• Title/Summary/Keyword: standard reference materials

검색결과 355건 처리시간 0.033초

Study of Characteristics for Red Adhesive in Traditional Gold Thread (전통 편금사에 사용된 붉은 접착제 특성 연구)

  • Kim, Ji Eun;Yu, Ji A;Han, Ye Bin;Chung, Yong Jae
    • Journal of Conservation Science
    • /
    • 제32권1호
    • /
    • pp.43-49
    • /
    • 2016
  • Gold threads mean thread made by metal, it is composed various material to gold leaf, adhesive and media. The making technique and using materials of Gold threads are different from region, it can be used to distinguish country of origin. So this study finds characteristics and making techniques for flat gold threads of relics. Standard samples are made of animal glue, lacquer, red lacquer and etc. This materials are based on the scientific investigation of cultural gold threads properties. Then traditional techniques were estimated by comparison and analysis of actual cultural properties and standard samples. As a result of investigating cultural properties, it is similar to the standard sample which are mixed with red soil additives. After analysis of SEM-EDS, it is detected to Al, Si, Fe. So it is to the conclusion that traditional gold thread is made of adhesive mixed with red soil to improve gold color better. And this ways are similar with china that uses animal glue and red soil to adhesive and different from japan that uses lacquer to adhesive. Through this study, it will be used to data and reference for reappearance and making techniques of traditional gold threads.

A Study on the Development Type of Component Joint Design for Environment Friendly Multi Housing Remodeling (공동주택의 친환경 리모델링을 위한 부품접합부 개선방안의 유형화에 관한 연구 II;욕실 및 주방을 중심으로)

  • Lim, Seok-Ho;Kim, Soo-Am;Hwang, Eun-Kyoung;Yun, Mae-Han
    • Proceeding of Spring/Autumn Annual Conference of KHA
    • /
    • 한국주거학회 2006년도 추계학술발표대회 논문집
    • /
    • pp.370-373
    • /
    • 2006
  • Lastly, the problem of filling occurs in the process of concealed joint of adjacent components and was seen in joints between the structure and an electrical or mechanical device. Therefore, the dry processing which replaces wet joint was seen in joints between the structure and a door, ones between the structure and a finishing materials, ones between a gypsum board and electrical device, and ones between a water pipe and a tile finishing. And a process of separating the area of jointed parts in order to eliminate the problem of overlap was seen in joints between a door and a finishing material and ones between a gypsum board on the ceiling and a light. Lastly, an analysis of a process of exposing concealed parts indicated that the problem of filling could be applied to joints between the structure and an electrical or mechanical device and ones between a finishing material and a mechanical device. This study sought out methods to apply Environment Friendly Multi Housing Remodeling that allow easy remodeling as part of environment- preserving policies. It also contains basic data useful to implement long-life houses in the future by presenting a comprehensive design standard for them

  • PDF

Preconcentration and Determination of Fe(III) from Water and Food Samples by Newly Synthesized Chelating Reagent Impregnated Amberlite XAD-16 Resin

  • Tokahoglu, Serife;Ergun, Hasan;Cukurovah, Alaaddin
    • Bulletin of the Korean Chemical Society
    • /
    • 제31권7호
    • /
    • pp.1976-1980
    • /
    • 2010
  • A simple and reliable method has been developed to selectively separate and concentrate trace amounts of Fe(III) ions from water and food samples by using flame atomic absorption spectrometry. A new reagent, 5-hydroxy-4-ethyl-5,6-di-pyridin-2-yl-4,5-dihydro-2H-[1,2,4] triazine-3-thione, was synthesized and characterized by using FT-IR spectroscopy and elemental analysis. Effects of pH, concentration and volume of elution solution, sample flow rate, sample volume and interfering ions on the recovery of Fe(III) were investigated. The optimum pH was found to be 5. Eluent for quantitative elution was 10 mL of 2 M HCl. The preconcentration factor of the method, detection limit (3s/b, ${\mu}gL^{-1}$) and relative standard deviation values were found to be 25, 4.59 and 1%, respectively. In order to verify the accuracy of the method, two certified reference materials (TMDA 54.4 lake water and SRM 1568a rice flour) were analyzed. The results obtained were in good agreement with the certified values. The method was successfully applied to the determination of Fe(III) ions in water and food samples.

