• Title/Summary/Keyword: surface and interface

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The TEM Characterization of the Interfacial Microstructure between In Solder and Au/Ni/Ti Thin Films during Reflow Process (리플로 공정 후에 형성된 In과 Au/Ni/Ti 다층 박막의 계면 구조의 TEM 분석)

  • 조원구;김영호;김창경
    • Journal of the Korean institute of surface engineering
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    • v.32 no.4
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    • pp.503-512
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    • 1999
  • The crystal structure and the microstructure of the intermetallic compounds formed in the interface between In solder and Au/Ni/Ti thin films have been investigated by XRD, SEM, and TEM. Indium solder was deposited on the Au/Ni/Ti thin films/Si substrate by evaporation. The heat treatments simulated the flip chip solder joining were performed in RTA system or in furnace. $Auln_2$ phase is formed in all specimens.$ In_{27}$ $Ni_{10}$ and/or $In_{X}$ $Ni_{Y}$ phase are formed in the interface between $Auln_2$ and Ni depending the heat treatment conditions.

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Contact Damage and Fracture of Poreclain/Glass-Infiltrated Alumina Layer Structure for Dental Application (치아 응용을 위한 /유리침윤 알루미나 이중 층상구조의 접촉손상 및 파괴)

  • 정연길;여정구;최성설
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1257-1265
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    • 1998
  • Hertzian contact tests were used to investigate the evolution of fracturedamage in the coating layer as functions of contact load and coating thickness by studying crack patterns in porcelain on glass-infiltrated alumina bilayer system conceived to simulate the crown structure of a tooth. Cone cracks initiated at the coating top surface without delamination at interface and crack propagation to substrate. Preferentially the cracks made multi-cracks at the coating top surface rather than proceeding to interface. The cracks were highly stabilized with wide ranges between the loads to initiate first cracking and to cause final failure im-plying damage-tolerant capability. Finite element modelling was used to evaluate the stress distribution. Maximum tensile stress were responsible for the cracking at the coating layer and had a profound influence on the crack pattern and fracture damage in the layered structure materials.

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Surface Mophology of Blends Containing Poly(vinylidene fluoride) on the Basis of Atomic Force Microscopy (원자력간 현미경을 이용한 Poly(vinylidene fluoride)계 고분자 블렌드의 표면 모폴로지 연구)

  • Lee, Won-Ki;Park, Chan-Young;Cho, Won-Jei;Ha, Chang-Sik
    • Journal of Adhesion and Interface
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    • v.2 no.1
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    • pp.18-22
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    • 2001
  • Surface morphology of [poly(vinylidene fluoride)/poly(methyl methacrylate)] (PVDF/PMMA) was investigated on the basis of atomic force microscopy and differential scanning calorimeter measurements. The surface of (PMMA/PVDF) and (H14-PMMA/PVDF) blend films was fully composed with PVDF crystals. Although the difference of surface free energy between PMMA and PVDF is increased with increasing carboxyl group content in PMMA, however, in the case of (H24-PMMA/PVDF) blend film surface, the existence of aggregated H-PMMA was observed. It was found that the degree of surface enrichment of the blend is more affected by the magnitude of intermolecular interaction than the surface free energy difference, Besides, the introduction of carboxyl group for miscible (PVDF/PMMA) blend decreased the miscibility in the blend.

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Evaporation Cooling of Single Droplet on a Heated Solid Surface (가열된 고체표면에 부착된 단일 액적의 증발냉각)

  • Yu, Gap-Jong;Bang, Chang-Hun;Kim, Jeong-Su
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.6
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    • pp.845-852
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    • 2001
  • The characteristics of evaporation cooling of single droplet on a heated surface were studied experimentally. The two kinds of heater modules were tested to measure cooling characteristics of metal surface (high conductivity) and Teflon surface (low-energy surface, low conductivity). The results showed that time averaged heat flux during droplet evaporation increased exponentially with initial surface temperatures of brass, copper and steel. The heat flux and evaporation time did not varied with metal conductivities. However, the temperature drop after the deposition of droplet was larger on Teflon than on the metals. Thus, the correlation of interface temperature between liquid droplet and metal surface was proposed as a function of the initial surface temperature of heating materials, which could be applied to both metal and non-metal ones.

Surface passivation study of a-Si:H/c-Si heterojunction solar cells using VHF-CVD (VHF-CVD를 이용한 a-Si:H/c-Si 이종접합태양전지 표면 패시배이션 연구)

  • Song, JunYong;Jeong, Daeyoung;Kim, Kyoung Min;Park, Joo Hyung;Song, Jinsoo;Kim, Donghwan;Lee, JeongChul
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.05a
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    • pp.128.1-128.1
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    • 2011
  • In amorphous silicon and crystalline silicon(a-Si:H/c-Si) heterojuction solar cells, intrinsic hydrogenated amorphous silicon(a-Si:H) films play an important role to passivate the crystalline silicon wafer surfaces. We have studied the correlation between the surface passivation quality and nature of the Si-H bonding at the a-Si:H/c-Si interface. The samples were obtained by VHF-CVD under different deposition conditions. The passivation quality and analysis of all structures studied was performed by means of quasi steady state photoconductance(QSSPC) methods and fourier transform infrared spectrometer(FTIR) measurements respectively.

