• 제목/요약/키워드: superficial velocity

검색결과 129건 처리시간 0.028초

액체 크로마토그래피에 의한 메틸프룩토시드의 분리공정 연구 (A Study on the Purification Process of Methyl Fructoside by Liquid Chromatography)

  • 허주형;유인상김해성
    • KSBB Journal
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    • 제11권5호
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    • pp.529-535
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    • 1996
  • 효소적으로 합성된 메틸프룩토시드(methyl fruc­t to side )와 당의 혼합물로부터 Amberlite IRA -900 을 고정상 담체로 하여 당과 배당체를 액체 크로마 토그래피법으로 정밀 분리함으로써 메틸프룩토시드 를 출발물질로 하는 새로운 sugar ester의 합성 공 정이 연구개발되도록 하고, 액체 크로마토그래피법 에 의한 알킬배당체의 정밀 분리기술이 실용화될 수 있도록 최적조업조건과 해상도 빛 생산성을 검토하였다. Amberlite IRA-900을 고정상 담체로 한 메틸프 룩토시드의 정밀분리공정은 이론단수의 개념에 근거 한 선형 크로마토그래피 모델로 모사할 수 있었으며 에틸프룩토시드와 자당의 용출 크로마토그램을 잘 예측할 수 있었다. 급액농도가 각각 3g/L와 5g/L 인 메틸프룩토시드와 자당의 수용액으로부터 메틸프 룩토시드를 정밀분리하기 위해서는 급액을 $60^{\circ}C$에서 충전체적의 75%까지 주입하고공탑유속 1.13cm/mm의 중류수로 용출시킬 때 해상도 1.1에서 95% 이상의 회수율과 7mg MF/g-resin/h의 생산성을 얻었다.

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해수 조건에서 모래유동층 여과조의 TAN 부하량과 수온에 따른 질산화 효율 (Nitrification Efficiency of the Fluidized Sand Biofilter by TAN Leading Rates and Temperatures in the Simulated Seawater Aquaculture Condition)

  • 박정환
    • 한국수산과학회지
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    • 제38권6호
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    • pp.347-352
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    • 2005
  • These experiments investigated the conditioning pattern and the nitrification efficiency of a fluidized sand biofilter (FSB) for seawater application. The FSB fed artificial nutrient was fully conditioned within 22 weeks. The maximum nitrification efficiency of the FSB was achieved at a superficial water velocity (SWV) of 1.0 cm/sec. After fixing the superficial water velocity at 1.0 cm/sec, the nitrification rates of the FSB were assessed at 3 total ammonia nitrogen (TAN) loading rates (250, 500, 1,000 g TAN/$m^3$/day) and 3 water temperatures (12, 16, $20^{\circ}C$). The TAN concentration in the simulated culture tank ranged from 2.87 to 9.72 mg/L at TAN loading rate of 1,000 g TAN/$m^3$/day, while that ranged from 0.45 to 1.26 mg/L at TAN loading rate of 500 g TAN/$m^3$/day. The ranges of TAN concentration in the former were too high for aquatic organisms and those in the latter were acceptable. Therefore, the safe TAN loading rate for the FSB in seawater conditions was decided as 500 g TA/$m^3$/day. From these results, daily TAN removal rates (g TAN/$m^3$/day) of FSB under conditions of inlet TAN concentration (C, mg/L) and water temperature (T, $^{\circ}C$) were calculated by the following non-linear multi-regression equation: TAN removal rate: f(z)=-1,311.295+655.714LnT+225.775LnC ($r^2=0.962$).

해수 포말분리공정의 해석 및 모델 (Modeling of Foam Separator for Sea Water Treatment)

  • 허현철;서재관;박은주;김성구
    • 한국수산과학회지
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    • 제32권2호
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    • pp.165-169
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    • 1999
  • 포말분리 장치를 이용한 해수 중의 단백질 제거 특성을 조사한 결과, 단백질 농도가 높을 수록 또한 폭기량이 높을수록 단백질의 제거속도는 증가하는 것으로 나타났다. 이러한 각각의 제거특성을 통계학적으로 비선형 회귀분석하여 각각의 인자의 변화에 따른 단백질 농도의 변화를 다음의 식으로 나타낼 수 있었다. $$f\;(Co,\;u)=1.5712\times10^{-7}\timesCo^{3.061}\timesu^{1.258}$$ 위 식을 이용하여 유한차분법으로 시뮬레이션을 수행한 결과 실제 포말분리 운전에서 나타난 결과와 상관성이 아주 높은 결과를 얻을 수 있었다.

