• 제목/요약/키워드: standard reference materials

검색결과 357건 처리시간 0.031초

환경경영시스템의 도입에 따른 중소기업의 환경경영 개선 (Improvement of Environmental Management in Small and Medium-Sized Firms through the Implementation of Environmental Management System)

  • 이근상;정혜철
    • 품질경영학회지
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    • 제32권2호
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    • pp.1-14
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    • 2004
  • As environmental issues have been become critical concerns of business, many domestic small and medium enterprises(SME's) are rapidly accepting environmental management systems(EMS) that confirm ISO 14001 guidelines. The purpose of this paper is to present the results of an empirical study carried out on a sample of certified SME's with the aim of identifying obstacles encountered in adopting ISO 14001 standards and the impact of environmental systems on corporate performance after implementation of the ISO 14001 registration process. Data from this study show that the vast majority of respondents reported environmental improvements related to the implementation of an ISO 14001 EMS, especially in the area of employees' participation of the environmental management and responsibilities for reducing negative impacts, energy and resource conservation, materials reuse, and raising top management commitment. The greatest obstacles for implementing the ISO 14001 standard are lack of cooperation and a scarcity of resources such as personnel, money, and time. Results of this study serve as a reference point understanding the problems in the implementation of ISO 14001 in other small and medium firms.

Study on the Adhesive Properties of Polyesters Reinforcing Materials

  • Krump, H.;Hudec, I.;Cernak, M.;Janypka, P.
    • Elastomers and Composites
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    • 제37권3호
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    • pp.192-194
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    • 2002
  • Polyester cord yarns have been treated in an atmospheric-pressure nitrogen plasma reactor in order to enhance their adhesion to rubber. A thin layer or the plasma was generated in the close vicinity of the yam surface using various types or surface discharge. To assess the effect of the plasma treatment on fiber surface properties, the cord thread/rubber matrix adhesion values measured using the untreated and threads cord threads were compared. The static and dynamic adhesion of the cord thread to rubber was characterized by using the standard Henley test. The dynamic adhesion values for the reference and plasma treated fiber were $7,3{\pm}1,2\;N$ and $83,5{\pm}3,5\;N$. The surface properties were investigated by scanning electron microscopy, infrared spectroscopy and electron spin resonance spectroscopy. It is concluded that both polar group interactions and increased surface area of the fibers are responsible for the improved adhesive strength.

환원기화 원자 흡광광도법에 의한 대기분진중의 총 셀렌의 정량 (Hydride Generation-Atomic Absorption Spectrophotometric Determination of Total Selenium in Atmospheric Particulate)

  • 이용근;최건형;이동수;황규자
    • 한국대기환경학회지
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    • 제6권2호
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    • pp.147-154
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    • 1990
  • A sensitive method for the determination of total selenium in aerosol particles is described. The method involves dissolution of aerosol particles by $HNO_3-HClO_4$ mixed acids, pre-reduction of Se (VI) to Se (IV) by boiling hydrochloric acid, and hydride generation followed by atomic absorption detection. Dissolved Se (IV) in 4M hydrochloric acid is reacted with $NaBH_4$ to form $H_2Se$, which is subsequently collected in an U-tube cooled in liquid nitrogen. Upon the completion of $H_2Se$ generation, the collected $H_2Se$ is rapidly vaporized into a quartz cuvette burner by removing the U-tube from liquid nitrogen, atomized, and then detected by an atomic absorption spectrophotometer. The absolute sensitivity of the method is 0.49 ng/0.0044 Abs. The accuracy of the method evaluated by analyzing standard reference materials for urban aerosol is better than 10%. Analytical results for urban and rural aerosol particles are reported.