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Shear strength of connections between open and closed steel-concrete composite sandwich structures

  • Kim, Woo-Bum;Choi, Byong Jeong
    • Steel and Composite Structures
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    • v.11 no.2
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    • pp.169-181
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    • 2011
  • The behavior of connections between open sandwich slabs and double steel skin composite walls in steel plate-concrete(SC) structure is investigated by a series of experimental programs to identify the roles of components in the transfer of forces. Such connections are supposed to transfer shear by the action of friction on the interface between the steel surface and the concrete surface, as well as the shear resistance of the bottom steel plate attached to the wall. Experimental observation showed that shear transfer in slabs subjected to shear in short spans is explained by direct force transfer via diagonal struts and indirect force transfer via truss actions. Shear resistance at the interface is enhanced by the shear capacity of the shear plate as well as friction caused by the compressive force along the wall plate. Shear friction resistance along the wall plate was deduced from experimental observation. Finally, the appropriate design strength of the connection is proposed for a practical design purpose.

A Study on the Effect of Process Parameters to Mechanical Property in Forward Extrusion of Milli-size Cylindrical Pin (밀리 단위의 원형핀 전방압출에 있어서 공정인자가 기계적 성질에 미치는 영향 연구)

  • 심경섭;김용일;이용신;김종호
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.797-801
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    • 2003
  • The mechanical properties such as shear strength and the hardness of milli-size products that manufactured for various process parameters by forward extrusion using square dies are investigated. Shear strength test is implemented for the observation of relation between vickers hardness and shear strength in the interface of head and shaft part of a stepped pin. When the extrusion ratios of pure aluminum and pure copper billets increase, the hardness on both the surface and the center line of a pin also increase, especially the hardness on the surface is shown to be a little higher than on the center. The existence of knock-out pad in extrusion die caused hardness increase in the interface of a extruded pin. As compared shear strength with hardness of a pin, the approximated linear relations are suggested in this study.

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The Development of a Miniature Humanoid Robot System (소형 휴머노이드 로븟 시스템 개발)

  • 성영휘;이수영
    • 제어로봇시스템학회:학술대회논문집
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    • 2000.10a
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    • pp.43-43
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    • 2000
  • In this paper, we introduce a case study of developing a miniature humanoid robot that has 16 degrees of freedom and is able to perform statically stable walking. The developed humanoid robot is 37cm tall and weighs 1,200g. RC servo motors are used as actuators. The robot can walk forward and turn to any direction on even surface. It equipped with a small digital camera, so it can transmit vision data to a remote host computer via wireless modem. The robot can be operated in two modes; One is a remote-controlled mode, in which the robot behaves according to the command given by a human operator through the user-interface program running on a remote host computer, the other is a stand-alone mode, in which the robot behaves autonomously according to the pre-programmed strategy. The user-interface program also contains a robot graphic simulator that is used to produce and verify the robot's gait motion. In our walking algorithm, the ankle joint is mainly used lot balancing the robot. The experimental results shows that the developed robot can perform statically stable walking on even surface.

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Zn/HA Coating on the Ti-xNb Alloys after Nanotube Formation for Dental Implant

  • Byeon, In-Seop;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.11a
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    • pp.139-140
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    • 2015
  • Zn/HA coating on the Ti-xNb alloys after nanotube formation for dental lmplant was researched using various experimental methods. Due to g ood biocompatibility and osteoconductivity, hydroxyapatite (HA) coating s on metallic biomedical implants were widely employed in orthopedic and dental applications. To improve biocompatibilities, Zinc (Zn) plays very important roles in the bone formation and immune reg ulations. The nanotube formed Zn-HA films were characterized with X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), energy dispersive X-ray spectroscopy (EDS).

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Corrosion Behaviors of Ti-xNb Alloys for Biomaterials

  • Byeon, In-Seop;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.186-186
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    • 2014
  • In this study, corrosion behaviors of Ti-xNb alloys for biomaterials. The Ti-xNb binary alloys contained from 10 wt. % to 50 wt. % contents were manufactured by vacuum arc-melting furnace. Microstructures of the alloys were examined by optical microscope (OM) and field emission scanning electron microscope (FE-SEM). In order to identify the phase constitutents of the Ti-xNb alloys, X-ray diffractometer (XRD) with a Cu K radiation was used. The corrosion behaviors were investigated using potentiostat (Model2273,EG & GCo, USA) in NaCl solution at $(36.6{\pm}1.0)^{\circ}C$.

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