Satellite-detected red tide algal blooms in Korean and neighboring waters during 1999-2004

  • Ahn Yu-Hwan;Shanmugam Palanisamy
    • Proceedings of the KSRS Conference
    • /
    • 대한원격탐사학회 2006년도 춘계학술대회 논문집
    • /
    • pp.95-100
    • /
    • 2006
  • Measurements of ocean color from space since 1970s provided vital information with reference to physical and biogeochemical properties of the oceanic waters. The utility of these data has been explored in order to map and monitor highly toxic/or harmful algal blooms (HABs) that affected most of coastal waters throughout the world due to accelerated eutrophication from human activities and certain oceanic processes. However, the global atmospheric correction and bio-optical algorithms developed for oceanic waters were found to yield false information about the HABs in coastal waters. The present study aimed to evaluate the potential use of red tide index (RI) method, which has been developed by Ahn and Shanmugam (2005), for mapping of HABs in Korean and neighboring waters. Here we employed the SSMM to remove the atmospheric effect in the SeaWiFS image data and the achieved indices by RI method were found more appropriate in correctly identifying potential areas of the encountered HABs in Korean South Sea (KSS) and Chinese coastal waters during 1999-2004. But the existence of high absorbing and scattering materials greatly interfered with the standard OC4 algorithm which falsely identified red tides in these waters. In comparison with other methods, the RI approach for the early detection of HABs can provide state managers with accurate identification of the extent and location of these blooms as a management tool.

  • PDF

Evaluation of Comfort and Hand Characteristics of Lining Fabrics (안감용 직물의 태와 착용 쾌적성 평가)

  • Shim, Huen-Sup;McCullough, Elizabeth A.
    • Fashion & Textile Research Journal
    • /
    • 제10권4호
    • /
    • pp.537-543
    • /
    • 2008
  • The purpose of this study was to evaluate the comfort and fabric hand characteristics of selected lining fabrics made of acetate and polyester. The comfort of the linings was determined by human subjects wearing suit blazers constructed with different lining materials in an environmental chamber controlled at $30.6^{\circ}C$ air temperature and 50% relative humidity. The hand characteristics of the lining fabrics were determined by five trained panelists using standard fabric reference samples. The effect of lining fabrics on the subjects' thermal sensations was not statistically significant. But the subjects voted warmer when wearing the polyester surah lined blazer or the polyester taffeta blazer than wearing the acetate blazers. The results of the subjective comfort evaluation indicated that, in general, the subjects rated the acetate linings significantly less sticky, clammy, damp, and non-absorbent than the polyester linings. Acetate surah was rated a little higher than the other acetate fabrics on these comfort descriptors. The results of the subjective hand evaluation indicated that the lining fabrics rated low on the geometric and mechanical hand characteristics and rated moderate on noise. Acetate surah scored the highest on most of the hand characteristics, whereas, polyester taffeta scored the lowest.

Structure-property relations for polymer melts: comparison of linear low-density polyethylene and isotactic polypropylene

  • Drozdov, A.D.;Al-Mulla, A.;Gupta, R.K.
    • Advances in materials Research
    • /
    • 제1권4호
    • /
    • pp.245-268
    • /
    • 2012
  • Results of isothermal torsional oscillation tests are reported on melts of linear low density polyethylene and isotactic polypropylene. Prior to rheological tests, specimens were annealed at various temperatures ranging from $T_a$ = 180 to $310^{\circ}C$ for various amounts of time (from 30 to 120 min). Thermal treatment induced degradation of the melts and caused pronounced decreases in their molecular weights. With reference to the concept of transient networks, constitutive equations are developed for the viscoelastic response of polymer melts. A melt is treated as an equivalent network of strands bridged by junctions (entanglements and physical cross-links). The time-dependent response of the network is modelled as separation of active strands from and merging of dangling strands with temporary nodes. The stress-strain relations involve three adjustable parameters (the instantaneous shear modulus, the average activation energy for detachment of active strands, and the standard deviation of activation energies) that are determined by matching the dependencies of storage and loss moduli on frequency of oscillations. Good agreement is demonstrated between the experimental data and the results of numerical simulation. The study focuses on the effect of molecular weight of polymer melts on the material constants in the constitutive equations.

