• Title/Summary/Keyword: structure analysis method

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Detection of Undeclared Betamethasone Derivatives in Cosmetic Products Labeled to Contain Zinc Pyrithione as the Active Ingredient (아연피리치온을 유효성분으로 표기한 화장품류에서 미표기 성분인 베타메타손 유도체의 검출)

  • Lee, Jeong-Pyo;Park, Sung-Hwan;Yang, Seong-Jun;Kim, Sun-Mi;Son, Kyung-Hun;Yun, Mi-Ok;Choi, Sang-Sook
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.35 no.1
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    • pp.11-17
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    • 2009
  • Betamethasone propionate, an anti-inflammatory glucocorticosteroid, was detected in cosmetics with no indication on the label of this compound as an ingredient. The product was formulated as a topical spray or shampoo and labeled to contain zinc pyrithione as the active ingredient. A thin-layer chromatographic analysis was carried out on silica gel plates to provide a first indication about the presence of a compound with steroid structure and reactivity; then high-performance liquid chromatography (HPLC) separation allowed the identification of the corticosteroid agent and its quantification. To identify the corticosteroid agent from these commercial samples we collected the fractions suspected to have ketol steroids by prep HPLC and identified the compound as betamethasone propionate by NMR and MS spectrometry. Then we synthesized the standard for the betamethasone 17-propionate and 21-propionate and quantitate the corticosteroids from the sample by HPLC with that standards. By this method we identified the corticosteroid compounds from some commercial cosmetics such as zinc pyrithione sprays. The finding of betamethasone propionate in the products was shown by comparison to an authenticated standard of betamethasone propionate by retention time on reverse-phase HPLC. Two of the tested products contained betamethasone propionate at the levels of 0.005 ${\sim}$ 0.02% and the others were free of betamethasone propionate.

Development of a River Maintenance Management Technology Related with National River Management Data (국가하천관리자료와 연계한 하천유지관리 기술개발)

  • Jo, Myung-Hee;Kim, Kyung-Jun;Kim, Hyun-Jung
    • Journal of the Korean Association of Geographic Information Studies
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    • v.15 no.1
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    • pp.159-171
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    • 2012
  • This study has developed a technology for river basin including the management of the data related with riverbed and the analysis of the riverbed maintenance based on the high-resolution imagery data and LiDAR (Light Detection and Raging) in order to enhance the utilization of river management by using RIMGIS(River Information Management GIS) and to acquire the advanced operation for river management. Using the detailed river topographical map specially designed in the form of LiDAR or high-resolution images, riverbed data and river bank channel information that are dynamically changed were informationized and established in the RIMGIS DB. At this stage, a monitoring techniques that is established in the river management system associated with RIMGIS and minimized the impact of riverbed maintenance (fluctuations) has been studied. In addition, functions and data structure of RIMGIS containing the information of geography and management of the river have been supplemented to make an improvement of the real-time management of the river. Furthermore, a technology that is capable of supplementing RIMGIS has been developed, making it feasible to maintain the river in use of structural method including an structural scheme of cross-section of the river by providing the information of riverbed and cross-section of the river. This is considered to solve an issue of insufficient data on accuracy and based on a lack of information of the river based on the two-dimensional lines, making it feasible to (steadily) improve the function of RIMGIS and to operate management tasks. Therefore, it is highly expected to enhance aforementioned technology of the river information management as a great foundation that maximizes the utilization of the river management to support RIMGIS for the development of national river management data.

A Study of e-Textbook Format Standardization Scheme for Smart Education Circumstance (스마트 교육환경을 위한 e-교과서 포맷 표준화 방안 연구)

