• Korean Journal of Materials Research
• /
• v.9 no.5
• /
• pp.509-514
• /
• 1999

Interest in the integrated capacitors, which make it possible to reduce the size of and to obtain improved electrical performance of an electronic system, is expanding. In this study, $Ta_2$O\ulcorner thin film capacitors for MCM integrated capacitors were fabricated on a Upilex-S polymer film by DC magnetron reactive sputtering and the effects of low temperature annealing at various atmospheres and substrate surface morphology on the capacitor characteristics were discussed. The low temperature($150^{\circ}C$) annealing produced improved capacitor yield irrespective of the annealing at mosphere. But the leakage current of the $O_2$-annealed film was larger than that of any other films. This is presumably mosphere. But the leakage current of the $O_2$-annealed film was larger than that of any other films. This is presumably due to the change of the $Ta_2$O\ulcorner film surface by oxygen, which was explained by conduction mechanism study. Leakage current and breakdown field strength of the capacitors fabricated on the Upilex-S film were 7.27$\times$10\ulcornerA/$\textrm{cm}^2$ and 1.0 MV/cm respectively. These capacitor characteristics were inferior to those of the capacitors fabricated on the Si substrate but enough to be used for decoupling capacitors in multilayer package. Roughness Analysis of each layer by AFM demonstrated that the properties of the capacitors fabricated on the polymer film were affected by the surface morphology of the substrate. This substrate effect could be classified into two factors. One is the surface morphology of the polymer film and the other is the surface morphology of the metal bottom electrode determined by the deposition process. Therefore, the control of the two factors is important to obtain improved electrical of capacitors deposited on a polymer film.

• Journal of Surface Science and Engineering
• /
• v.57 no.4
• /
• pp.274-284
• /
• 2024

In this study, copper foil was electroplated under high current density conditions. We used Polyethylene Glycol (PEG), known for its thermal stability and low decomposition rate, as an inhibitor to form a stable and smooth copper layer on the titanium cathode. The electrolyte was composed of 50 g/L CuSO₄ and 100 g/L H₂SO₄, MPSA as an accelerator, JGB as a leveler, and PEG as a suppressor, and HCl was added as chloride ions for improving plating efficiency. The copper foil electroplated in the electrolyte added PEG which induced to inhibit the growth of rough crystals. As a result, the surface roughness value was reduced, and a uniform surface was formed over a large area. Moreover, the addition of PEG led to priority growth to the (111) plane and the formation of polygonal crystals through horizontal and vertical growth of crystals onto the cathode. In addition, the grains became fine when more than 30 ppm of PEG was added. As the microcrystalline structure changed, mechanical and electrical properties were altered. With the addition of PEG, the tensile strength increased due to grain refinement, and the elongation was improved due to the uniform surface. However, as the amount of PEG added increased, the corrosion rate and resistivity increased due to grain refinement. Finally, it was possible to manufacture a copper foil with excellent electrical and mechanical properties and the best surface properties when electroplating was carried out under the condition of additives with Cl-20 ppm, MPSA 10 ppm, JGB 5 ppm, and PEG 10 ppm.

• Structural Engineering and Mechanics
• /
• v.38 no.4
• /
• pp.443-457
• /
• 2011

The loss of strength in a structure as a result of cyclic loads over a period of life time is an important phenomenon for the life-cycle analysis. Service loads are accentuated at the areas of stress concentration, mainly at the connection of components. Structural components unavoidably are affected by defects such as surface scratches, surface roughness and weld defects of random sizes, which usually occur during the manufacturing and handling process. These defects are shown to have an important effect on the fatigue life of the structural components by promoting crack initiation sites. The value of equivalent initial flaw size (EIFS) is calculated by using the back extrapolation technique and the Paris law of fatigue crack growth from results of fatigue tests. We try to analyze the effect of EIFS distribution in a multiple site damage (MSD) specimen by using the extended finite element method (XFEM). For the analysis, fatigue tests were conducted on the centrally-cracked specimens and MSD specimens.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.41 no.9
• /
• pp.839-844
• /
• 2017

In the past few years, three-dimensional (3D) printing has been developed as a rapid prototyping (RP) technique. The fused deposition modeling (FDM)-type 3D printing is one of the most useful RP methods; however, it still has several disadvantages, such as low conductivity, heat degradation, and low surface quality. In this study, test specimens are fabricated using an FDM-type 3D printer with an ABS material. Then, the specimens undergo post-processing on submerging in acetone with various processing times. As the processing time increases, surface roughness is enhanced significantly within the first five seconds by chemical processing, following which the processing effects are reduced. Furthermore, post processing causes the ultimate strength and strain to increase slightly with increased processing time.

• Journal of the Korean Society for Precision Engineering
• /
• v.30 no.12
• /
• pp.1237-1243
• /
• 2013

This study has focused on the effect of ultrasonic vibration table in ELID grinding process of aluminum nitride ceramics. Aluminum nitride ceramics has superior physical and chemical properties and widely used in IC, LSI substrate, package and so on. To achieve the high effective machining of brittle and high strength ceramics as like aluminum nitride, machining method combined ELID grinding and ultrasonic vibration has been adopted in this study. From the experimental results, material removal rate, MRR has been increased maximum 36 percent and spindle resistance has been decreased in using ultrasonic table. Surface roughness of ground surface became a little worse in using ultrasonic table but was somewhat improved in feed direction.

