• Title/Summary/Keyword: spherical particle

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Synthesis of FePt Nanoparticles by Chemical Reduction Process (화학적인 환원 공정에 의한 FePt 나노입자의 합성)

  • 김순길;이창우;이재성
    • Journal of Powder Materials
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    • v.11 no.3
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    • pp.242-246
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    • 2004
  • FePt nanoparticles for high-density magnetic recording media were synthesized by the simultaneous chemical reduction of Fe(acac) $_2$ and Pt(acac) $_2$ with 1,2-hexadecanediol as the reducing reagent. TEM images showed that the shape of as-synthesized FePt nanoparticle was spherical and average particle size was 3 nm. Also, SAD pattern showed that crystal structure was disordered FCC (face centered cubic). These FCC structured nanoparticles were transformed FCT (face centered tetragonal) structure by annealing at 55$0^{\circ}C$ for 30 min in Ar atmosphere. XRD analysis revealed that as-synthesized FePt nanoparticles were transformed from disordered FCC to ordered FCT. Finally, the coercivity of 2 kOe for FePt nanoparticles with FCT structure was obtained by VSM measurement.

Liquid mist and videotape signal dropouts in gravure roll coating (Gravure롤 코팅방식에서 비산도료에 의한 비디오 신호의 dropouts)

  • 김명룡
    • Electrical & Electronic Materials
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    • v.8 no.5
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    • pp.633-639
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    • 1995
  • Dropouts in magnetic media are a primary quality deficiency which is detrimental to magnetic signal quality and thus the major impediment to error-free recording, especially in high density digital recorders. The specific form of defects and causes found to be responsible for signal dropouts occurring in magnetic tape were studied. Dropout occurred when the RF signal falls to low level due to the various types of surface defects. However, the fall in the level of the RF signal in gravure roll coated tapes was most often caused by foreign particles adhering to the magnetic tape. It was also shown from the present study that scattered particles trapped under the tape surface or put on the top can lift it as it crosses the head, creating a spherical tent shaped defect and causing a temporary signal drop. Dropout producing substances were identified through optical and microchemical analyses. The results were correlated with measured electrical signal losses combined with analytical microscopy to clarify source identification of defects.

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Determination of DEM Input Parameters for Dynamic Behavior Simulation of Aggregates (골재의 동적 거동 모사를 위한 DEM 입력변수의 결정 연구)

  • Yun, Tae Young;Yoo, Pyeong Jun;Kim, Yeon Bok
    • International Journal of Highway Engineering
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    • v.16 no.1
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    • pp.21-30
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    • 2014
  • PURPOSES : Evaluation of input parameters determination procedure for dynamic analysis of aggregates in DEM. METHODS : In this research, the aggregate slump test and angularity test were performed as fundamental laboratory tests to determine input parameters of spherical particles in DEM. The heights spreads, weights of the simple tests were measured and used to calibrate rolling and static friction coefficients of particles. RESULTS : The DEM simulations with calibrated parameters showed good agreement with the laboratory test results for given dynamic condition. CONCLUSIONS : It is concluded that the employed calibration method can be applicable to determine rolling friction coefficient of DEM simulation for given dynamic conditions. However, further research is necessary to connect the result to the behavior of aggregate in packing and mixing process and to refine static friction coefficient.

Preparation of Silica-Gold Composite particles (실리카-골드 복합체의 합성 연구)

  • Kim, Dae-Wook;Shim, Seung-Bo;Chun, Yong-Jin
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.11
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    • pp.5365-5369
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    • 2011
  • Silica-gold composite particles were prepared by wet chemical route including impregnation method. The effect of precursor and solvent on the preparation of silica-gold particles was investigated. When spherical silica particles and PVP and hydrogentetrachloroaurate(III) hydrate aqueous solution were used as support material and precursor solution, silica-gold composite particles with light pink color successfully obtained. Obtained composite particles were characterized using FE-SEM, FE-TEM and XRD.

Neutron Cross Section Evaluation on Dy Isotopes

  • Lee, Y. D.;J. H. Chang
    • Nuclear Engineering and Technology
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    • v.34 no.2
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    • pp.154-164
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    • 2002
  • Neutron cross section data on Dy-160, Dy-161, Dy-162, Dy-163 and Dy-164 were calculated and evaluated in the energy range of 1 keV to 20 MeV using a spherical optical model, statistical model and pre-equilibrium model. The energy dependent optical model potential parameters were obtained based on the recent experimental data. The width fluctuation correction in Hauser-Feshbach particle decay and the quantum mechanical approach in pre-equilibrium analysis were introduced and gave a better cross section calculation in EMPIRE-II. The total, elastic scattering and threshold reaction cross sections were evaluated and compared with the evaluated files. The model calculated (n, tot), (n, ${\gamma}$) and (n, p) cross sections were in good agreement with the experimental data in the measured energy range. The results will be applied to ENDF/B-VI for data improvement.