  • Sohn, Won-Sung;Lim, Soon-Bum;Kim, Jae-Kyung
    • Journal of The Korean Association of Information Education
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    • v.16 no.3
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    • pp.327-336
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    • 2012
  • The Korea government has recently announced "A Master Plan for Smart Education", including application of digital textbooks and composition of education system using cloud computing. Our education system in future circumstance, over the conventional e-learning methods, needs the smart education solutions which enable students to study and communicate on various types of devices. The ongoing government project related with the digital textbook has been performed as mid- and long-term goals, whereas PDF-based e-textbook project, similar to e-book model and, has been already completed for the short-term goal. For the purpose of improved future smart education circumstance, however, a specific strategy is required in the following areas: flexibility of format conversion and independency of original text sources among the multiple device platforms. Therefore, in this paper, we propose a standardization scheme for e-textbook format based on e-book structure. To do this, we survey trends in e-book technologies, and research on standardization of e-book format for digitalization of textbooks, based on the analysis of existing textbooks. Moreover, we produce an example e-book content using our proposed standard method. As a result, our approach can be applied to the future smart education circumstance, and we may say that it will be efficiently applicable to the long-term digital textbook project.

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Edge-based spatial descriptor for content-based Image retrieval (내용 기반 영상 검색을 위한 에지 기반의 공간 기술자)

  • Kim, Nac-Woo;Kim, Tae-Yong;Choi, Jong-Soo
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.42 no.5 s.305
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    • pp.1-10
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    • 2005
  • Content-based image retrieval systems are being actively investigated owing to their ability to retrieve images based on the actual visual content rather than by manually associated textual descriptions. In this paper, we propose a novel approach for image retrieval based on edge structural features using edge correlogram and color coherence vector. After color vector angle is applied in the pre-processing stage, an image is divided into two image parts (high frequency image and low frequency image). In low frequency image, the global color distribution of smooth pixels is extracted by color coherence vector, thereby incorporating spatial information into the proposed color descriptor. Meanwhile, in high frequency image, the distribution of the gray pairs at an edge is extracted by edge correlogram. Since the proposed algorithm includes the spatial and edge information between colors, it can robustly reduce the effect of the significant change in appearance and shape in image analysis. The proposed method provides a simple and flexible description for the image with complex scene in terms of structural features of the image contents. Experimental evidence suggests that our algorithm outperforms the recently histogram refinement methods for image indexing and retrieval. To index the multidimensional feature vectors, we use R*-tree structure.

Optical properties of $Ag_2CdSnSe_4$ and $Ag_2CdSnSe_4:CO^{2+}$ single crystals ($Ag_2CdSnSe_4$$Ag_2CdSnSe_4:Co^{+2}$단결정의 광학적 특성)

  • 이충일
    • Journal of the Korean Vacuum Society
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    • v.10 no.1
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    • pp.16-21
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    • 2001
  • Optical properties of $Ag_2CdSnSe_4$ and $Ag_2CdSnSe_4:Co^{+2}$ quaternary semiconductor single crystals grown by the chemical transport reaction method were investigated. The analysis of the X - ray powder diffraction measurements showed that these crystals have a wurtzite structure with lattice constants a = 4.357 $\AA$, c = 7.380 $\AA$, for $Ag_2CdSnSe_4$ and a = 4.885 $\AA$, c = 7.374 $\AA$, for $Ag_2CdSnSe_4:CO^{2+}$. The direct band gap at 298K, obtained from the optical absorption measurement, is found to be 1.21 eV for $Ag_2CdSnSe_4$ and 1.02 eV for $Ag_2CdSnSe_4:CO^{2+}$. The shrinkage of the band gap due to Co-doping is observed and is about 190 meV, We observed four absorption bands of $Co^{2+}$ ions in two near infrared regions of optical absorption spectra of $Ag_2CdSnSe_4$:$Co^{+2}$. These absorption bands were assigned as due to electronic transitions between the split energy levels of $Co^{2+}$ ions in $T_d$ crystal field under spin-orbit interactions.

