• 제목/요약/키워드: surface densification

검색결과 136건 처리시간 0.025초

소결 분위기에 따른 이산화 우라늄의 치밀화 및 입자성장 (Effect of Sintering Atmosphere on the Densification and Grain Growth of Uranium Dioxide at the Final-Stage Sintering)

  • 이영우
    • 한국분말재료학회지
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    • 제4권3호
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    • pp.214-221
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    • 1997
  • The densification and grain growth mechanisms of $UO_{2+x}$ in $H_2$ and in $CO_2$ have been investigated. Uranium dioxide powder compacts were sintered at 1$700^{\circ}C$ in $H_2$ or at 110$0^{\circ}C$ in $CO_2$ for various times from 0.5 h to 16 h. The grain size and density of the specimens were measured. From the measured data, the mechanisms of the densification and grain growth were determined by use of available kinetic equations which express the relations between densification and grain growth. In both atmospheres, it has been found that the densification was controlled by the lattice diffusion and the grain growth by the surface diffusion of atoms around pores. It appears that the surface diffusivity as well as the lattice diffusivity increase considerably with the increase in O/U ratio in the specimen.

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Al-20Si-5.5Fe-1.2Mg-0.5Mn 합금분말의 치밀화에 미치는 소결온도와 분위기의 영향 (Effects of Sintering Temperature and Atmosphere on Densification of Hypereutectic Al-Si Alloy Powders)

  • 이재욱;박상빈;양상선;김용진
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.196-203
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    • 2008
  • The densification behavior of Al-20Si-5.5Fe-1.2Mg-0.5Mn powders was investigated through micro-structure analysis of sintered specimens. The specimens sintered in vacuum or in high purity (99.999%) nitrogen showed porous near-surface microstructures. The densification of near-surface part was enhanced by means of ultra-high purity (99.9999%) nitrogen atmosphere. The relationship between slow densification and oxide surfaces of Al alloy powders was discussed. And the effects of Mg addition, nitrogen gas, and humidity on densification were discussed. In addition, the rapid growth of primary Si crystals above the critical temperature was reported.

Power-law 크리프 변형을 따르는 분말 성형체의 말기 치밀화 모델 (Constitutive Models for Final Stage Densification of Powder Compacts with Power-Law Creep Deformation)

  • 양훈철;김기태
    • 대한기계학회논문집A
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    • 제28권7호
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    • pp.930-939
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    • 2004
  • Constitutive models for final stage densification of metal powder compacts with power-law creep deformation were investigated. The constitutive models were implemented into a finite element program (ABAQUS) by using user subroutine CREEP and, from FEM results, useful densification curves were obtained when hydrostatic and uniaxial stress were applied to the powder compacts at various pressures and temperatures. Because the densification behavior varied as the constitutive models, the equivalent stress surface on each constitutive equation was investigated to analyze the difference of densification behavior.

The Application of P/M Advanced Techniques to Sintered Gears

  • Chongxi, Bao;Zhouqiang, Shen;Zhengping, Shu
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.987-988
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    • 2006
  • The processes of P/M affect the properties of sintered gears. The different techniques of P/M lead to the different properties of sintered gears. This paper summarizes new progress in powder metallurgy for sintered gears. These progresses include warm compaction, high velocity compaction, sinter hardening, high temperature sintering, infiltration, CNC powder press and surface densification etc.

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Surface Densification Coupled with Higher Density Processes Targeting High-performance Gearing

  • Hanejko, Francis;Rawlings, Arthur;King, Patrick;Poszmik, George
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.738-739
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    • 2006
  • This paper will describe a powder and processing method that facilitates single press-single sintered densities approaching $7.5g/cm^3$. At this sintered density, mechanical properties of the powder metal (P/M) component are significantly improved over current P/M technologies and begin to approach the performance of wrought steels. High performance gears have the added requirement of rolling contact fatigue durability that is dependent upon localized density and thermal processing. Combining high density processing of engineered P/M materials with selective surface densification enables powder metal components to achieve rolling contact fatigue durability and mechanical property performance that satisfy the performance requirements of many high strength automotive transmission gears. Data will be presented that document P/M part performance in comparison to conventional wrought steel grades.

