• Title/Summary/Keyword: surface microhardness

검색결과 320건 처리시간 0.027초

Ag+ 이온교환에 따른 유리의 착색 효과 (The Coloring Effect of Glasses by Ag+ Ion Exchange)

  • 이용근;이동인;윤종석;이희수
    • 한국세라믹학회지
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    • 제26권4호
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    • pp.499-504
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    • 1989
  • Coloring effect, mechanical properties resulting from silver ions exchange of glasses immersed into the mixed molten salt of KNO3 and AgNO3 were investigated in this study. Ion exchange coloring of glasses made it possible to obtain glasses with a range from yellow to yellowish-brown, and spectral transmittance was investigated. The amount of ion exchange and peneration depth increased with treatment temperature and time. The activation energy decreased with mole fraction of AgNO3. It can be seem that the bending strength of ion exchanged glasses were 3~4 times higher than the parent glass and Ag+ colloids prevented from increasing surface microhardness.

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분산법이 무전해 Ni-CNT 복합도금막 형성에 미치는 영향 (Effect of Dispersion Method on Formation of Electroless Ni-CNT Coatings)

  • 배규식
    • 반도체디스플레이기술학회지
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    • 제13권3호
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    • pp.51-55
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    • 2014
  • Ni-CNT(Carbon Nanotubes) composite coating is often used for the surface treatment of mechanical/electronic devices to improve the properties of the Ni coating. For the Ni-CNT coating, the dispersion of CNT fibers is a critical process. In this study, ultrasonic treatment instead of the conventional ball milling was attempted as a dispersion method for the electroless Ni-CNT coating. SEM-EDX analysis was performed and contact angle, sheet resistance, and micro-hardness were measured. Results showed that the ultrasonic treatment was comparable to the ball milling, as a dispersion method, but the difference was negligible. However, combined ball milling and ultrasonic treatment(double treatment) showed much improved micro-hardness value, above 350Hv(close to the value obtained by the Ni-CNT electroplating). In addition, electroless Ni-CNT(double-treated) coatings formed on the thin Ni film deposited by the electroless plating(double coating) showed better mechanical properties. Thus, double treatment and double coating are suggested as an improved electroless Ni-CNT coating method.

이온교환에 따른 비정질 고체재료의 특성화(II) : 기계적 물성 거동 (Characterization of Glasses by Ion-Exchange(II) : Behavior of Mechanical Properties)

  • 이동인;이용근;이희수
    • 한국세라믹학회지
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    • 제25권6호
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    • pp.665-670
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    • 1988
  • The behavior of mechanical properties of ion exchanged glasses was investigated in this study. The used glasses were soda-lime-silica glasses that were produced by float process. The maximum values of the bending strength and the curvature depth are 45Kg/$\textrm{mm}^2$ and 8.6mm respectively treated at 45$0^{\circ}C$ for 6h, which are 4.4 times and 3.3 times higher than parent glass. In the case, the thermalshock resistance ΔT is 335$^{\circ}C$ that is 205$^{\circ}C$ higher than parent glass, which is the maximum values in this study. The maximum values of the surface microhardness is 490Kg/$\textrm{mm}^2$ in case of 43$0^{\circ}C$ for 4h. It is also found out that annealing points are increased linearly with increasing the amount of K+ ion exchange independent of treatment temperature. Furthermore, the present work shows that the ion exchange strengthened glasses are more effective than the physical tempering glasses ; the bending strength and the curvature depth are 1.8 times and twice higher respectively.

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도시가스용 D3507 및 D3631 강관의 파괴특성 (Fracture Characteristics of D 3507 and D 3631 City Gas Steel Pipes)

  • 박재학;김한국;신규인;김만원
    • 한국안전학회지
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    • 제16권4호
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    • pp.39-46
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    • 2001
  • It is noted that KS D 3507 pipe steel has several problems when it is used as a city gas pipe at medium pressure. So new pipe steel, KS D 3631, was developed in order to be used as a pipe for medium and low pressure and now it is being substituted for D 3507. In this study, several mechanical tests, such as tensile test, microhardness test, and Charpy impact test were conducted to get material properties of D 3507 and D 3631 pipe steels. And also microstructures at the weld and heat affected zones were observed for the two materials. From the Charpy test results $K_{IC}/$ was estimated for the upper and lower shelf and the critical crack length is calculated for supposed axial semi-elliptical surface cracks. And the burst pressure is estimated as a function of wear depth for a defective D 3631 pipe by using the finite element method. The burst pressure is also calculated for pipes with an axial crack by using the published equations.

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입자분산이 Ni-CNT 복합도금막의 특성에 미치는 영향 (Effect of Particle Dispersion on Physical Properties of Ni-CNT Composite Coatings)

  • 천영훈;배규식
    • 반도체디스플레이기술학회지
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    • 제10권2호
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    • pp.91-95
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    • 2011
  • Ni-CNT(carbon nanotubes) composite coating is often used for the surface treatment of electronic/mechanical devices to improve the properties of the exisiting Ni electroplating. For this, the dispersion of CNT particle is a critical process. In this study, ball milling and additive called sodium dodecyl sulfate(SDS) are employed for dispersion. Electroplated Ni-CNT films were examined by SEM-EDX, AES, microhardness tester, 4-point probe and contact angle measurement to find the optimum dispersion conditions. Ni-CNT coatings formed by ball milling for 9 hrs and with addition of SDS 12 times of CNT contents showed the highest hardness, reasonable resistivity and non-stick characteristics.

