• Title/Summary/Keyword: surface investigation

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Introduction of a novel swabbing material of a wiper and establishment of an optimal method for the collection of organic explosive residues

  • Sung, Tae-myung;Lee, Jong Hyup;Cho, Ju-ik
    • Analytical Science and Technology
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    • v.30 no.6
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    • pp.319-328
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    • 2017
  • The identification of explosive residues on specimens obtained from an explosion event is a crucial factor for assessing the cause of the explosion. In order to detect the components of explosives, the explosive residues deposited on surfaces are commonly extracted using swabbing materials pre-wetted with an organic solvent. The residues are then analyzed with analytical instruments such as LC/MS and CE/MS. Most conventionally used swabbing media such as cotton swabs or cotton tip swabs seem unsuitable for extracting explosive residues from the surface of a large area of clothes because the swabbing materials tend to be damaged easily, and because only a relatively small amount of explosives is collected. To overcome these problems, we have introduced a novel wiper ($215{\times}210mm$, single layer, Yuhan-Kimberly, Republic of Korea) as a swabbing material to recover representative organic explosives, namely, TNT, RDX, tetryl, HMX, PETN, and NG, from a large area of clothes. Different sides of the wiper, which was folded in half five times, was used to swab the surface of a clothing. We compared this novel wiper with a cotton swab and a cotton tip swab in terms of the recovery efficiency for the aforementioned organic explosives by pre-wetting with methanol, acetone, and acetonitrile, respectively. We identified that this novel wiper collected a significantly higher amount of organic explosive residues than a cotton swab or a cotton tip swab when using methanol as an extracting solvent.

Assessment of Cutting Ability for CBN Ball End-Milling (금형가공에서의 CBN 공구의 절삭성능평가)

  • Choi, Won-Sik
    • Journal of the Korean Society of Industry Convergence
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    • v.8 no.4
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    • pp.227-234
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    • 2005
  • In this study an experimental investigation was conducted to assesment of cutting ability for CBN ball end-milling, STD11 and NAK80 materials. The cutting force and surface roughness of the work-pieces were obtained in machining center. The assessment of CBN tools were inspected through the tool dynamotor and SEM. When $30^{\circ}$ negative rake angle, the wear and cutting force were good, surface roughness was better at cutting fluid during CBN cutting.

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TUNNELLING IN SOFT GROUND IN URBAN AREAS

  • Fujita, Keiichi
    • Proceedings of the Korean Geotechical Society Conference
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    • 1990.10a
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    • pp.9-24
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    • 1990
  • Most tunnels in soft soils in urban areas are constructed by shield tunnelling method for environmental reasons. Ground surface settlements are caused by shield tunnelling so that auxiliary measures are often required. Simple methods to predict ground surface settlement are given. The use of the slurry or the earth pressure balance shield machine and the application of new methods of grouting with computer aided operation control systems decreases the ground surface settlement to 3 mm. The construction cost of tunnels is almost identical whichever type of shield machine is employed according to a statistical investigation.

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Determination of Surface Diffusivities of Oxides by the Combined Sintering (소결에 의한 산화물촉매의 표면확산계수의 측정)

  • 문세기;유경옥;김형진
    • Journal of the Korean Ceramic Society
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    • v.14 no.2
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    • pp.73-77
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    • 1977
  • The surface diffusion coefficients for nickel, nickel oxide, cuppric oxide, cobalt oxide, alumina and ferric oxide have been determined at various temperatures using the sintering technique. This investigation is based on the model accounting for the sum of the contribution of volume and surface diffusion to the overall shrinkage rate during the initial stage of sintering. Simultaneous measurements of shrinkages and shrinkage rates of the materials compacts were conducted for various annealing times, the results of which were then correlated to the diffusion coefficient.

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Numerical Investigation of Secondary Flow in 3 Pump Stages: Centrifugal Multistage/Mixed-flow Stage/ Axial-flow Stage (원심형, 사류형, 축류형 펌프단에서 살펴본 이차유동의 수치적 고찰)

  • Oh, Justin
    • 유체기계공업학회:학술대회논문집
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    • 2005.12a
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    • pp.359-364
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    • 2005
  • Centrifugal pump shows the strongest secondary flow. Wake is formed near pressure surface close to hub at impeller exit for centrifugal pump impeller. Pressure gradient drives secondary flow in the inducer region, while in the remaining region the following sources drive together: > Pressure gradient > Coriolis force Low-momentum fluid near suction surface hub moves toward pressure surface hub in mixed-flow pump impeller. Tip leakage vortex dominate secondary flow in axial-flow pump impeller. Tip leakage vortex dominate secondary flow in axial-flow in axial-flow pump impeller