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Effect of the Head Support on a Change in Muscle Thickness for Longus Colli and Sternocleidomastoid During Cranio-Cervical Flexion Test in Subjects With Forward Head Posture (앞쪽머리자세를 가진 대상자의 머리-목 굽힘 검사 시 머리받침 유무에 따른 긴목근과 목빗근의 근두께 변화량 비교)

  • Park, Jun-sang;Song, Si-jeong;Jung, Hee-seok;Kwon, Oh-yun
    • Physical Therapy Korea
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    • v.23 no.3
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    • pp.11-20
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    • 2016
  • Background: A forward head posture (FHP) is one of the most common types of poor head posture in patients with neck disorder. A prolonged FHP might increase pressure on the posterior cranio-cervical structure and exhibit reduced performance on a cranio-cervical flexion test (CCFT). CCFT is included to activate deep cervical flexor muscles and inhibit excessive activation of superficial cervical flexor muscles. Therefore, the selective activation of deep cervical flexors is needed for effective exercise for FHP. Objects: The purpose of this study was to compare muscle thickness between longus colli (Lco) and sternocleidomastoid (SCM) using ultrasonography in subjects with FHP depending on head support. Methods: This was a cross-sectional, case-control research design study. The ultrasonographic images of Lco and SCM were taken in 17 subjects with FHP during the 5 phases of the CCFT with and without a head support. Towel was used for supporting head to make the neutral head position in supine. Changes in muscle thickness during the test were calculated to infer muscle activation. Data were analyzed using repeated measures of two-way analysis of variance with the significance level of .05. Results: When subjects performed the CCFT with head support, there was a significant difference in muscle thickness of Lco and SCM (p<.05). According to a post hoc paired t-test, change of thickness of Lco was greater at all phases, and change of thickness of SCM muscle was less at phase 4 and 5 in condition with head support (p<.01) compared to condition without head support (p<.01). Conclusion: The result of this study suggest that applying head support for neutral head position during CCFT could be a useful method for activating Lco muscle without excessive activation of SCM muscle.

Characteristics of vegetation succession on the Pinus thunbergii forests in warm temperate regions, Jeju Island, South Korea

  • Hong, Yongsik;Kim, Euijoo;Lee, Eungpill;Lee, Seungyeon;Cho, Kyutae;Lee, Youngkeun;Chung, Sanghoon;Jeong, Heonmo;You, Younghan
    • Journal of Ecology and Environment
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    • v.43 no.4
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    • pp.438-453
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    • 2019
  • Background: To investigate the trends of succession occurring at the Pinus thunbergii forests on the lowlands of Jeju Island, we quantified the species compositions and the importance values by vegetation layers of Braun-Blanquet method on the Pinus thunbergii forests. We used multivariate analysis technique to know the correlations between the vegetation group types and the location environmental factors; we used the location environment factors such as altitudes above sea level, tidal winds (distance from the coast), annual average temperatures, and forest gaps to know the vegetation distribution patterns. Results: According to the results on the lowland of Jeju Island, the understory vegetation of the lowland Pinus thunbergii forests was dominated by tall evergreen broad-leaved trees such as Machilus thunbergii, Neolitsea sericea, and Cinnamomum japonicum showing a vegetation group structure of the mid-succession, and the distribution patterns of vegetation were determined by the altitudes above sea level, the tidal winds on the distance from the coast, the annual average temperatures, and the forest gaps. We could discriminate the secondary succession characteristics of the Pinus thunbergii forests on the lowland and highland of Jeju Island of South Korea. Conclusions: In the lowland of Jeju Island, the secondary succession will progress to the form of Pinus thunbergii (early successional species)→Machilus thunbergii, Litsea japonica (mid-successional species)→Machilus thunbergii (late-successional species) sequence in the temperate areas with strong tidal winds. In the highland of Jeju Island, the succession will progress to the form of Pinus thunbergii (early successional species)→Neolitsea sericea, Eurya japonica (mid-successional species)→Castanopsis sieboldii (late-successional species) sequence in the areas where tidal winds are weak and temperatures are relatively low. However, local differences between lowland and highland of Jeju Island will be caused by the micro-environmental factors resulting from the topographic differences and the supply of tree seeds. From the characteristics of succession study, we could properly predict and manage the Pinus thunbergii forest ecosystem on lowland and highland of Jeju Island.