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휜이 있는 협소 사각 유로에서 대향류 기/액 2상 유동 (Counter-Current Gas-Liquid Two-Phase Flow in Narrow Rectangular Channels with Offset Strip Fins)

  • 손병후;김병주;정시영
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 춘계학술대회논문집E
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    • pp.229-234
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    • 2001
  • An adiabatic counter-current vertical two-phase flow of air and water in narrow rectangular channels with offset strip fm was investigated experimentally. Tests were systematically performed with downward liquid superficial velocities and upward gas velocities covering 0 to 0.06 m/s and 0 to 2.5 m/s ranges, respectively. Two-phase flow regimes were classified by examining the video images of flow patterns in transparent test sections of 760 mm long and 100 mm wide channel with gaps of 3.0 and 5.0 mm. The channel average void fraction was measured by the quick-closing valve method. Unlike the flow regimes in the channels without fin, where bubbly, slug, chum, and annular flow were identified, only bubbly and chum flow regimes were found for the channels with offset strip fin. However the existence of fin in the channels showed negligible effects on the void fraction. Instead counter-current flow limitations were found to happen at lower air superficial velocity once offset strip fin was introduced in narrow rectangular channels.

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실험실 규모 순환유동층 연소로에서 2차공기 주입이 냉간유동에 미치는 영향 (Secondary Air Injection Effect on Cold Flow in a Laboratory-scale Circulating Fluidized Bed Combustor)

  • 장석돈;라승혁;황정호;강경태
    • 한국연소학회:학술대회논문집
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    • 한국연소학회 2000년도 제21회 KOSCO SYMPOSIUM 논문집
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    • pp.217-228
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    • 2000
  • Circulating Fluidized Bed Combustor(CFBC) has been used for the incineration of waste sewage sludge and for the power generation. In this study hydrodynamic characteristics of two phase flow have been studied in a riser section of CFBC. A lab-scale riser is designed and SiC (Geldart type B) is used for solid particles. Experiments are performed by controlling the fluidization parameters including superficial velocity and secondary air to primary air ratio for determination of solid holdup profiles in the riser. Superficial velocities of each fluidization regime are well agreed with results predicted by a theoretical model. The results show that the axial solid holdup distributions calculated by measuring differential static pressures in the riser are found to show a basic profile described by a simple exponential function. Our flow regime during experiments mainly belongs to fast fluidization regime for particle size of 300${\mu}m$. As the SA/PA ratio increases, solid holdup in the lower dense region of the riser increases.

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순환유동층 소각로의 수력학적 특성에 관한 연구 (Hydrodynamic Characteristics of Circulating Fluidized Bed Incinerator)

  • 변영철;박선호;황정호;김세원
    • 한국연소학회:학술대회논문집
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    • 한국연소학회 1999년도 제19회 KOSCO SYMPOSIUM 논문집
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    • pp.173-182
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    • 1999
  • Internally Circulating Fluidized Bed Combustor(ICFBC) has been used for the incineration of waste sewage sludge. In this study hydrodynamic characteristics of two phase flow have been studied in a riser section of ICFBC. A lab-scale riser(l/5 scale of pilot plant) is designed and SiC (Geldart type B) is used for solid particles. Experiments are performed by controlling the fluidization parameters including superficial velocity, particle diameter and secondary air to primary air ratio for determination of solid holdup profiles in the riser. Our flow regime during experiments mainly belongs to the onset of turbulent regime(for d_{p}:300{\mu}m) and fast fluidization regime(for d_{p}:100{\mu}m). Superficial velocities of each regime are well agreed with results obtained by other researches. The results show that the axial solid holdup distributions calculated by measuring differential static pressures in the riser are found to show a basic profile described by a simple exponential function. As the particle size decreases, solid holdup along the riser is more uniformly distributed. To prove these experimental results, numerical calculations are being performed.

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Two-Phase Flow Regimes for Counter-Current Air-Water Flows in Narrow Rectangular Channels

  • Kim, Byong-Joo;Sohn, Byung-Hu;Siyoung Jeong
    • Journal of Mechanical Science and Technology
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    • 제15권7호
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    • pp.941-950
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    • 2001
  • A study of counter-current two-phase flow in narrow rectangular channels has been performed. Two-phase flow regimes were experimentally investigated in a 760mm long and 100mm wide test section with 2.0 and 5.0mm gap widths. The resulting flow regime maps were compared with the existing transition criteria. The experimental data and the transition criteria of the models showed relatively good agreement. However, the discrepancies between the experimental data and the model predictions of the flow regime transition become pronounced as the gap width increased. As the gap width increased the transition gas superficial velocities increased. The critical void fraction for the bubbly-to-slug transition was observed to be about 0.25. The two-phase distribution parameter for the slug flow was larger for the narrower channel. The uncertainties in the distribution parameter could lead to a disagreement in slug-to-churn transition between the experimental findings and the transition criteria. For the transition from churn to annular flow the effect of liquid superficial velocity was found to be insignificant.

