• Title/Summary/Keyword: steam autoclave

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A Study on Physical Properties of Concrete using Admixtures for High Strength Concrete (고강도콘크리트용 혼화재를 사용한 콘크리트의 물성에 관한 연구)

  • 이승한
    • Magazine of the Korea Concrete Institute
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    • v.7 no.2
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    • pp.155-164
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    • 1995
  • This study was performed to get high strength of the precase concrete adopting a steam curing by using a gypsum-admixture for the high strength concrete. The superplasticizer was used to compensate low slump of base concrete keeping its slump up about $6{\pm}1cm$. To examine the property for strength revelation of concrete using admixtures for a high strength concrete, steam and standard curing were compared each other. Test results were shown that admixtures for high strength concrete were more effective in steam curing than standard curing. On the condition that the unit cement content is about $530{\sim}600kg/m^3$, the compressive strength of concrete replacing by 10% of the admixture was obtained over $65Okgf/cm^2$, which was increased as 1.3 times as that for the nonreplacement. When the admixture was replaced to 15-30%, the compressive strengh was obtained over $700kgf/cm^2$ which was increased as 1.4 - 1.5 times. Therefore, the admixture for high strength concrete, being effective in steam curing, was more efficient to get a high strength concrete using only steam curing instead of an autoclave curing for the secondary products of cement.

Repassivation Behavior of Ni Base Alloys in a Mild Alkaline Water at 300℃

  • Hwang, Seong Sik;Kim, Dong Jin;Kim, Joung Soo;Kim, Hong Pyo
    • Corrosion Science and Technology
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    • v.5 no.3
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    • pp.85-89
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    • 2006
  • KAERI(Korea Atomic Energy Research Institute) has developed a repassivation rate test system which can be operated at $300^{\circ}C$. It consists of an autoclave, three electrodes for an electrochemical test and a diamond scratch tip. All the electrodes are electrically insulated from the autoclave by using high temperature fittings. Reproducible repassivation curves of alloy 600 at 300 C were obtained. Repassivation rate of alloy 600 at pH 13 was slower than that of pH 10. Stress corrosion cracking test was carried as a function of the pH at a high temperature. At pH 10, alloy 600 showed a severe stress corrosion cracking(SCC), whereas it did not show a SCC at pH 7. From the viewpoint of a relationship between the current density and the charge density, a big difference was observed in the two solutions; the slope of pH 13 was steeper than that of pH 10. So the stress corrosion susceptibility at pH 13 seems to be higher than that of pH 10. The system would be a good tool to evaluate the SCC susceptibility of alloy 600 at a high temperature.

An Experimental Study on the Compressive Strength of Ultra High Strength Concrete with Vacuum Water Absorbing Curing (진공포수양생을 적용한 초고강도 페이스트의 압축강도 발현에 관한 실험적 연구)

  • Jang, Jong-Min;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2019.11a
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    • pp.27-28
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    • 2019
  • In this study, the characteristics of compressive strength of ultra high strength concrete supplied with moisture from outside by vacuum water absorbing curing method were investigated. Specimens were prepared by replacing the binder(Silifa fume and GGBS) by 25 wt% with respect to the weight of cement at W/B 0.16. Each specimen was subjected to water Vacuum absorbing curing time 0 min, 30 min, 60 min, 90 min and 120 minutes immediately after the demolding. Curing was performed at $20^{\circ}C$ Air-dry curing, $90^{\circ}C$ steam curing, $90^{\circ}C$ steam curing and $180^{\circ}C$ autoclave curing. Experimental results showed that water absorbing degree increased with increasing water absorbing curing time, and BS25 sample had higher water absorbing degree than SF25 sample at same time. Compressive strength tended to increase up to about 40% in water absorbing degree, but compressive strength decreased again in water absorbing more than 40%.

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Extraction Procedures for Free Radical Scavenging Activity from Noni Fruit (Morinda citrifolia) (노니 과실에 함유된 항산화물의 추출 공정)

  • Gwak, Mi-Kyung;Choi, Hee-Sun;Manochai, Benya;Hong, Jeong-Hwa
    • Korean Journal of Medicinal Crop Science
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    • v.19 no.1
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    • pp.38-46
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    • 2011
  • In this study, we investigated maximum yield of radical scavenging activity (RSA) using each of various extraction solvents and procedure from noni friut (Morinda citrifolia). Noni fruits were either sun-dried (FS) or hot-air dried (FO) at $60^{\circ}C$ after steam blanching. For optimum aqueous extraction, noni fruits should be sun dried and autoclave extraction time should not be over 30 min to produce extraction with high RSA with low cost. In case of 50% ethanol extraction, reflux extracts of FS and FO resulted in $IC_{50}$ of 1.92 mg/mL and 3.06 mg/mL at 8 hr. When $IC_{50}$ values were lower than 5 mg/mL, coefficient of correlation was 0.71 indicating that 71% of the phenolic antioxidants in noni fruits were accounted for the activity by scavenging free DPPH. However, coefficient of correlation significantly decreased to 0.63 over $IC_{50}$ values of 5 mg/mL. Autoclave extraction contained chlorogenic acid of $14.69 \;{\mu}g/mL$ and scopoletin of $3.86 \;{\mu}g/mL$. Reflux extraction showed all three compounds, chlorogenic acid ($26.19 \;{\mu}g/mL$), quercetin ($19.59 \;{\mu}g/mL$), and scopoletin ($17.4 \;{\mu}g/mL$). Therefore, the result of this study indicated that the potential antioxidant activities and functional values were obtained significantly with reflux extraction from noni fruit.