A Correction Method for the Peak Tailing Backgrounds for Accurate Isotope Ratio Measurements of Uranium in Ultra Trace Levels using Thermal Ionization Mass Spectrometry

  • Park, Jong-Ho;Choi, In-Hee;Park, Su-Jin;Lee, Myung-Ho;Song, Kyu-Seok
    • Bulletin of the Korean Chemical Society
    • /
    • 제32권12호
    • /
    • pp.4327-4331
    • /
    • 2011
  • A new method in thermal ionization mass spectrometry (TIMS) was developed to correct peak tailing backgrounds in the isotope ratio measurements of uranium in ultra trace levels for higher accuracy. Two different uranium standard reference materials (U005 and U030) were used to construct databases of signal intensities at mass 234 u and mass 236 u, which correspond to the two uranium minor isotopes, and signal intensity of $^{238}U$. Correlations between peak tailing backgrounds and $^{238}U$ were obtained by least-squares regression on calculated backgrounds at mass 234 u and mass 236 u with respect to the signal intensity of $^{238}U$ followed by separation of the peak tails of the two major isotopes of uranium ($^{235}U$ and $^{238}U$), which enables us to obtain a master equation for peak tailing background correction on all kinds of samples. Verification of the correction method was carried out using U010 and IRMM-040a.

Development and Evaluation of the Usefulness for Hoffman Brain Phantom Based on 3D Printing Technique (3D 프린팅 기법 기반의 Hoffman Brain 팬텀 개발 및 유용성 평가)

  • Park, Hoon-Hee;Lee, Joo-Young
    • Journal of radiological science and technology
    • /
    • 제42권6호
    • /
    • pp.441-446
    • /
    • 2019
  • The purpose of this paper is to recognize the usefulness of the Phantom produced with 3D printing technology by reproducing the original phantom with 3D printing technology. Using CT, we obtained information from the original phantom. The acquired file was printed by the SLA method of ABS materials. For inspection, SPECT/CT was used to obtain images. We filled the both Phantom with a solution mixed with 99mTcO4 1 mCi in 1 liter of water and acq uired images in accordance with the standard protocol. Using Image J, the SNR for each slice of the image was obtained. As a reference images, AC images were used. For the analysis of acquired images, ROI was set in the White mater and Gray mater sections of each image, and the average Intensity Value within the ROI were compared. According to the results of this study, 3D printed phantom's SNR is about 0.1 higher than the conventional phantom. And the ratio of Intensity Value was shown in the original 1 : 3.4, and the printed phantom was shown to be 1 : 3.2. Therefore, if Calibration Value is applied, It is assumed that it can be used as an alternative to the original.

Development of Analytical Techniques for Human Serum and Urine by Using Glow Discharge (글로우 방전을 이용한 혈청과 뇨의 분석기술 개발)

  • Lee, Sang Chun;Choi, Kyung-Soo;Son, Eun-Ho;Sim, Young-Jin
    • Analytical Science and Technology
    • /
    • 제11권3호
    • /
    • pp.167-173
    • /
    • 1998
  • An electrothermal vaporization-hollow cathode glow discharge-atomic emission spectrometer(ETV-HCGD-AES) has been developed for detecting heavy metals in human serum and urine samples. Fisrt of all, we designed a glow discharge cell for atomic emission spectrometry and its analytical performance was studied with the standard reference materials(SRMs) purchased from the NIST. Practically, the ETV-HCGD-AES demonstrated better instrumental sensitivity and selectivity for detecting Hg and Pb in the SRMs, serum and urine, than ICP-OES since the ETV-HCGD-AES was not required the complicate sample digestion procedure, which improved sample transportation efficiency.

  • PDF

Application of Methane Mixed Plasma for the Determination of Ge, As, and Se in Serum and Urine by ICP/MS

  • Park, Kyung-Su;Kim, Sun-Tae;Kim, Young-Man;Kim, Yun-je;Lee, Won
    • Bulletin of the Korean Chemical Society
    • /
    • 제24권3호
    • /
    • pp.285-290
    • /
    • 2003
  • An analytical method for the simultaneous determination of trace Ge, As and Se in biological samples by inductively coupled plasma/mass spectrometry has been investigated. The effects of added organic gas into the coolant argon gas on the analyte signal were studied to improve the detection limit, accuracy and precision. The addition of a small amount of methane (10 mL/min.) into the coolant gas channel improved the ionization of Ge, As and Se. The analytical sensitivity of the proposed Ar/CH₄system was superior by at least two-fold to that of the conventional Ar method. In the present method, the detection limits obtained for Ge, As and Se were 0.014, 0.012 and 0.064 ㎍/L, respectively. The analytical reliability of the proposed method was evaluated by analyzing the certified standard reference materials (SRM). Recoveries of 99.9% for Ge, 103% for As, 96.5% for Se were obtained for NIST SRM of freeze dried urine sample. The proposed method was also applied to the biological samples.