• Journal of the Korean Society for Precision Engineering
• /
• v.25 no.7
• /
• pp.116-123
• /
• 2008

In the fossil power plant, the reliability of the components which consist of the many welded parts depends on the quality of welding. The residual stress is occurred by the heat flux of high temperature during weld process. This decreases the mechanical properties as the strength of fatigue and fracture or causes the stress corrosion cracking and fatigue fracture. Especially, the accidents due to the residual stress occurred at the weld parts of high-temperature and high-pressure pipes and steam headers. Also, the residual stress of the welded part in the recently constructed power plants has been brought into relief as the cause of various accidents. The aim of this study is the measurement of the residual stress using the x-ray diffraction method. The merits of this are more accurate and applicable than other methods. The materials used for the study is P92 steel for the use of high temperature pipe on super critical condition. The variables of tests are the post-weld heat treatment, the surface roughness and the depth from the original surface. The test results were analyzed by the distributed characteristics of the full width at half maximum intensity (FWHM) in x-ray diffraction intensity curve and by the relation of hardness with FWHM.

• Korean Journal of Metals and Materials
• /
• v.47 no.11
• /
• pp.740-747
• /
• 2009

The purpose of this study is to identify the effect of electrolyte compositions on electrodeposited copper foil. First of all, the polyimide substrate was pretreated with plasma. Finally, copper foil was deposited on a Cu/Ni/Polyimide substrate using the electroplating technique. As the quantity of Cu increased, preferred orientations changed into (111). Increasing sulfuric acid, on the other hand, brought down the preferred orientation of (111). The lowest sheet resistance, surface roughness, and fine adhesion were detected when the ratio of $Cu^{2+}$ and $H_2SO_4$ is 50:50(g/l).

• Tunnel and Underground Space
• /
• v.17 no.3 s.68
• /
• pp.203-215
• /
• 2007

Stability and mechanical deformation behavior of rock masses are highly dependent on the mechanical characteristics of contained discontinuities. Therefore, mechanical characteristics of the discontinuities should be considered in the design of tunnel and underground structures. In this study, direct shear tests for rough granite joints were carried out under constant normal stiffness conditions. Effects of initial normal stress, shear velocity, and surface roughness on the characteristics of shear strength and deformation behaviors were examined. Results of shear testing under constant normal stiffness conditions reveal that shear behaviors could be classified into two categories, based on the amount of decrease in shear stress at the Int peak shear stress. With initial normal stiffness increasing, it turned out that shear displacement at peak stress and the first peak shear stress increased, however friction angle and friction coefficient showed decrease. In case of shear stiffness and average friction coefficient, it turned out that they are not dependent on the initial normal stress. Minor effects of shear velocity on rough joints were observed in several shear quantities. However, the effects of shear velocity were insignificant regardless of the normal stress increase. Change of shear strength and deformation characteristics on joint roughness were examined, however, it turned out that the variations were attributed to deviation of shear test specimens.

• The Journal of Advanced Prosthodontics
• /
• v.12 no.3
• /
• pp.157-166
• /
• 2020

PURPOSE. The aim of this study was to evaluate the clinical performance and reliability of plasma sprayed nanostructured zirconia (NSZ) coating. MATERIALS AND METHODS. This study consisted of three areas of analysis: (1) Mechanical property: surface roughness of NSZ coating and bond strength between NSZ coating and titanium specimens were measured, and the microstructure of bonding interface was also observed by scanning election microscope (SEM). (2) Biocompatibility: hemolysis tests, cell proliferation tests, and rat subcutaneous implant test were conducted to evaluate the biocompatibility of NSZ coating. (3) Mechanical compatibility: fracture and artificial aging tests were performed to measure the mechanical compatibility of NSZ-coated titanium abutments. RESULTS. In the mechanical study, 400 ㎛ thick NSZ coatings had the highest bond strength (71.22 ± 1.02 MPa), and a compact transition layer could be observed. In addition, NSZ coating showed excellent biocompatibility in both hemolysis tests and cell proliferation tests. In subcutaneous implant test, NSZ-coated plates showed similar inflammation elimination and fibrous tissue formation processes with that of titanium specimens. Regarding fatigue tests, all NSZ-coated abutments survived in the five-year fatigue test and showed sufficient fracture strength (407.65-663.7 N) for incisor teeth. CONCLUSION. In this study, the plasmasprayed NSZ-coated titanium abutments presented sufficient fracture strength and biocompatibility, and it was demonstrated that plasma spray was a reliable method to prepare high-quality zirconia coating.

• Journal of Korean Society of Steel Construction
• /
• v.23 no.2
• /
• pp.137-146
• /
• 2011

In the fabrication of steel bridges, blast cleaning prior to painting is carried out on the steel members to clean the forged surface and to increase the adhesive property of the applied painting systems. The effect of blast cleaning on the fatigue strength improvement of the weld joints, however, is not clear. In this study, Almen strips and steel specimens were blast-treated, conforming to ten types of blast-cleaning conditions deducted from the blast-cleaning conditions of seven steel structure fabrication companies. The arc height, roughness, hardness, and compressive residual stress were measured before and after the implementation of the ten blast-cleaning methods, and the relationship between the blast conditions and the measured values was studied. The geometry of the weld toe and the compressive residual stress near the weld toe were also measured before and after the blast cleaning of the butt-welded joints, and fatigue tests were carried out on the butt weld joints. The test results showed that blast cleaning significantly increases the fatigue strength and limit.