An Experimental Study on the Curing Method and PP Fiber Mixing Ratio on Spalling Resistance of High Strength Concrete (양생요인 및 PP 섬유 혼입율 변화에 따른 고강도 콘크리트의 폭렬특성)

  • Han, Cheon-Goo;Kim, Won-Ki
    • Journal of the Korea Institute of Building Construction
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    • v.9 no.6
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    • pp.113-119
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    • 2009
  • This study is to investigate the fundamental and fireproof qualities of high strength concrete corresponding to changes in the curing factors and the PP fiber ratio. The results were as follows. For the fundamental characteristics of concrete, the fluidity was reduced in proportion to the increase in the PP fiber ratio. The compressive strength was somewhat reduced according to an increase in the PP fiber ratio. However, it had the high strength scope of more than 60 MPa at 7 days and of more than 90 MPa at 28 days. On the spalling mechanism followed by changes of the water content ratio, spalling was prevented in all combinations, except the specimen without PP fiber and subjected to 3.0% of moisture contents. When spalling was prevented at that time, the residual compressive strength ratio was 22%~41% and the mass reduction ratio was 5%~7%, which was relatively favorable. As the spalling mechanism corresponds to changes in the curing method, spalling was prevented in concrete with a PP fiber mixing ratio of more than 0.05% in the event of standard curing, and in concrete with a PP fiber mixing ratio of more than 0.10% in the case of steam curing and autoclave curing. In these cases, when spalling was prevented, the residual compressive strength ratio was 23~42% and the mass reduction ratio was 7~11%. In these results, the ease of spalling prevention in high strength concrete was inversely proportional to the water content ratio. Depending on the curing method, spalling was prevented in concrete with over 0.05% PP fiber with standard curing and in concrete with over 0.1% PP fiber with steam curing and autoclave curing.

Mycelial growth of Lentinula edodes in response to different mixing time, pressure intensity, and substrate porosity

  • Chang, Hyun You;Seo, Geum Hui;Lee, Yong Kuk;Jeon, Sung Woo
    • Journal of Mushroom
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    • v.15 no.4
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    • pp.164-167
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    • 2017
  • Biological efficiency (BE), the ratio of fresh mushrooms harvested per dry substrate weight, expressed as the percentage of Lentinula edodes, also known as shiitake, was determined using the 'Sanjo 701' strain stored in the Department of Mushroom at the Korea National College of Agriculture and Fisheries. The mycelia were grown in glass columns with varying levels of moisture content and varying mixing periods of 0.5, 1, 2, and 3 hours. The substrate was sterilized using a steam pressure autoclave sterilizer at normal and high pressure to avoid contamination. The results showed that mycelial growth (126 mm/15 days) was optimized at 55% moisture content. The best mycelial growth of 117 mm/15 days was obtained with 2 hours of mixing time. Normal pressure sterilization yielded better results with mycelial growth of 96 mm/15 days at $100^{\circ}C$ compared to 88 mm /15 days with sterilization at $121^{\circ}C$. Mycelial density was higher, i.e. 3(+++), with normal pressure sterilization compared to 2(++) with high pressure sterilization. Furthermore, sawdust mixed with 5% woodchips increased the substrate porosity and yielded higher mycelial growth. Thus, we demonstrated that the optimum harvest or potential increased yield of shiitake can be obtained by modulating moisture content, mixing time, and substrate porosity.

Effect of Hot Water Boiling and Autoclaving on Physicochemical Properties of American Ginseng (Panax quinquefolium L.)

  • Kim, Kyung-Tack;Yoo, Kyung-Mi
    • Journal of Ginseng Research
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    • v.33 no.1
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    • pp.40-47
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    • 2009
  • This study evaluates changes in the chemical composition and bioactivities of American ginseng (Panax quinquefolius L.) processed by boiling in water, $75^{\circ}C$ for 10, 20, 30, and 40 min, and autoclaving at high temperatures, $115^{\circ}C$ for 30 and 60 min and $130^{\circ}C$ for 90 and 120 min. Total ginsenoside contents of boiled ginseng remained relatively unchanged, whereas the contents of autoclaved ginseng samples significantly decreased with an increase of both time and temperature. Compared to unheated ginseng (control), the color of both boiled and autoclaved ginseng decreased in lightness and increased in redness. The acidic polysaccharide contents, the total phenolic contents and the antioxidant capacity of boiled and autoclaved ginseng were higher than the untreated ginseng, with the highest values being exhibited by the autoclaved samples. In particular, the antioxidant capacity of unheated ginseng increased about 2.5 times ($285.7{\pm}14.03\;mg$/100g to $777.2{\pm}26.4\;mg$/100g) when ginseng was autoclaved at $130^{\circ}C$ for 120 min as compared to the control. It was concluded that as American ginseng was processed at a high temperature, especially steam-heated in an autoclave, its chemical constituents changed and, in particular, acidic polysaccharides, total phenolics and antioxidant capacity were considerably increased.