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벤치규모 가압유동층연소로에서 석회석에 의한 국내무연탄의 탈황특성 (Desulfurization Characteristics of Domestic Anthracite by Limes at Bench Scale Pressurized Fluidized Bed Combustor .)

  • 한근희;류정인;진경태
    • 대한기계학회논문집B
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    • 제25권10호
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    • pp.1373-1383
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    • 2001
  • The desulfurization characteristics of anthracite in a bench scale pressurized fluidized bed combustor are investigated. The coal used in the experiment is domestic anthracite from Kangwon Taeback area. The desulphurization experiment is performed with limestone from Chungbuk Danyang. The pressure of the combustor is maintained at 6 atm, and the combustion temperatures are 850, 900, and 950$\^{C}$. The superficial gas velocities are 0.9, 1.1, and 1.3 m/s. The excess air ratio is varied from 5 to 35%. The Ca/S mole ratios are 0.5, 1.5, 2.5 and 4.5 mole. All experiments are executed at 2m bed height. Consequently, SO$_2$ concentration in the flue gas is increased with incresing bed temperature and superficial gas velocity. However SO$_2$ concentration is decreased with incresing excess air ratio and Ca/S mole ratio.

비비등 선회유동에서의 2상 대류열전달 증가 (Two phase convective heat transfer augmentation in swirl flow with non-boiling)

  • 차경옥;김재근
    • 대한기계학회논문집
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    • 제19권10호
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    • pp.2586-2594
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    • 1995
  • Two phase flow phenomena are observed in many industrial facilities and make much importance of optimum design for nuclear power plant and various heat exchangers. This experimental study has been investigated the classification of the flow pattern, the local void distribution and convective heat transfer in swirl and non-swirl two phase flow under the isothermal and nonisothermal conditions. The convective heat transfer coefficients in the single phase water flow were measured and compared with the calculated results from the Sieder-Tate correlation. These coefficients were used for comparisons with the two-phase heat transfer coefficients in the flow orientations. The experimental results indicate, that the void probe signal and probability density function of void distribution can used into classify the flow patterns, no significant difference in voidage distribution was observed between isothermal and non-isothermal condition in non-swirl flow, the values of two phase heat transfer coefficients increase when superficial air velocities increase, and the enhancement of the values is observed to be most pronounced at the highest superficial water velocity in non-swirl flow. Also two phase heat transfer coefficients in swirl flow are increased when the twist ratios are decreased.

외부 순환 공기리프트 반응기의 동특성 (Dynamic Characteristics of External loop Air-Lift Reactor)

  • 강귀현;김춘영정봉우
    • KSBB Journal
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    • 제7권1호
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    • pp.59-65
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    • 1992
  • 외부 순환식 공기리프트 반응기에서 기상유속과 액상의 점도를 변수로 하여 기체체류량과 액체의 순환시간, 혼합시간, 순환속도 및 축방향분산계수를 측정하여 다음과 같은 결론을 얻었다. 1. 기체체류량은 기체유속이 증가함에 따라 증가 하였으며, 점도가 증가함에 따라서는 약간 감소하는 경향을 보였다. 또 기체유속이 증가함에 따라 상승관에서는 기체체류량의 증가율이 감소한 반면 하강관에서는 증가하였다. 2. 기체유속이 증가함에 따라 순환시간 및 혼합시간은 초기에 급격히 짧아지다가 거의 일정한 값을 나타내었으며, 액체의 점도가 증가함에 따라 순환기산과 혼합시간은 모두 증가하였다. 3. 순환 액체의 속도는 기체의 속도에 따라 초기에 급격히 증가하나 기체속도가 약 5cm/sec이상이 되면 그 증가율이 매우 둔화되었으며, 점도가 증가함에 따라 약간 감소함을 알 수 있었다. 또한 압력수지식으로 예측한 이론값과 실험값은 낮은 기체유속 영역에서는 잘 일치하였으나 기체유속이 증가함에 따라 실험값이 이론값보다 작은 값을 나타내었다. 4. 기체유속이 증가함에 따라 Bodenstein number는 감소하였고, 축방향분산계수는 증가하였으며, 점도가 증가함에 따라 약간 감소하는 경향을 보였다. 본 실험범위에서 분산이 많이 일어나mixed folw에 근접함을 알 수 있었다.

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