• The Journal of Advanced Prosthodontics
• /
• v.12 no.4
• /
• pp.197-203
• /
• 2020

PURPOSE. The aim of this study was to evaluate the effect of multiple firings on the bond strength between yttriatetragonal zirconia polycrystals (Y-TZP) and 2 types of resin cements. MATERIALS AND METHODS. Sixty 3Y-TZP specimens (LAVA Frame Multi) were divided into 3 groups depending on the following firing procedures: (1) 2-firing cycles, (2) 5-firing cycles, (3) 10-firing cycles. Two samples from each group were investigated by using SEM to determine the morphological changes. All specimens were treated with 125 ㎛ airborne-particle abrasion and the surface roughness of each specimen was measured. The specimens from each firing group were then further divided into 2 subgroups (n = 9) to apply 2 types of resin cement (MDP-free resin cement: RelyX Unicem-RU, and MDP containing resin cement: Panavia F 2.0-PA). The shear bond strength (SBS) test was performed and failure types of all the debonded specimens were classified by using a stereomicroscope as adhesive, cohesive, and mixed. The statistical analysis of surface roughness and SBS data were performed by using 1-way ANOVA and 2-way ANOVA followed by Tukey-HSD tests (α=.05). Failure modes were calculated as a percentage for each group. RESULTS. The bond strength of RU and PA to the specimens obtained with 2 firings were not statistically different from each other (P=.1). However, the SBS values of PA were found to be significantly higher than RU for the specimens obtained with 5 and 10 firing cycles (P=.001 and P=.02, respectively). Surface roughness analysis revealed no statistical difference between groups (P=.2). The SEM analysis of samples fired 5- and 10- times showed irregularities and boundary loss in zirconia grains, and empty spaces between zirconia grains. CONCLUSION. The bond strength of PA cement was higher than that of RU to the zirconia subjected to repeated firings (5 and 10 firing cycles). When zirconia is subjected to multiple firings, using MDP-containing resin cement can be recommended.

• Polymer(Korea)
• /
• v.38 no.5
• /
• pp.620-625
• /
• 2014

The effect of polyvinyl alcohol/polyamide-epichlorohydrin (PVA/PAE) complex strengthening additive on dry and wet strength and surface properties of paper was investigated. The enhancements of dry and wet strength and dimensional stability were found when PVA/PAE was applied as a complex strengthening additive compared with the cases of applying individual PVA or PAE. This was understood as physical crosslinking between PVA and PAE in the PVA/PAE complex strength additive. This complex strengthening additive also lowered surface roughness and increased sizing. As a result, PVA/PAE complex strengthening additive provided the distinctive gain dot in printed papers.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.16 no.2
• /
• pp.940-946
• /
• 2015

The turning clearance angle changes the machining characteristics. In this study, three workpiece materials, machine structural carbon steel, chrome-molybdenum steel and stainless steel, were examined. The experiments revealed how the features of selected materials changed when they were processed with machining operation. To find the surface roughness of workpiece materials, the workpiece materials, which have a higher tensile strength, showed a much better surface roughness in the surface roughness tester. Moreover, the process feed rate was compared between 0.07 mm/rev and 0.10 mm/rev. When the process feed rate was 0.07 mm/rev, the surface roughness has superior results without reference to the quality of the materials. According to this research on the turning clearance angle, the best roughness value was observed when the quality of the materials were $0.9^{\circ}$, whereas the worst roughness was observed when quality of the materials was $0.3^{\circ}$.