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Development of the Graphite-Moderated Neutron Calibration Fields Using 241Am-Be Sources in JAEA-FRS

  • Nishino, Sho;Tanimura, Yoshihiko;Ebata, Yoshiaki;Yoshizawa, Michio
    • Journal of Radiation Protection and Research
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    • 제41권3호
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    • pp.211-215
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    • 2016
  • Background: The moderated neutron calibration fields using $^{241}Am$-Be sources and a graphite moderator have been constructed at the Facility of Radiation Standard (FRS) in the Japan Atomic Energy Agency (JAEA). Materials and Methods: The neutron spectra of the fields were evaluated by the Monte-Carlo calculations and measurements using the Bonner Multi-sphere Spectrometer. Results and Discussion: The fields have continuous neutron spectra from several MeV to thermal neutron energy, with fluence-averaged energies of 0.84 MeV and 0.60 MeV. Reference values of fluence rates and ambient/personal dose equivalent rates were determined from neutron spectra by measurements. Conclusion: Currently, the fields are available for calibration or performance test of neutron measuring instruments.

Load-ratio 법에 의한 SA508C-3와 알루미늄 합금의 탄소성 파괴저항 곡선평가 (Evaluation on elastic-plastic fracture resistance curve of SA508C-3 and aluminum alloy steels by load-ratio method)

  • ;윤한기;차귀준
    • 한국해양공학회지
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    • 제10권2호
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    • pp.98-105
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    • 1996
  • A method is proposed to evaluate the elastic-plastic fracture resistance curve only with load displacement records without the crack length measurement in CT specimen. This method is based on the idea that the effect of plastic deformation and the crack growth can be measured only by using a load-displacement record. If we know the reference-load curve representing the hardening of specimen, then the crack extension can be calculated by the elastic compliance determined from the load ratio. The results of this proposed method were compared to those of the elastic-plastic fracture resistance curve for the ASTM standard unloading compliance method. The experimental results for two kinds of ductile materials showed that the proposed method well simulates the material J-R curves. This method is currently applied for CT specimens. but it can be extended to the other specimen geometries.

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지하 콘크리트 구조물에 적용되는 에폭시 수지계 주입형 누수보수재료의 화학저항성능 평가 (Evaluation of Chemical Resistance of Epoxy Resin Injection Type Leakage Repairing Materials Applied to Underground Concrete Structures)

  • 박소영;김수연;오상근
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2017년도 추계 학술논문 발표대회
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    • pp.41-42
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    • 2017
  • In this study, an investigation was made to study the chemical resistance performance of epoxy resin injection type leakage repair material used in the Korean construction market in accordance to the test method outlined in "ISO TS 16774, Part 2; Test Method for Chemical Resistance." This is a new standard document used for quality control method of injection type repair material used for leakage cracking of underground concrete structures. The results of this study can be expected to be utilized as reference data that can be used for quality improvement of the maintenance methods for future construction.

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A study of neutron activation analysis compared to inductively coupled plasma atomic emission spectrometry for geological samples in Iran

  • Mohammadzadeh, Mohammad;Ajami, Mona;shadeghipanah, Arash;Rezvanifard, Mehdi
    • Nuclear Engineering and Technology
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    • 제50권8호
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    • pp.1349-1354
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    • 2018
  • Inductively Coupled Plasma Atomic Emission Spectroscopy (ICP-AES) is widely used for the determination of trace elements in geological samples in Iran. In this paper, we have calculated the detection limits of neutron activation analysis (NAA) for some of the common elements in such samples utilizing the ORIGEN and MCNP codes and verified the simulations using the experimental results of three soil standard reference materials, namely, G02.SRM, G18.SRM, and G28.SRM. The results show that while the detection limit of ICP-AES method is usually in the mg/kg range, it is represented to the ${\mu}g/kg$ range for most of the elements of interest using the NAA method, and the simulations can be verified in a tolerance range of 20%.