Fire Resistance of High Strength Concrete Pepending on Curing Method and Polypropylene fiber (양생방법 및 PP 섬유 혼입률 변화에 따른 고강도 콘크리트의 내화특성)

  • Son, Ho-Jung;Pei, Chang-Chun;Kim, Won-Ki;Han, Min-Cheol;Yang, Seong-Hwan;Han, Cheon-Goo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2009.05a
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    • pp.481-482
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    • 2009
  • This study analyzed fire resistance characteristics of high strength concrete according to changes in curing method and PP fiber content, and the results are as follows. First in case of standard curing, spalling was prevented at PP fiber content of 0.05 % or higher. Autoclave and steam curing showed prevention of spalling at content of 0.1 % or higher. For residual compressive strength, measurement of strength for plain was impossible due to spalling phenomenon. A satisfactory trend was shown with increase in PP fiber content with the strength of about 30 MPa.

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Effect of Tin on Corrosion Behavior and Precipitate Characteristics of Zr-base Alloys (Zr 합금의 부식거동 및 석출물 특성에 미치는 Sn의 영향)

  • Yeon, Yeong-Myeong;Jeong, Yong-Hwan;Wi, Myeong-Yong
    • Korean Journal of Materials Research
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    • v.7 no.9
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    • pp.772-780
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    • 1997
  • Zr-Nb-Sn 의 3원계 합금에서 Sn 함량 변화가 부식에 미치는 영향과 석출물 특성에 미치는 영향을 평가하여 신합금 개발을 위한 Sn의 최적 함유량을 도출하고자 Zr-0.4Nb-xSn(x=0.4,0.8, 1.2, 1.6)계의 4종 합금을 제조하여 여러 가지 특성시험을 실시하였다. 부식특성은 42$0^{\circ}C$ steam(1500psi)조건의 autoclave를 이용하여 시험하였으며 부식과정에서 발생하는 무게증가량을 측정하였고 산화막 특성은 X-ray를 이용하여 조사하였다. 부식관점에서 Sn량이 적을수록 내식성은 증가하는 경향을 보였다. 즉, 0.4Sn합금에서 가장 낮은 무게증가량과 1.6Sn 합금에서 가장 높은 무게 증가량을 보였다. 그러나 수소흡수성면에서는 Sn량이 많을수록 수소흡수율이 작아지는 경향을 보였다. 산화막내에서 tetra-ZrO$_{2}$량은 Sn량이 많을수록 적게 나타나는데, 이같은 결과로부터 Sn량이 많을수록 tetra-ZuO$_{2}$에서 mono-ZrO$_{2}$로의 상변태가 가속되어 Sn이 많이 함유된 합금에서 부식 저항성은 저하된다고 사료된다. Sn량이 증가함에 따라 강도는 점차적으로 증가하는 경향을 보였다. Sn량 변화에 따른 석출물의 특성을 조사한 결과, Zr-0.4Nb-xSn계 합금에서는 Sn이 석출물 형성에 거의 영향을 미치지 않으며, 또한 석출물 크기도 내식성에 커다란 영향을 미치지 않는 것을 확인하였다.

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Effective Thermal Inactivation of the Spores of Bacillus cereus Biofilms Using Microwave

  • Park, Hyong Seok;Yang, Jungwoo;Choi, Hee Jung;Kim, Kyoung Heon
    • Journal of Microbiology and Biotechnology
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    • v.27 no.7
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    • pp.1209-1215
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    • 2017
  • Microwave sterilization was performed to inactivate the spores of biofilms of Bacillus cereus involved in foodborne illness. The sterilization conditions, such as the amount of water and the operating temperature and treatment time, were optimized using statistical analysis based on 15 runs of experimental results designed by the Box-Behnken method. Statistical analysis showed that the optimal conditions for the inactivation of B. cereus biofilms were 14 ml of water, $108^{\circ}C$ of temperature, and 15 min of treatment time. Interestingly, response surface plots showed that the amount of water is the most important factor for microwave sterilization under the present conditions. Complete inactivation by microwaves was achieved in 5 min, and the inactivation efficiency by microwave was obviously higher than that by conventional steam autoclave. Finally, confocal laser scanning microscopy images showed that the principal effect of microwave treatment was cell membrane disruption. Thus, this study can contribute to the development of a process to control food-associated pathogens.