a beam with rectangular or circular cross-section. A response surface method (RSM) is introduced to design numerical simulation experiments to build up experimental formula to detect Young's modulus of stepped shafts. The numerical simulation performed by finite element method (FEM) to obtain enough simulation data for RSM analysis. After analysis and calculation, the relationship of flexural resonant frequencies, dimensions of stepped shafts and Young's modulus is obtained. Numerical simulations and experimental investigations show that the IET method can be used to investigate Young's modulus in stepped shafts, and the FEM simulation and RSM based IET formula proposed in this paper is applicable to calculate the Young's modulus in stepped shaft. The method can be further developed to detect mechanical parameters of more complicated structures using the combination of FEM simulation and RSM.

Characterization of Thin Film Materials by Nanoindentation and Scanning Probe Microscopy (나노인덴테이션과 주사탐침현미경을 이용한 박막 재료의 특성평가)

  • Kim, Bong-seob;Yun, Jon-do;Kim, Jong-kuk
    • Korean Journal of Materials Research
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    • v.13 no.9
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    • pp.606-612
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    • 2003
  • Surface and mechanical properties of thin films with submicron thickness was characterized by nanoindentation with Berkovich and Vickers tips, and scanning probe microscopy. Nanoindention was made in a depth range of 15 to 200 nm from the surface by applying tiny force in a range from 150 to $9,000 \mu$N. Stiffness, contact area, hardness, and elastic modulus were determined from the force-displacement curve obtained. Reliability was first tested by using fused quartz, a standard sample. Elastic modulus and hardness values of fused quartz measured were the same as those reported in the literature within two percent of error. Mechanical properties of ITO thin film were characterized in a depth range of 15∼200nm. As indentation depth increased, elastic modulus and hardness decreased by substrate effect. Ion beam deposited DLC thin films were indented in a depth range of 40∼50 nm. The results showed that the DLC thin film using benzene and bias voltage 0∼-50 V has elastic modulus and hardness value of 132 and 18 GPa respectively. Pure DLC thin films showed roughnesses lower than 0.25 nm, but silicon-added DLC thin films showed much higher roughness values, and the wavy surface morphology.

Surface Characteristics of TiN and ZrN Film Coated STD 61 by Sputtering (스퍼터링법으로 TiN 및 ZrN 피막 코팅된 STD 61의 표면특성)

  • Eun, Sang-Won;Choe, Han-Cheol
    • Journal of the Korean institute of surface engineering
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    • v.43 no.6
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    • pp.260-265
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    • 2010
  • STD 61 steel has been widely used for tools, metallic mold and die for press working because of its favorable mechanical properties such as high toughness, and creep strength as well as excellent oxidation resistance. The STD 61 tool steel coated with TiN and ZrN by sputtering results in improvement of wear and corrosion resistance. In this study, surface characteristics of TiN and ZrN film coated STD 61 by sputtering were studied by using FE-SEM, EDS, XRD, and XRR and nanoindentation tests. From the results of surface characteristics of coated specimen, the ZrN coated surface showed finer granular than that of TiN coated surface. The coated layer structures of ZrN and TiN were grown to (111) and (200) preferred orientation. From the results of XRR test for surface roughness, density and growth rate of coating film, surface roughness and growth rate of ZrN coated film revealed lower values those of TiN coated film, whereas density of ZrN coated film showed higher values than that of TiN coated film. From the nanohardness and elastic modulus test, nanohardness value and elastic modulus of ZrN coated film became higher than those of TiN coated film.

A study on the Polymer surface treatment of GF-filter bag for collection of fine Particle like carbon black (카본블랙류 미세입자 포집을 위한 유리섬유 필터백의 고분자 표면처리에 관한 연구)

  • Lee, B.;Choi, H.L.;Moon, C.K.
    • Journal of Power System Engineering
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    • v.12 no.3
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    • pp.55-59
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    • 2008
  • In this paper, we have investigated on collection efficiency of fine particle of glass fiber-filter bag according to the surface treatment. The solution consisted of polytetrafluoroethylene(teflon), graphite powder, silicon resin and water was used as a basic surface treatment agent. Tensile strength of glass filter-bag increased with up to 3hrs and then decreased with surface treatment time. Tensile strength and initial modulus of the glass fiber-filter bag treated by iodine after basic surface treatment for 3hrs were lower than those of basic surface treatment for 3hrs, however collection efficiency and fracture strain were higher than those of basic surface treatment for 3hrs. Glass fiber-filter bag with lower initial modulus and more strain will be extend the durable period and the one treated by iodine after basic surface treatment 3or 3hrs is expected high collection efficiency of fine particle. This method makes it possible to manufacture glass fiber-filter bag of the optimum condition.

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