• Title/Summary/Keyword: strain aging

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Study on the Thermal Degradation Behavior of FKM O-rings

  • Lee, Jin Hyok;Bae, Jong Woo;Choi, Myoung Chan;Yoon, Yoo-Mi;Park, Sung Han;Jo, Nam-Ju
    • Elastomers and Composites
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    • v.53 no.4
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    • pp.213-219
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    • 2018
  • The degradation mechanism and physical properties of an FKM O-ring were observed with thermal aging in this experiment. From X-ray photoelectron spectroscopy (XPS) analysis, we could observe carbon (285 eV), fluoro (688 eV), and oxygen (531 eV) peaks. Before thermal aging, the concentration of fluoro atoms was 51.23%, which decreased to 8.29% after thermal aging. The concentration of oxygen atoms increased from 3.16% to 20.39%. Under thermal aging, the FKM O-ring exhibited debonding of the fluoro-bond by oxidation. Analysis of the C1s, O1s, and F1s peaks revealed that the degradation reaction usually occurred at the C-F, C-F2, and C-F3 bonds, and generated a carboxyl group (-COOH) by oxidation. Due to the debonding reaction and decreasing mobility, the glass transition temperature of the FKM O-ring increased from $-15.91^{\circ}C$ to $-13.79^{\circ}C$. From the intermittent CSR test, the initial sealing force was 2,149.6 N, which decreased to 1,156.2 N after thermal aging. Thus, under thermal aging, the sealing force decreased to 46.2%, compared with its initial state. This phenomenon was caused by the debonding reaction and decreasing mobility of the FKM O-ring. The S-S curve exhibited a 50% increase in modulus, with break at a low strain and stress state. This was also attributed to the decreasing mobility due to thermal aging degradation.

Effect Of The Microstructure And Aging Treatment Conditions On Strength Of High Strength Invar Alloy (고강도 인바합금의 강도에 미치는 미세구조와 시효처리 조건의 영향)

  • Jung, J.Y.;Lee, K.D.;Ha, T.K.;Jeong, H.T.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.322-325
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    • 2007
  • Precipitation characteristics of the Fe-36Ni based high strength Invar alloy for power transmission wire was investigated in this study. High strength can be obtained in this alloy through solution hardening, precipitation hardening and strain hardening by cold working. In the present study, ingots of Fe-36Ni based Invar alloys with the contents of C, Mo and V varied. Microstructure observations by OM, SEM, and TEM were carried out to validate the simulation results. BCC phase and $FeNi_3$ phase are also expected at lower temperatures below $500^{\circ}C$. Aging treatments were carried out at temperatures ranging from 400 to $900^{\circ}C$ for time intervals from 3 min to 100hrs. Peak aging condition was obtained as $400^{\circ}C$ and 1 hr. With temperature increased, peak strength was decreased abruptly. Microstructure observation was conducted by optical microscopy, scanning electron microscopy, and transmission electron microscopy.

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Isolation of Debaryomyces hansenii and selection of an optimal strain to improve the quality of low-grade beef rump (middle gluteal) during dry aging

  • Yoonjeong Yoo;Hyemin Oh;Yohan Yoon
    • Animal Bioscience
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    • v.36 no.9
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    • pp.1426-1434
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    • 2023
  • Objective: The objective of this study was to evaluate the effect of Debaryomyces hansenii isolated from dry-aged beef on the tenderness and flavor attributes of low-grade beef during dry aging. Methods: Five D. hansenii strains were isolated from dry-aged beef samples. The rump of low-grade beef was inoculated with individual D. hansenii isolates and subjected to dry aging for 4 weeks at 5℃ and 75% relative humidity. Microbial contamination levels, meat quality attributes, and flavor attributes in the dry-aged beef were measured. Results: Of the five isolates, the shear force of dry-aged beef inoculated with SMFM201812-3 and SMFM201905-5 was lower than that of control samples. Meanwhile, all five isolates increased the total free amino acid, glutamic acid, serine, glycine, alanine, and leucine contents in dry-aged beef. In particular, the total fatty acid, palmitic acid, and oleic acid contents in samples inoculated with D. hansenii SMFM201905-5 were higher than those in control samples. Conclusion: These results indicate that D. hansenii SMFM201905-5 might be used to improve the quality of beef during dry aging.

