• Journal of the Korean Society for Heat Treatment
• /
• v.30 no.6
• /
• pp.251-257
• /
• 2017

The effect of annealing temperature on the martensitic transformation behavior, tensile deformation chracteristics and shape recovery etc., has been studied in TiNi based shape memory ribbon fabricated by coldrolling of wire. TiNi based shape memory wire (${\phi}=500{\mu}m$) of which structure is intermetallic compound could be cold-rolled without process annealing up to the reduction rate in thickness of 50%, but a few cracks appear in cold-rolled ribbon in the reduction rate in thickness of 65%. The $B2{\rightarrow}R{\rightarrow}B19^{\prime}$ martensitic transformation or $B2{\rightarrow}B19^{\prime}$ martensitic transformation occurs in annealing conditions dissipating lattice defects introduced by coldrolling. However, in case of higher reduction rate or lower annealing temperature, martensitic transformation in cold-rolled and then annealed ribbons does not occur. The maximum shape recovery rate of cold-rolled ribbons with the reduction rate of 35 and 65% could be achieved at annealing temperatures of 250 and $350^{\circ}C$, respectively. The shape recovery rate seems to be related to the stress level of plateau region on stress-strain curve.

• Journal of Korean Association for Spatial Structures
• /
• v.14 no.3
• /
• pp.93-100
• /
• 2014

Ethylene Tetrafluoroethylene (ETFE) has been widely used in long-span buildings because of its light weight and high transparency. This paper studies the short and long term creep behaviour of ETFE foil. A series of short-term creep and recovery tests were performed, in which the residual strain was observed. A long-term creep test of the ETFE foil was also performed over 110 days. A viscoelastic-plastic model was then established to describe the short-term creep and recovery behaviour. The model contains a traditional multi-Kelvin part and an added steady-flow component to represent the viscoelastic and viscoplastic behaviour, respectively. The model successfully fit the data for three stresses and six temperatures. Additionally, time-temperature equivalency was adopted to predict the long-term creep behaviour of ETFE foil. Horizontal shifting factors were determined from the process of shifting creep-curves at six temperatures. The long-term creep behaviours at three temperatures were predicted. Finally, the long-term creep test showed that the short-term creep test at identical temperatures insufficiently predicted additional creep behaviour, and the long-term test verified the horizontal shifting factors derived from the time-temperature equivalency.

• Proceedings of the Computational Structural Engineering Institute Conference
• /
• 2003.04a
• /
• pp.288-295
• /
• 2003

An adaptive procedure in finite element analysis is presented by p-refinement of meshes in conjunction with a posteriori error estimator that is based on the recovery technique. In case of the recovery technique, the SPR(superconvergent patch recovery) approach has been modified for p-adaptive mesh refinement. The strategy of finding a nearly optimal distribution of polynomial degrees on a fixed finite element mesh is discussed such that a particular element has to be refined automatically to obtain an acceptable level of accuracy by increasing p-levels non-uniformly. To verify the proposed algorithm, the limit value approach is proposed which utilizes the exact strain energy computed from the extrapolation equation. A new pre-processor is developed for the p-version finite element program in which the vector graphic editor is used for the automatic generation of node connection and coordinate by halfedge solid data structure according to uniform or nonuniform p-distribution. The general 2-D algorithm is also developed to generate face modes and internal modes in accordance with different mesh types. The quality of the error estimator is investigated with the help of two mumerical examples. The results show that the sequences of p-distributions obtained by the proposed error indicator closely follow the optimal trajectory.

• Korean Journal of Materials Research
• /
• v.26 no.4
• /
• pp.167-172
• /
• 2016

The high temperature deformation behavior of $Ni_3Al$ and $Ni_3(Al,Mo)$ single crystals that were oriented near <112> was investigated at low strain rates in the temperature range above the flow stress peak temperature. Three types of behavior were found under the present experimental conditions. In the relatively high strain rate region, the strain rate dependence of the flow stress is small, and the deformation may be controlled by the dislocation glide mainly on the {001} slip plane in both crystals. At low strain rates, the octahedral glide is still active in $Ni_3Al$ above the peak temperature, but the active slip system in $Ni_3(Al,Mo)$ changes from octahedral glide to cube glide at the peak temperature. These results suggest that the deformation rate controlling mechanism of $Ni_3Al$ is viscous glide of dislocations by the <110>{111} slip, whereas that of $Ni_3(Al,Mo)$ is a recovery process of dislocation climb in the substructures formed by the <110>{001} slip. The results of TEM observation show that the characteristics of dislocation structures are uniform distribution in $Ni_3Al$ and subboundary formation in $Ni_3(Al,Mo)$. Activation energies for deformation in $Ni_3Al$ and $Ni_3(Al,Mo)$ were obtained in the low strain rate region. The values of the activation energy are 360 kJ/mol for $Ni_3Al$ and 300 kJ/mol for $Ni_3(Al,Mo)$.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2000.04a
• /
• pp.76-79
• /
• 2000