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산화처리된 구형 Fe 분말 성형제의 방전플라즈마 소결거동에 관한 연구 (Densification Behavior of the Oxidation-treated Spherical Fe-powder Compact during Spark-Plasma Sintering Process)

  • 권영순;김윤호;김지순;석명진;문진수;김환태
    • 한국분말재료학회지
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    • 제8권1호
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    • pp.61-69
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    • 2001
  • Spark-Plasma Sintering(SPS) is one of the new sintering methods which takes advantages both inconventional pressure sintering and electric current sintering. It is known that SPS is very effective for the densification of hard-to-sinter materials like refractory metals, intermetallic compounds, glass and ceramics without grain growth. However, a clear explanation for sintering mechanism and an experimental evidence for the formation of weak plasma during SPS are not given yet. In this study, fundamental study on sintering behavior and mechanism of SPS was investiged. For this study, various spherical Fe powders were prepared such as as-received, as-reduced, and as-oxidized and then sintered by SPS facility. In order to confirm the surface cleaning effect during SPS neck region and fracture surface of sintered body was observed and analyzed by SEM/EPMA. Densification behavior was analyzed from the data of deflection along the pressure axis. Some specimens were additionally produced by Hot Pressing and the results were compared with those of SPS.

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Performance of a Surface Densified P/M Gear for a Passenger Car Gear Box

  • Rau, Gunter;Sigl, Lorenz S.;Mork, Gerold;Wattenberg, Frank
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.389-390
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    • 2006
  • Selective surface densification is a tool for improving the mechanical properties of PM steels, such that the requirements for highly loaded gears can be matched. This paper describes the manufacturing and the properties of a helical P/M gear. The gear performance was evaluated on a 3-shaft back to back test rig, on a load bearing test rig and on a sound test bench. The results of these tests are presented and compared to data obtained from solid steel gear with identical geometry and surface quality. This comparison indicates that P/M gears have a load bearing capacity and noise level which are both well comparable to solid steel gears.

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열화상분석 및 CLSM을 이용한 재생지의 고밀화 현상 연구 (Studies on the Densification of Recycled Sheet Structure with Thermal Image Analysis and CLSM)

  • 이학래;김철환;윤혜정;정태민
    • 펄프종이기술
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    • 제31권4호
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    • pp.8-15
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    • 1999
  • The effects of Condebelt press drying on the densification of recycled sheets made from KOCC , AOCC UKP and BKP were examined using CLSM (Confocal Laser Scanning Microscope) and thermal image analysis techniques. It was shown that significant improvement in sheet density, compression strength, tensile strength, surface smoothness was obtained by Condebelt drying. Densification effect by press drying was most prominent for recycled KOCC sheets. And this beneficial effect of Condebelt drying of increasing sheet density and strength was shown to provide opportunities of reducing the utilization ratio of AOCC for cost saving.

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Distribution of Deposited Carbon in Carbon Brake Disc Made by Pressure-Gradient Chemical Vapor Infiltration

  • Chen, Jianxun;Xiong, Xiang
    • Carbon letters
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    • 제8권1호
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    • pp.25-29
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    • 2007
  • The carbon brake discs were manufactured by densification the carbon fiber preform using PG-CVI technology with Propene as a carbon precursor gas and Nitrogen as a carrier gas. The densities of carbon brake discs were tested at different densification time. The results indicate that the densification rate is more rapid before 100 hrs than after 200 hrs. The CTscanning image and the SEM technology were used to observe the inner subtle structure. CT-images show the density distribution in the carbon brake disc clearly. The carbon brake disk made by PG-CVI is not very uniform. There is a density gradient in the bulk. The high-density part in the carbon brake is really located in the friction surface, especially in the part of inner circle. This density distribution is most suitable for the stator disc.

$Al_2O_3-SiC$ 복합재료의 상압소결시 치밀화에 미치는 SiC 원료분말의 크기영향 (Effect of SiC Particles Size on the Densification of $Al_2O_3-SiC$ Composite During Pressureless Sintering)

  • 채기웅
    • 한국세라믹학회지
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    • 제36권11호
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    • pp.1261-1265
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    • 1999
  • Effect of SiC particle size of the densification of Al2O3-SiC composite during pressureless sintering was investigated. Two types of SiC powders having average particle size of 0.15${\mu}{\textrm}{m}$ and 3${\mu}{\textrm}{m}$ were used. Densification rate of the specimen containing 0.15${\mu}{\textrm}{m}$ SiC particles was slower than that of the specimen containg 3${\mu}{\textrm}{m}$ SiC particles. Although the relative density of the specimen containing 0.15${\mu}{\textrm}{m}$ SiC particles was below 90% of theoretical density after sintering at 155$0^{\circ}C$ the complete closure of open pores occurred. Therefore full densification could be obtained by subsequent HIP. On the other hand in the specimen containing 3${\mu}{\textrm}{m}$ SiC particles the complete closed pore was observed at 95% of theoretical density. Such a fast pore closure in the specimen containing 0.15${\mu}{\textrm}{m}$ SiC particles is likely to occur as a result of dense reaction layer formation on the specimen surface which is attributed to the high reactivity of small size particles with sintering atmosphere.

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