• Korean Journal of Metals and Materials
• /
• v.50 no.12
• /
• pp.913-920
• /
• 2012

In spite of some problems in processability and bondability, Au wires in the microelectronics industry are gradually being replaced by copper wires to reduce the cost of raw material. In this article, the effects of surface roughness enhanced capillaries on thermosonic Cu wire bonding were evaluated. The roughness-enhanced zirconia toughened alumina (ZTA) capillaries were fabricated via a thermal grooving technique. As a result, the shear bond strength of first bonds (ball bonds) bonded using the roughness-enhanced capillary was enhanced by 15% as compared with that of normal bonds due to more effective plastic deformation and flow of a Cu ball. In the pull-out test of second bonds (stitch bonds), processed at two limit conditions on combinations of process parameters, the bond strength of bonds formed using the roughness-enhanced capillary also resulted in values higher by 55.5% than that of normal bonds because of the increase in the bonding area, indicating the expansion of a processing window for Cu wire bonding. These results suggest that the adoption of roughness-enhanced capillaries is a promising approach for enhancing processability and bondability in Cu wire bonding.

• Journal of the Korean Geotechnical Society
• /
• v.15 no.4
• /
• pp.247-260
• /
• 1999

It was found that surface roughness has a first-order effect on the interface shear strength and accordingly it should be accurately quantified if its role is to be properly understood. Most of the surface roughness parameters are based on the trisector approach (three dimensional parameter) which can provide a good measure of the surface roughness from a static perspective. However, if roughness is to be correlated with a directional sensitive parameter such as interface shear then a two dimensional parameter could be more meaningful if the roughness measurements are made parallel to the direction of shearing. In this paper, alternative roughness parameters which consider the direction of shearing are described. These directional parameters are compared with the existing roughness parameters, and the relationship between these directional and non-directional parameters are investigated. The surface roughness was quantified by using the Optical Profile Microscopy (OPM) method (Dove and Frost, 1996) based on the digital image analysis. The results showed that the various surface roughness parameters measured in this study exhibit similar trend of roughness values, so that, good relationships are obtained between these roughness parameters. As the surface roughness increases, the roughness values measured in trisector coupons are increasing higher than those measured in parallel coupons.

• Composites Research
• /
• v.33 no.6
• /
• pp.371-376
• /
• 2020

The adhesive strength can be improved through surface treatment. The most common method is to improve physical bonding by varying the surface conditions. This study presents the effect of laser surface treatment on the adhesive strength of CFRP. The surface roughness was patterned using a 1064 nm laser. The effects of the number of laser shots and the direction and length of the pattern on the adhesion of the CFRP/CFRP single joint were investigated through tensile tests. Tests according to ASTM D5868 were performed, and the bonding mechanism was determined by analyzing the damaged surface after a fracture. The optimized number of the laser shots and the optimized depth of the roughness should be required to increase the bonding strength on the CFRP surface. When considering the shear stress in the tensile direction, the roughness pattern in the direction of 45° that increases the length of the fracture path in the adhesive layer resulted in an increase of the adhesive strength. The surface treatment of the bonding surface using a laser is a suitable method to acquire a mechanical bonding mechanism and improve the bonding strength of the CFRP bonding joint. The study on the optimized laser process parameters is required for utilizing the benefits of laser surface processing.

• The Journal of Advanced Prosthodontics
• /
• v.11 no.1
• /
• pp.1-6
• /
• 2019

PURPOSE. The purpose of this in vitro study was to evaluate the effect of surface grinding and polishing procedures using high speed zirconia diamond burs with different grit sizes on the phase transformation and flexural strength of zirconia. MATERIALS AND METHODS. Forty disc shape specimens ($15{\times}1.25mm$) with a cylindrical projection in the center of each disc ($1{\times}3mm$) were fabricated with 3Y-TZP (Prettau, Zirkonzahn, Italy). The specimens were divided into 4 groups (n=10) according to the grinding and polishing procedures: Control group - grinding (coarse-grit diamond bur), Group 1 - grinding (coarse-grit diamond bur) + polishing, Group 2 - grinding (fine-grit diamond bur) + polishing, and Group 3 - grinding (fine grit diamond bur). Each specimen was analyzed by 3D-OM, XRD analysis, and biaxial flexural strength test. RESULTS. Based on the surface morphology by 3D-OM images, polished specimens showed smoother surface and lower roughness value (Ra). In the result of XRD analysis, partial phase transformation from tetragonal to monoclinic zirconia occurred in all groups. Control group, ground with a coarse grit diamond bur, showed more $t{\rightarrow}m$ phase transformation and lower flexural strength than Groups 1 and 2 significantly. CONCLUSION. The flexural strength in all specimens after grinding and polishing showed over 500 MPa, and those were clinically acceptable. However, grinding with a coarse grit diamond bur without polishing induced the phase transformation and low strength. Therefore, surface polishing is required for the occlusal adjustment using a high speed zirconia diamond bur to reduce the phase transformation and to prevent the decrease of flexural strength of zirconia.