Mechanical Reliability Evaluation of Sn-37Pb Solder/Cu and Sn-37Pb Solder/ENIG Joints Using a High Speed Lap-shear Test (고속 전단시험법을 이용한 Sn-37Pb/Cu 와 Sn-37Pb/ENIG 솔더 접합의 기계적신뢰성 평가)

  • Jeon, Seong-Jae;Hyun, Seung-Min;Lee, Hoo-Jeong;Lee, Hak-Joo
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.250-255
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    • 2008
  • This study utilized a high speed lap-shear test to evaluate the mechanical behavior of Sn-37Pb/Cu and Sn-37Pb/Electroless Nickel immersion Gold under bump metallization solder joints under high speed loading and hence the drop reliability. The samples were aged for 120 h at different temperatures ($120^{\circ}C,\;150^{\circ}C,\;170^{\circ}C$) and afterward tested at different displacement rates (0.01 mm/s to 500 mm/s) to examine the effects of aging on the drop life reliability. The combination of the stress-strain graphs captured from the shear tests and identifying a fracture mode dominant in the samples for different strain rates leads us to conclude that the drop reliability of solder joints degrades as the aging temperature increases, possibly due to the role of the IMC layer. This study successfully demonstrates that the analysis based on a high speed lap-shear test could be critically used to evaluate the drop reliability of solder joints.

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Determination of Lamellar Tearing Initiation Temperatures and the Effect of Non-metallic Inclusions on Tear (라멜라균열의 생성온도와 비금속개재물의 영향)

  • 고진현
    • Journal of Welding and Joining
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    • v.10 no.2
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    • pp.43-50
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    • 1992
  • This study was aimed at resolving uncertainties about lamellar tearing initiation temperatures and studying the effect of nonmetallic inclusions on the tear initiation. In order to measure the lamellar tearing initiation temperature, the slice bend test was conducted in the temperature range of 20.deg.C to 425.deg.C on A572 Grade 50 and A588 Grade A steels. In addition, the weld restrain test was carried out to measure directly the tear initiation temperature with A572 steel. In slice bend tests, A572 steel showed the most susceptible region to lamellar tearing to be in the range of 100 to 300.deg.C, where the steel showed the minimum ductility. The observed tear initiation by the weld restraint test was to be in the range of 200to 300.deg.C. The tears became narrower and less rounded at the susceptible temperatures. It was confirmed in this study that lamellar teraring initiated during cooling from welding in the range of 200 to 300.deg.C and they were initiated by strain aging embrittlement.

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High Temperature Deformation Behavior of Ti-Al Intermetallic Compound - Microstructure Effect (TiAl 금속간 화합물의 미세조직에 따른 고온변형특성)

  • 하태권;정재영;이광석;장영원
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.05a
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    • pp.295-298
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    • 2003
  • High temperature deformation behavior of a Ti-Al intermetallic compound has been investigated. Specimens with a near gamma and a lamella structures were obtained by performing heat treatment at 1200 and 1330$^{\circ}C$, respectively, for 24 hr and stabilized at 900$^{\circ}C$ for 4 hr followed by air cooling. A series of load relaxation tests has been conducted on these samples at temperatures ranging from 850 to 950$^{\circ}C$ to construct flow curves in the strain rate range from 10$\^$-6//s to 10$\^$-3//s. Strain hardening was observed even at the temperature of 950$^{\circ}C$ in both the near gamma and the lamella structures. Further aging treatment for 12 hr at test temperatures has found to cause no softening in both microstructures.

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