Polymeric composites exhibit highly nonlinear and rate dependent behavior during loading and unloading in off-axis directions. The equilibrium state of stress during loading is lower than the state of stress produced at finite strain rates. The amount of stress relaxation during loading decreases. Interestingly, however, the stress goes up to reach to the equilibrium state of stress for a fixed displacement during unloading. The unloading behavior is quite similar to the loading behavior. The stress relaxation patterns during loading and unloading is also similar, and those depend on the fiber orientation angles and the loading and unloading rates. The AS4/PEEK thermoplastic composite is used to characterize the relaxation behavior for different off-axis angles and loading rates. There exists a transient loading region at the beginning of unloading. The effective stress and effective plastic strain concept is used to establish a master curve of stress recovery pattern for different off-axis angles and unloading rates.

• Korean Journal of Food Science and Technology
• /
• v.23 no.4
• /
• pp.394-399
• /
• 1991

The strain OK-63 isolated from katsuobushi was cultured on wheat bran medium and the isolate was morphologically identified as an Aspergillus niger group and showed maximum pretense activity and multiplication after 6 days of cultivation. Protease was purified by ammonium sulfate fractionation. Sephadex G-100 gel filtration and DEAE-cellulose column chromatography. The purified enzyme showed single band by polyacrylamide gel electrophoresis and the purity was 150 times higer than crude enzyme. The recovery of enzyme activity was found to be 45%.

• Korea-Australia Rheology Journal
• /
• v.14 no.1
• /
• pp.25-32
• /
• 2002

We report the first steps of a collaborative project between the University of Queensland, Polyflow, Michelin, SK Chemicals, and RMIT University, on simulation, validation and application of a recently introduced constitutive model designed to describe branched polymers. Whereas much progress has been made on predicting the complex flow behaviour of many - in particular linear - polymers, it sometimes appears difficult to predict simultaneously shear thinning and extensional strain hardening behaviour using traditional constitutive models. Recently a new viscoelastic model based on molecular topology, was proposed by McLeish and carson (1998). We explore the predictive power of a differential multi-mode version of the porn-pom model for the flow behaviour of two commercial polymer melts: a (long-chain branched) low-density polyethylene (LDPE) and a (linear) high-density polyethylene (HDPE). The model responses are compared to elongational recovery experiments published by Langouche and Debbaut (19c99), and start-up of simple shear flow, stress relaxation after simple and reverse step strain experiments carried out in our laboratory.

• Structural Engineering and Mechanics
• /
• v.23 no.4
• /
• pp.339-352
• /
• 2006

Observing the unique stress-strain curves of the superelastic shape memory alloy (SMA) in tension and compression, the primary intention of this study is to investigate the behavior of the shafts made of the same material, under torsional loading-unloading cycles for large angle of twist. Experiments have been performed for the superelastic SMA shafts with different unsupported lengths and angles of twist and the results are compared with those of stainless steel (SUS304) shafts under similar test conditions. As expected for the superelastic SMA, the residual strains are small enough after each cycle and consequently, the hysteresis under loading-reverse loading is much narrower than that for the SUS304. For large angle of twists, the torsional strength of the superelastic SMA increases nonlinearly and exceeds that of SUS304. Most interestingly, the slender solid superelastic SMA shafts are found to buckle when acted upon torsion for large angle of twist.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2006.05a
• /
• pp.215-218
• /
• 2006

A study was made to investigate microstructural evolution and mechanical properties of ultra-fine grained (UFG) pure-Ti produced by equal channel angular (ECA) pressings. The deformed structures were analyzed by finite element method and transmission electron microscopy with the increment of straining. After 4 isothermal ECA pressings, initial coarse grains ($30{\mu}m$) were significantly refined to ${\sim}0.3{\mu}m$ with homogeneous distribution of microstructure which was resulted from $180^{\circ}$ rotation of the sample between pressings. UFG pure-Ti exhibited the considerable improvement in yield strength while losing strain hardening capacity as compared to coarse grained microstructure at ambient temperature, which was mainly attributed to ultra-fine grain microstructure with non-equilibrium grain boundaries.

• KSBB Journal
• /
• v.11 no.1
• /
• pp.115-123
• /
• 1996

Two kinds of mutants were isolated to clone a cluster of genes essential for zooglan biosynthesis. Zoogloea ramigera 115 strains produce capsular polysaccharide. To achieve conjugation in strain 115 and to facilitate recovery of product, a capsule non-forming strain was isolated via successive centrifugation and screening. The other kind of mutants devoid of or producing altered exopolysaccharides were obtained using classical transposon(Tn5) technique and screened for altered colony morphology and celluflour binding properties. Complementation of these mutants was achieved with Z. ramigera 115 slime gene library constructed in a broad host range cosmid vector and helper plasmid by triparental conjugation.