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Investigation on Various Surface Treatment Technology for Durability Improvement Under Dynamic Condition (동적 환경하에서 내구성 향상을 위한 다양한 표면처리 기술 연구)

  • Kim, Seong-Jong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.3-3
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    • 2018
  • 산업 발전과 더불어 각종 장비들은 기존에 비해 현저히 가혹한 조건에서 운전되고 있다. 그러한 이유로 고유속, 고회전 등에 기인한 침식 및 캐비테이션 손상이 정적 환경과 비교할 수 없을 정도로 내구성이 저하되어 큰 손상 사고로 이어지는 사례가 다발하고 있다. 아울러 해양환경은 가혹한 부식 조건이므로 동적 손상과 복합적으로 작용하여 그 장비수명은 현저히 단축되고 있는 실정이다. 이를 극복하기 위한 다양한 표면처리 기술이 필요하다고 할 수 있다.

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Investigation and research trend and for SiC complex made by Si-vapor diffusion reaction on carbon surface (카본표면에서 Si 증기입자의 확산 반응에 의한 SiC 복합체형성 검토 및 연구동향)

  • Park, Jang-Sik;Hwang, Jeong-Tae
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.195-195
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    • 2014
  • 탄화규소(SiC)의 복합체는 고온강도, 내식성, 내마모성, 내화학 특성, 열충격성 및 기계적 특성이 우수하며 제조공정으로 CVD 공정은 많이 연구되어져 있으나 비교적 간단한 구조로 우수한 특성을 얻을 수 Si 증발입자 확산방법에 대한 체계적인 연구가 수행되고 있지 않다. 본 논문에서는 Si 증발입자가 탄소표면에서 확산 반응으로 형성되는 SiC 복합체에 대한 검토 및 연구 개발 동향을 기술한다.

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Investigation of Ar ion-milling rates for ultrathin single crystals

  • Lee, Min-Hui;Kim, Gyu-Hyeon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.05a
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    • pp.143-144
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    • 2015
  • Here we report the Ar-ion milling rates of ultrathin Si and GaAs single crystals. The thickness change is measured using convergent beam electron diffraction (CBED) technique with the help of Bloch wave simulation method. This study suggests the experimental procedures to determine the references for an etching rate to reduce a sample thickness or to remove the damaged sample surface using Ar-ion source.

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Platinum Model Catalysts Dispersed on Alumina with Regular Pores (규칙적 세공을 가진 알루미나에 분산된 백금 모형촉매)

  • 윤천호;임헌성
    • Journal of the Korean institute of surface engineering
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    • v.33 no.4
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    • pp.261-265
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    • 2000
  • Geometrically and chemically well defined Pt/alumina model catalysts have been prepared. To this end, we fabricated electrochemically alumina supports in which pores of constant size, length and shape were regularly distributed over a wide area of the surface. Platinum particles were dispersed on the pore surfaces via organometallic chemical vapor deposition technique using (trimethyl) methylcyclopentadienylplatinum (IV) as a precursor. The chemical composition of the alumina plane surfaces was examined by Auger electron spectroscopy and the adsorption characteristics of the platinum particles were studied by thermal desorption spectroscopy. A variety of industrial catalytic problems are now open for further investigation utilizing the Pt/alumina model catalysts.

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Investigation of texturing to reduce surface reflectance of crystalline silicon solar cells (텍스쳐링을 이용한 결정질 실리콘 태양전지의 표면 반사율 감소에 대한 연구)

  • Choe, Jun-Yeong;Kim, Beom-Ho;Lee, Eun-Ju;Lee, Su-Hong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.04a
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    • pp.141-142
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    • 2007
  • 표면 수정에 의한 결정질 실리콘 태양전지의 표면 반사율의 감소는 실리콘 태양전지에 있어서 가장 중요한 문제들 중 하나다. 결정질 실리콘 기판 표면에 텍스쳐링을 이용하여 반사방지막을 형성하는 것은 태양전지의 표면 반사율을 줄이는 측면에서 주목할 만한 것이다. 이 논문에서는 단결정 실리콘과 다결정 실리콘에 텍스쳐링을 이용하여 표면 반사율을 감소할 수 있는 방안에 대해서 연구한다.

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