소형시험편의 Master Curve 방법을 이용한 원자로 압력용기강의 파괴인성 천이특성평가 (Evaluation of the Fracture Toughness Transition Characteristics of RPV Steels Based on the ASTM Master Curve Method Using Small Specimens)

  • 양원존;허무영;김주학;이봉상;홍준화
    • 대한기계학회논문집A
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    • 제24권2호
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    • pp.303-310
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    • 2000
  • Fracture toughness of five different reactor pressure vessel steels was characterized in the transition temperature region by the ASTM E1921-97 standard method using Charpy-sized small specimens. T he predominant fracture mode of the tested steels was transgranular cleavage in the test conditions. A statistical analysis based on the Weibull distribution was applied to the interpretation of the scattered fracture toughness data. The size-dependence of the measured fracture toughness values was also well predicted by means of the Weibull probabilistic analysis. The measured fracture toughness transition curves followed the temperature-dependence of the ASTM master curve within the expected scatter bands. Therefore, the fracture toughness characteristics in the transition region could be described by a single parameter, so-called the reference temperature (T。), for a given steel. The determined reference temperatures of the tested materials could not be correlated with the conventional index temperatures from Charpy impact tests.

장비정도관리에 Calibrator[I-125] Set 적용 (The Application of New Calibrator[I-125]Set for Equipment Quality Management)

  • 김지나;안재석;원우재
    • 핵의학기술
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    • 제19권2호
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    • pp.108-111
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    • 2015
  • Purpose Lately, in accordance with the increasing interest about Healthcare accreditation program and International laboratory accreditation scheme, requirements about the instrument quality management are gradually taking shape. In nuclear medicine In vitro laboratory, the most typical instruments are multi detector gamma counter and automatic dispensing system. Each laboratory continue with the quality control adequate for circumstances. The purpose of this study is to application and establish the new Calibrator[I-125]Set which is efficient at standardization of equipment quality management. Materials and Methods Deviation between detectors were measured with 12 solid samples of the Calibrator[I-125]Set. their activities differ from each other by less than 1%. Multi detector gamma counters are GAMMA-10;Shinjin medics. Inc, Goyansi, Korea(Gamma counter A), SR300;Stratec biomedical systems AG, Gewerbestr, Germany(Gamma counter B) and COBRA II; Packard Instrument Co. Inc, Meriden, USA(Gamma counter C). Evaluation of two automatic dispensing system used A, B liquid tracer of the Calibrator[I-125]Set. After dispensing and counting, calculated using the ratio of the measured value and proposed value. We used solution A for 20, 25ul and solution B for 50, 100ul. Method of data analysis and reference range was provided by kit documentation. Furthermore, we could calculate our counter efficiency indirectly. Results The CV(%) of measured values by Gamma counter A, B, C are 0.34, 0.70, 1.30. Calculated value are 1.05314, 2.10419, 4.08485. Provided reference range is less than 3. A dispensing system's calculated values are 0.986, 0.989, 1.023, 1.017 and B are 0.874, 0.725, 1.021, 0.904. Provided reference range is from 0.95 to 1.05. Also, counter's efficiency are 74.18, 72.79, 74.32% at counter A, B, C and efficiency of the one detector counter is 79.26%. Conclusion If using this Calibrator[I-125]Set after verifying whether quality assurance, is applicable to equipment quality management on behalf of the role of gold standard.

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중금속분석용 폐수표준물질 제조 및 실험실간 비교평가 (Preparation of wastewater-based reference materials for heavy metal analysis and interlaboratory study)

  • 김영희;송기봉;신선경;이정섭;정기택;홍은진;박진주;유석민
    • 분석과학
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    • 제23권3호
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    • pp.295-303
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    • 2010
  • 폐수 시료를 이용한 중금속분석용 수질표준물질을 제조하여, 납, 카드뮴, 크롬, 구리, 아연, 망간, 철 등 중금속 7 종에 대해 인증분석 및 불확도 등을 평가하고, 24 개 환경측정분석기관을 대상으로 실험실간 비교실험을 실시하였다. 폐수표준물질의 인증값 및 확장불확도는 KS A ISO 가이드 35(2005)에 의해 도출하였으며, 균질성에 기인한 표준불확도는 특성값의 0.43~2.67%로 나타났다. 환경측정분석기관간 비교실험에서 모든 항목의 비교실험 결과값이 정규분포를 따랐으며, 로버스트 평균값과 폐수표준물질의 인증값과 비교한 결과, 대부분의 항목에서 로버스트 평균값이 인증값보다 낮게 나타났다.