• 한국진공학회:학술대회논문집
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• 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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• pp.107.1-107.1
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• 2014

We have developed and commercialize a time-of-flight - medium energy ion scattering spectrometry (TOF-MEIS) system (model MEIS-K120). MEIS-K120 adapted a large solid acceptance angle detector that results in high collection efficiency, minimized ion beam damage while maintaining a similar energy resolution. In addition, TOF analyzer regards neutrals same to ions which removes the ion neutralization problems in absolute quantitative analysis. A TOF-MEIS system achieves $7{\times}10^{-3}$ energy resolution by utilizing a pulsed ion beam with a pulse width 350 ps and a TOF delay-line-detector with a time resolution of about 85 ps. TOF-MEIS spectra were obtained using 100 keV $He^+$ ions with an ion beam diameter of $10{\mu}m$ with ion dose $1{\times}10^{16}$ in ordinary experimental condition. Among TOF-MEIS applications, we report the quantitative compositional profiling of 3~5 nm CdSe/ZnS QDs, As depth profile and substitutional As ratio of As implanted/annealed Si, Ionic Critical Dimension (CD) for FinFET, Direct Recoil (DR) analysis of hydrogen in diamond like carbon (DLC) and InxGayZnzOn on glass substrate.

• 한국안전학회지
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• 제28권1호
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• pp.12-17
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• 2013

Considering the wind power system and the rotor blades which are composed of much technology, the wind power blade would be the most dangerous part because it revolves at high speed and weighs about dozens of tons, if the accident happens. Therefore, the light weight composite materials have been replacing as substitutional materials. The object of this study is to examine the delamination and damage for CFRP/GFRP hybrid composite that is used for strength improvement of a wind power blade. The influence of the initial crack length and fiber orientation for the interlaminar delamination was exposed for the blade safety. Plain woven CFRP instead of GFRP was inserted into the layer of the box spar for improving the strength and blade life. DCB(Double Cantilever Beam) specimen was used for evaluating fracture toughness and damage evaluation of interlaminar delamination. The material used in the experiment is a commercial material known as CF 3327 EPC in plain woven carbon prepreg(Hankuk Carbon Co.) and UD glass fiber prepreg(Hyundai Fiber Co.). From the results, crack growth rate is not so different according to the variation of the initial crack length. Mode I interlamainar fracture toughness of fiber direction $0^{\circ}$ is higher than that of $45^{\circ}$. Interlaminar fracture has an effect on fiber direction and K decreased with lower value according to increasing initial crack length. Also energy release rate fracture toughness was evaluated because CFRP/GFRP hybrid composite with a different thickness is under the mixed mode loading condition. The interlaminar fracture was almost governed by mode I fracture even though the mixed mode.

• 열처리공학회지
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• 제24권6호
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• pp.318-326
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• 2011

This study has been performed to investigate the effect of Al addition on High Temperature Gas Nitriding (HTGN) in 13%Cr-0.16%C stainless steel with different Al contents of 0.54%, 1.76% and 2.36%, respectively. HTGN treatment was carried out at $1100^{\circ}C$ for 1 hr, 5 hrs and 10 hrs. Nitrogen-permeated surface layers showed round type carbides of $Cr_{23}C_6$ and needle type nitrides of AlN in the matrix of martensite, representing 600~700 Hv. And the thickness of the surface layer increased with increasing Al content and HTGN treatment time. The inner region that was not permeated nitrogen showed chromium carbides in the mixed phase of martensite and ferrite for the 0.53% Al alloyed steel, however chromium carbides in the matrix of ferrite single phase were shown for the steels with the addition of 1.76%Al and 2.36%Al, representing the hardness of ~200 Hv. During nitrogen permeation from surface to the interior, substitutional elements of Cr, Al and Si moved toward the surface and interstitial element of carbon also moved from interior to the surface. This movement of alloying elements leads high concentration of these elements at the outmost surface, subsequently the lowest peak of substitutional elements were shown in the vicinity of near surface. After showing the lowest peak, the high concentration region of Al and C were formed due to the continuous movement of Al toward the surface. The long discontinuous precipitates of $Cr_{23}C_6$ and AlN were formed along the outmost surface owing to the high concentration of these alloying elements.

• 생명과학회지
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• 제12권2호
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• pp.129-135
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• 2002

여러 종류의 호열성, 호기성 간균(Bacillus genus)군, 중금속 leaching 미생물군(Thiobacillus, T. ferooxidans), 그리고 여러 가지 난분해성 물질을 분해하는 미생물군 (Pseudomonas genus)을 활용하여 퇴비화의 조건을 연구하고 이를 이용하여 축산폐기물의 퇴비화에 미치는 효과를 연구하였다. 35∼40의 C/N비, 50∼65%의 함수율 범위에서 실험실용 회전드럼형 반응조에서의 퇴비화는 온도상승이 수동식 반응조보다 낮으며 느리게 일어났다. 퇴비화 후 성분분석에서 높은 수준의 광물질을 함유하는 것으로 화학비료 대체효과를 보여주며 퇴비화 전후 중금속 분석에서 As는 모든 퇴비에서, Cr은 돈분, ph은 축분, Hg은 계분, 그리고 Cu는 축분퇴비에서 규제값 이하를 보여주었다. 여러 가지 부숙도 분석에서 퇴비의 숙성도를 나타내었다. SS 또는 EMB agar plate을 이용한 살모넬라균과 대장균의 검사에서 병원균에 대한 퇴비의 안전성이 확인되었다. 이러한 결과는 금속 및 다른 난분해성 물질을 생분해하는 미생물을 투입하여 퇴비의 중금속감소와 퇴비화 속도증가의 가능성을 시사한다.

• Metals and materials international
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• 제24권6호
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• pp.1193-1201
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• 2018

Dilatometry is a useful technique to obtain experimental data concerning transformation. In this paper, a dilation conversional model was established to calculate carbides fraction in AISI H13 hot-work tool steel based on the measured length changes. After carbides precipitation, the alloy contents in the matrix changed. In the usual models, the content of carbon atoms after precipitation is considered as the only element that affects the lattice constant and the content of the alloy elements such as Cr, Mo, Mn, V are often ignored. In the model introduced in this paper, the alloying elements (Cr, Mo, Mn, V) changes caused by carbides precipitation are incorporated. The carbides were identified using scanning electron microscope and transmission electron microscope. The relationship between lattice constant of carbides and temperature are measured by high-temperature X-ray diffraction. The results indicate that the carbides observed in all specimens cooled at different rates are V-rich MC and Cr-rich $M_{23}C_6$, and most of them are V-rich MC, only very few are Cr-rich $M_{23}C_6$. The model including the effects of substitutional alloying elements shows a good improvement on carbides fraction predictions. In addition, lower cooling rate advances the carbides precipitation for AISI H13 specimens. The results between experiments and mathematical model agree well.