• Journal of the Korean institute of surface engineering
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• v.48 no.4
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• pp.169-173
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• 2015

$CuInSe_2$ thin films which have been widely used for thin solar cells as a light absorber were prepared by hydrazine solution processing, and their microstructural properties were investigated. Hydrazine $CuInSe_2$ precursor solutions were prepared by dissolving $Cu_2S$, S, $In_2Se_3$ and Se powder in hydrazine solvent. Multilayer $CuInSe_2$ chalcopyrite phase thin films were prepared by repeating spin-coating process using the precursor solution. Unfortunately, the presence of the interfaces between each $CuInSe_2$ layer formed by multi-layer coating impeded grain growth across the interface. Here, by doing simple interface engineering to solve the limited grain growth issue, the large grained (${\sim}1{\mu}m$) $CuInSe_2$ thin films were obtained.

• Journal of Adhesion and Interface
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• v.19 no.3
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• pp.123-128
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• 2018

As a mussel-inspired surface independent modification chemistry using catecholamine family molecule was suggested on 2007, there are tremendous efforts being done by researchers from around the world to adjust and develop diverse applications using catecholamine family. Accordingly, we will discuss about the novel method to extend catecholamine applications, which is through the functional group substitution of catecholamine molecules.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2015.05a
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• pp.106-106
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• 2015

In this study, we investigated electrochemically formed nanotube shape on ternary Ti-25Ta-xHf alloys with Hf contents. Ti-25Ta-xHf (x=0~15 wt.%) alloys were manufactured by vacuum arc-melting furnace. The obtained ingots were homogenized in an argon atmosphere at $1050^{\circ}C$ for 2h and then water quenching. The specimens were cut from ingots to 4 mm thickness and first ground and polished using SiC paper (grades from #100 to #2000). The anodization treatments on Ti-25Nb-xHf alloys were carried out at room temperature for experiments. The formation of nanotubular film was conducted by electrochemical method in mixed electrolytes with 1 M $H_3PO_4$ + 0.8 wt. % NaF at 30 V for 2 h. The morphologies of nanotube depended on the Hf content in Ti-25Ta-xHf ternary system.

• Journal of the Korean GEO-environmental Society
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• v.13 no.8
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• pp.65-73
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• 2012

Soil-rock interface, mainly founded in Granite region of Korea, is known as one of the important factor of the slope failure at the rainfall due to smaller shear strength than soil itself. However, research of the effect on slope stability by soil-rock interfaces is insufficient. Therefore, a series of direct shear tests were performed in order to investigate the effect of soil-rock interface on slope stability. The method of tests is to get sand itself and sand-artificial rock interface shear strength from different grain size of sands and artificial rock samples. The results of tests show that the friction angle of interface depends primarily on particle size and surface roughness. Interface friction angle ratio ${\mu}(={\delta}/{\Phi})$ is in the range of 0.75 ~ 0.96, this results indicate that interface friction angle is smaller than sand itself.

• Structural Engineering and Mechanics
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• v.23 no.1
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• pp.43-61
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• 2006

An investigation of the effectiveness of the interface treatment when column concrete jacketing is performed is presented. Alternative methods of interface connection were used in order to investigate the performance of strengthened concrete columns. These connecting techniques involved roughening the surface of the original column, embedding steel dowels into the original column and a combination of these two techniques. The experimental program included three strengthened specimens, one original specimen (unstrengthened) and one as-built specimen (monolithic). The specimens represented half height full-scale old Greek Code (1950's) designed ground floor columns of a typical concrete frame building. The jackets of the strengthened specimens were constructed with shotcrete. All specimens were subjected to displacement controlled earthquake simulation loading. The seismic performance of the strengthened specimens is compared to both the original and the monolithic specimens. The comparison was performed in terms of strength, stiffness and hysteretic response. The results demonstrate the effectiveness of the strengthening methods and indicate that the proper construction of a jacket can improve the behaviour of the specimens up to a level comparable to monolithic behaviour. It was found that different methods of interface treatment could influence the failure mechanism and the crack patterns of the specimens. It was also found that the specimen that combined roughening with dowel placement performed the best and all strengthened columns were better at dissipating energy than the monolithic specimen.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.3 no.4
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• pp.256-262
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• 1991

The corrosion effects on thermal contact resistance were experimentally studied for a given contact interface of a couple of metals. 2 cylindrically shaped test pieces, the one was carbon steel whose surface was machined by lathe and the other was stainless steel, ground, were come into contact under pressure, and then submerged to $HNO_3$ gas environment. While the corrosion process was going on, the thermal contact resistance was measured with time. The experiment was performed for 2 cases; 1) Highly compress the test pieces and then bring them to $HNO_3$ gas environment. 2) Anteriorly corrode the interface under low contact pressure and then increase the contact pressure. The results were as follows; In 1st. case of experiment, the thermal contact resistance seemed to be very stable, and showed low values with a tendancy of small decrease with time. But in 2nd. case the resistance was unstable and jumped to a value of 200-250% more then that expected for uncontaminated interface. More over it demonstrated some increase with time.