• Journal of the Microelectronics and Packaging Society
• /
• v.24 no.1
• /
• pp.91-101
• /
• 2017

In this study, we conducted the preliminary research for high speed laser cutting of LED module. In particular, the feasibility of ultra-high speed laser cutting of 100 mm/s which exceeds the cutting speed of conventional dicing saw was examined. For this, copper/ceramic and silicone/ceramic hybrid substrates, which are the components of the LED module, were fabricated, and the surface morphology, surface roughness and flexural strength of the laser-cut samples were investigate and compared with the dicing-cut samples. To investigate optimal laser cutting conditions for hybrid substrates, the effects of various laser cutting conditions on cutting surface characteristics were studied using single ceramic and copper substrate. Optimal laser cutting conditions of the hybrid substrates were the use of Ar assist gas, high laser power and high assist gas pressure. Comparing the cutting surface of the hybrid substrates, the surface characteristics of the laser-cut samples are slightly inferior to those of the dicing-cut samples. The average surface roughness of the laser-cut samples was about $9{\mu}m$, and that of the dicing-cut samples was about $4{\mu}m$. However, considering very low cutting speed (3 mm/s) of the dicing saw, the surface morphology of the laser-cut sample was relatively uniform, and the surface roughness was not much different from that of the dicing-cut sample. The flexural strength of the laser-cut samples was equivalent to or slightly inferior to the flexural strength of dicing-cut samples. However, if the laser processing conditions are sufficiently optimized, the ultra-high speed laser cutting of the LED module will be possible.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2004.04a
• /
• pp.232-236
• /
• 2004

The fracture characteristics of unidirectional composite single-lap bonded joints were investigated experimentally and numerically. The effects of bonding method, surface roughness, bondline thickness and the existence of fillet on the failure characteristics and strength of bonded single-lap joints were evaluated experimentally. The failure process, failure mode and the behavior of load-displacement curve was apparently different according to bonding method. The failure load of the specimen co-cured without adhesive was definitely superior to other types of specimens but the specimens co-cured with adhesive film had a less strength than secondary bonded specimens. In the secondary bonded specimens, the lower value of surface roughness and existence of fillet improved the strength of specimens. The strain energy release rates calculated by geometric nonlinear finite element analyses and Virtual Crack Closure Technique for the secondary bonded specimens considering the three types of initial cracks - comer crack, edge crack and delamination crack - were consistent with the test results.

• Geomechanics and Engineering
• /
• v.12 no.3
• /
• pp.399-415
• /
• 2017

A series of direct shear tests were conducted to investigate the frictional properties of the interface between structures and the filling soil of Chongqing airport fourth stage expansion project. Two types of structures are investigated, one is low carbon steel and the other is the bedrock sampled from the site. The influence of soil water content, surface roughness and material types of structure were analyzed. The tests show that the interface friction and shear displacement curve has no softening stage and the curve shape is close to the Clough-Duncan hyperbola, while the soil is mainly shear contraction during testing. The interface frictional resistance and normal stress curve meets the Mohr-Coulomb criterion and the derived friction angle and frictional resistance of interface increase as surface roughness increases but is always lower than the internal friction angle and shear strength of soil respectively. When surface roughness is much larger than soil grain size, soil-structure interface is nearly shear surface in soil. In addition to the geometry of structural surface, the material types of structure also affects the performance of soil-structure interface. The wet interface frictional resistance will become lower than the natural one under specific conditions.