The Joint Determination of Leverage and Debt Maturity (레버리지와 부채만기 결정의 상호관계)

  • Kim, Chi-Soo;Kwon, Kyeung-Taek
    • The Korean Journal of Financial Management
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    • v.22 no.1
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    • pp.1-36
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    • 2005
  • In this study, we analyzed determinant factors of leverage ratio and debt maturity for Korean firms in the simultaneous equation system using 2SLS (two stage least square) method under assumption that two variables are jointly determined in the capital structure decision. As a result of the analysis, we found that leverage ratio and debt maturity are positively related. Also, as for determinant factors of debt maturity, agency cost hypothesis, asset maturity matching hypothesis, signalling and liquidity risk hypothesis are all generally supported, and further leverage ratio are significantly positively related with firm size, but negatively related with default risk. However, when we divided samples into groups according to bank debt level and Chaebul affiliation, with contrast to existing study which worked on similar issues with OLS, we found no evidence supporting the argument that the information asymmetry problem is less severe in firms with more bank debt, whereas information asymmetry and financial constraint problems are more severe in non-Chaebul affiliated firms.

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Numerical Analysis of Bragg Reflector Type Film Bulk Acoustic Wave Resonator (수치적 계산을 이용한 Bragg Reflector형 탄성파 공진기의 특성 분석)

  • 김주형;이시형;안진호;주병권;이전국
    • Journal of the Korean Ceramic Society
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    • v.38 no.11
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    • pp.980-986
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    • 2001
  • Bragg reflector type FBAR was fabricated on the Si(100) substrate. We measured a frequency response of the resonator at 5.2 GHz and analyzed it by numerical calculation considering actual acoustic losses of each layer in the structure. We fabricated nine layer Bragg reflector of W-SiO$_2$pairs using r.f. sputtering method and fabricated AlN piezoelectric and Al electrodes using pulsed dc sputtering. The return loss(S$_{11}$) of the fabricated Bragg reflector type FBAR was 12 dB at 5.38 GHz and the series resonance frequency(f$_{s}$) was 5.376 GHz and the parallel resonance frequency(f$_{p}$) was 5.3865 GHz. Effective electro-mechanical coupling constant (K$_{eff{^2}}$) and Quality factors(Q$_{s}$), the Figures of Merit of the resonator, were about 0.48% and 411, respectively. We extracted acoustic parameters of AlN piezoelectric and reflection coefficient of the Bragg reflector by numerical calculation. We could know that material acoustic impedance and wave velocity of AlN piezoelectric decreased for intrinsic value and the electromechanical coupling constant(K$_2$) value was very low owing to the poor quality of the AlN piezoelectric. Reflection coefficient of Bragg reflector was 0.99966 and reflection band was very wide from 2.5 to 9.5 GHz.

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Estimation of Leaf Area, Leaf Fresh Weight, and Leaf Dry Weight of Irwin Mango Grown in Greenhouse using Leaf Length, Leaf Width, Petiole Length, and SPAD Value (엽장, 엽폭, 엽병장 및 SPAD 값을 이용한 온실 재배 어윈 망고의 엽면적, 엽생체중과 엽건물중 추정)

  • Jung, Dae Ho;Cho, Young Yeol;Lee, Jun Gu;Son, Jung Eek
    • Journal of Bio-Environment Control
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    • v.25 no.3
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    • pp.146-152
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    • 2016
  • Due to complicate canopy structures of Irwin mangoes grown in greenhouses, it is difficult to determine their growth parameters accurately. Leaf area, leaf fresh weight, and leaf dry weight are widely used as indicators to diagnose the tree growth. Therefore, it is necessary to establish models that can non-destructively estimate these growth indicators. The objective of this study was to establish regression models to estimate leaf area, leaf fresh weight, and leaf dry weight of Irwin mangoes (Mangifera indica L. cv. Irwin) by using leaf length, leaf width, petiole length, and SPAD value. The input values of leaf length, leaf width, petiole length, and SPAD value of 6-year old Irwin mangoes were measured, and the corresponding output values of leaf area, leaf fresh weight, and leaf dry weight were also measured. After 14 models were selected among the existing models, coefficients of the models were estimated by regression analysis. Three models with higher $R^2$ and lower RMSE values selected. In validation the $R^2$ values for the selected models were 0.967, 0.743, and 0.567 in the leaf area, leaf fresh weight, and leaf dry weight models, respectively. It is concluded that this models will be helpful to conveniently diagnose the growth of the Irwin mango.