• Transactions of the Korean hydrogen and new energy society
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• v.1 no.1
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• pp.48-54
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• 1989

Semiconductive property of the passivating $TiO_2$ film was investigated by measuring the impedance of passivated titanium electrode in a 0.1 N NaOH solution. The passive film was prepared galvanostatically with $10mA/cm^2$ at formation potential of 50 V in a 1 N $H_2SO_4$ solution. The impedance measurement was conducted by superimposing an ac voltage of 5 m V amplitude with the frequency ranging from 5 to 10000 Hz on a dc bias (applied potential). The donor distribution in the film was depicted from the analysis of the non-linear slope of Mott-Schottky plot. The region with nearly constant concentration of donors near the electrolyte/film interface amounts at about 60 percent of the total film thickness and donor concentration increases largely with distance from the surface in an inner region near the film/metal interface. In a region of the film/metal interface the donor concentration showed a frequency dependence greater than in a region of the electrolyte/film interface. The result of donor concentration against frequency suggests a transition from crystalline to amorphous state with distance from the electrolyte/film interface in the passivating $TiO_2$ films. This is also confirmed by the ac conductivity measurement.

• Journal of the Korean Geotechnical Society
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• v.15 no.4
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• pp.247-260
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• 1999

It was found that surface roughness has a first-order effect on the interface shear strength and accordingly it should be accurately quantified if its role is to be properly understood. Most of the surface roughness parameters are based on the trisector approach (three dimensional parameter) which can provide a good measure of the surface roughness from a static perspective. However, if roughness is to be correlated with a directional sensitive parameter such as interface shear then a two dimensional parameter could be more meaningful if the roughness measurements are made parallel to the direction of shearing. In this paper, alternative roughness parameters which consider the direction of shearing are described. These directional parameters are compared with the existing roughness parameters, and the relationship between these directional and non-directional parameters are investigated. The surface roughness was quantified by using the Optical Profile Microscopy (OPM) method (Dove and Frost, 1996) based on the digital image analysis. The results showed that the various surface roughness parameters measured in this study exhibit similar trend of roughness values, so that, good relationships are obtained between these roughness parameters. As the surface roughness increases, the roughness values measured in trisector coupons are increasing higher than those measured in parallel coupons.

• Structural Engineering and Mechanics
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• v.48 no.1
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• pp.41-56
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• 2013

Initiation and growth of delamination is a great concern of designers of composite structures. Interface elements with de-cohesive constitutive law in the content of continuum damage mechanics can be used to predict initiation and growth of delamination in single and mixed mode conditions. In this paper, an interface element based on the cohesive zone method has been developed to simulate delaminatoin growth of post-buckled laminate under fatigue loading. The model was programmed as the user element and user material by the "User Programmable Features" in ANSYS finite element software. The interface element is a three-dimensional 20 node brick with small thickness. Because of mixed-mode condition of stress field at the delamination-front of post-buckled laminates, a mixed-mode bilinear constitutive law has been used as user material in this model. The constitutive law of interface element has been verified by modelling of a single element. A composite laminate with initial delamination under quasi-static compressive Loading available from literature has been remodeled with the present approach. Moreover, it will be shown that, the closer the delamination to the free surface of laminate, the slower the delamination growth under compressive fatigue loading. The effects of laminate configuration on delamination growth are also investigated.

• Proceedings of the Korean Vacuum Society Conference
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• 1999.07a
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• pp.183-183
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• 1999

The phases and interface formation of MgF2 on Si(111) were studied by using LEED, AES, and TPD. When thick MgF2 film was deposited on the Si(111) surface at RT뭉 annealed at higher temperatures, a sequence of LEED patterns (no LEED pattern $\longrightarrow$1$\times$1$\longrightarrow$3$\times$1$\longrightarrow$7$\times$7) was observed. On the 1$\times$1 model in which Mg adsorbs on T4 site and F on H3 site could explain the simultaneous desorption of SiF2 and Mg. When thin MgF2 film was deposited, and initial $\alpha$-$\times$1 phase transforms to 3$\times$3 and $\beta$-1$\times$1 by thermal annealing with a slow evaporation of F and diffusion of Mg into the surface. the 3$\times$3 surface changes to ${\gamma}$-1$\times$1 by the selective desorptioon of F under e-beam irradiation and subsesquently to a Mg-induced {{{{ SQRT { 3} }}}} structure by annealing at $600^{\circ}C$.