Nozzles from Alumina Ceramics with Submicron Structure Fabricated by Radial Pulsed Compaction

  • Kaygorodov, Anton;Rhee, Chang;Kim, Whung-Whoe;Ivanov, Viktor;Paranin, Sergey;Spirin, Alexey;Khrustov, Vladimir
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.368-369
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    • 2006
  • By means of magnetic pulsed compaction and sintering of weakly aggregated alumina based nanopowders the jet forming nozzle samples for the hydroabrasive cutting were fabricated. The ceramics was obtained from pure alumina, as well as from alumina, doped by $TiO_2$, MgO and AlMg. It was shown that the samples sintered from AlMg doped $Al_2O_3$ powder have the best mechanical properties and structural characteristics: relative density ${\sim}0.97$, channel microhardness. - 18-20 GPa, channel surface roughness ${\sim}0.7\;{\mu}m$, average crystallite size ${\sim}1\;{\mu}m$.

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Tribological Properties of Ti(C,N)-based Cermet after Hot Isostatic Pressing at High Nitrogen Pressure

  • Xiong, Wei-hao;Zheng, Li-yun;Yan, Xian-mei
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.663-664
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    • 2006
  • Sintered Ti(C,N)-based cermets were treated with hot isostatic pressing (HIP) at different nitrogen pressures. The tribological properties of the treated cermets have been evaluated. The results show that a hard near-surface area rich in TiN formed after HIP treatment. The cermets treated at higher pressure had a relatively lower friction coefficient and specific wear rate. In all cases the microhardness of treated cermets is higher than that without HIP natridation. The wear mechanisms of cermets were hard particle flaking-off and ploughing. It was also found that the HIP natridation is well-suited for improving the tribological properties of cermets.

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급속응고 Al-20 wt% Si 합금 분말의 ECAP를 통한 고형화 (Consolidation of Rapidly Solidified Al-20 wt% Si Alloy Powders Using Equal Channel Angular Pressing)

  • 윤승채;홍순직;서민홍;정영기;김형섭
    • 한국분말재료학회지
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    • 제11권3호
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    • pp.233-241
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    • 2004
  • In this study, bottom-up type powder processing and top-down type SPD (severe plastic deformation) approaches were combined in order to achieve both full density and grain refinement of Al-20 wt% Si powders without grain growth, which was considered as a bottle neck of the bottom-up method using the conventional powder metallurgy of compaction and sintering. ECAP (Equal channel angular pressing), one of the most promising method in SPD, was used for the powder consolidation. The powder ECAP processing with 1, 2, 4 and 8 passes was conducted for 10$0^{\circ}C$ and 20$0^{\circ}C$ It was found by microhardness, compression tests and micro-structure characterization that high mechanical strength could be achieved effectively as a result of the well bonded powder contact surface during ECAP process. The SPD processing of powders is a viable method to achieve both fully density and nanostructured materials.

플라즈마 절단 후 제작도니 용접부의 기계적 특성 (Mechanical Properties of Welded Materials after Plasma Cutting)

  • 신규인;김형곤;박재학;김성청
    • 한국정밀공학회지
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    • 제16권9호
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    • pp.68-74
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    • 1999
  • The influence of surface preparation methods after plasma cutting on the quality of weld zone was investigated. For comparison, three types of welded specimens were prepared by machining (WM), plasma cutting with light regrinding (WPG) and without regrinding (WP), by using three kinds of materials, carbon steel (SM45C), stainless steel (STS304) and aluminum alloy (A6061-T6). Nondestructive examination, hardness test, microstructure examination, and fracture toughness test were performed. The results showed that there was no appreciable reduction in hardness or fracture toughness in WP specimens. But a little difference in heat affected zone size was observed.

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冷間壓廷鋼板의 Aluminizing에 對한 速度論的인 硏究 (A Study on the kinetics of Aluminizing of Cold rolled Steel Sheets)

  • 윤병하;김영기
    • 한국표면공학회지
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    • 제12권2호
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    • pp.75-83
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    • 1979
  • The Rates of formation and heats of activation for the intermatallic Compound Layers between Cold rolled sheet and molten aluminium &ath (adding small amounts of silicon) has been determined by Continous aluminizing method in the temperature range of 680$^{\circ}$ to 760$^{\circ}C$ and with immerssion time. The structure of the intermetallic Compound Layers was the shape of "Tongues" in pure Al-Bath and Al-Bath Containing 1% Si, But in Al-5% Si Bath was "Band" the Composition of the intermetallic Compound Layers were checked by microhardness measurements and X-Ray probe micro analyzer. FeAl intermetallic Compound layer was found to be uniform in pure Al-Bath and Al-5% Si Bath, But Fe Al intermetallic Compound Layer was shown in Al-1% Si Bath. The growth Rates of the intermetallic Compound Layers was most rapidly increased at Temperatures from 720$^{\circ}$ to 760$^{\circ}C$, at the immorsion time above 60 Second in pure Al-Bath, But in Al-1% Si Bath was solwly increased for the same conditions, and then in Al-5% Si Bath was hardly effected by these experimental condition. Heasts of activation of 29, 46 Kcal per mole which calculuted from Layer growth experiments were found in pure Al-Bath, Al-1% Si Bath respectively.

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