Opto-electrokinetic Technique for Microfluidic Manipulation of Microorganism (광-전기역학 기술을 이용한 미생물의 미세유체역학적 제어)

  • Kwon, Jae-Sung
    • Journal of the Korean Society of Visualization
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    • v.17 no.1
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    • pp.69-77
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    • 2019
  • This paper introduces microfluidic manipulation of microorganism by opto-electrokinetic technique, named rapid electrokinetic patterning (REP). REP is a hybrid method that utilizes the simultaneous application of a uniform electric field and a focused laser to manipulate various kinds and types of colloidal particles. Using the technique in preliminary experiments, we have successfully aggregated, translated, and trapped not only spherical polystyrene, latex, and magnetic particles but also ellipsoidal glass particles. Extending the manipulation target to cells, we attempted to manipulate saccharomyces cerevisiae (S. cerevisiae), the most commonly used microorganism for food fermentation and biomass production. As a result, S. cerevisiae were assembled and dynamically trapped by REP at arbitrary location on an electrode surface. It firmly establishes the usefulness of REP technique for development of a high-performance on-chip bioassay system.

Tribological and Mechanical Properties of UHMWPE/HDPE Composites

  • Na, Woo Seok;Lee, Kwang Ho;Kong, Tae Woong;Baek, Jung Youn;Oh, Jeong Seok
    • Elastomers and Composites
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    • v.53 no.4
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    • pp.234-238
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    • 2018
  • The influence of reinforcing UHMWPE powder on the tribological and mechanical properties of HDPE was investigated. The circularizing of UHMWPE powder was improved by high-speed rotation to enhance particle distribution and flowability. HDPE composites reinforced with UHMWPE powder in the range of 0-50 wt% were prepared by co-rotating twin screw extrusion. The abrasion resistance, plane friction coefficient, tensile strengths, and impact strengths of the composites were investigated as a function of the UHMWPE content. An increasing UHMWPE content decreased the plane friction coefficient and increased the abrasion resistance and impact strength. It is expected that HDPE composites reinforced with spherical UHMWPE powder particles can be used to improve the durability of products such as pipes in the future.

Heat Transfer from a Sphere in Fluctuating Flow (맥동류에 놓인 구로부터의 열전달)

  • Kwon Young-Pil;Lee Kye-Cheul
    • The Magazine of the Society of Air-Conditioning and Refrigerating Engineers of Korea
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    • v.16 no.2
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    • pp.185-193
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    • 1987
  • The heat transfer characteristics from a solid sphere in a fluctuating air flow is simulated numerically in the range of the Reynolds numbers, $1\;{\leqslant}\;Re\;{\leqslant}\;40.$ Such a situation may be encountered in forced convection from a heated spherical particle in a sound field or oscillat-ing flow. The amplitude and phase delay in the heat transfer response to the flow oscillation are computed for a small amplitude flow. The instantaneous response of heat transfer is simulated for the large amplitude oscillation and compared with the quasi-steady response. The effect of the oscillation on the time - mean value in the local and overall heat transfer rate is discussed along with the change in the flow .field.

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Morphology Control of NTO Crystals with Various Recrystallization Techniques

  • Lee, H.Y.;K.K. Koo;Kim, K.J.;G.B. Lim;W.B. Jeong;Kim, S.H.;Kim, H.S.;Park, B.S.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1997.10a
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    • pp.123-127
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    • 1997
  • Various recrystallization techniques has been applied to control morphology and size of NTO(3-nitro-1, 2, 4-triazole-5-one) crystals. With cooling method, it was found that the size of NTO at aqueous solution was controlled in the range of 5 to 500 $\mu\textrm{m}$. The spherical or cubic shapes of particles were obtained by adjusting operating conditions. Hexagonal and cubic shaped crystals of NTO were also obtained by sonication and evaporative method using aqueous solution of NTO. Their particle sizes were ranged 20 to 30 $\mu\textrm{m}$. In gas anti-solvent method with NTO/DMF and NTO/DMSO solutions, cubic type of NTO was obtained and the range of their sizes was 0.5-2$\mu\textrm{m}$.

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The Studies on synthesis of $SnO_2$ doped $In_2O_3$ (ITO: Indium Tin Oxide) powder by spray pyrolysis (분무열분해법(Spray Pyrolysis)에 의한 주석산화물이 도핑된 $In_2O_3$(ITO: Indium Tin Oxide)의 분말 제조에 대한 연구)

  • Kim, Sang Hern
    • Journal of the Korean Applied Science and Technology
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    • v.31 no.4
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    • pp.694-702
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    • 2014
  • The micron-sized ITO(indium tin oxide) particles were prepared by spray pyrolysis from aqueous precursor solutions for indium, and tin and organic additives solution. Organic additives solution with citric acid(CA) and ethylene glycol(EG) were added to aqueous precursor solution for Indium and Tin. The obtained ITO particles prepared by spray pyrolysis from the aqueous solution without organic additives solution had spherical and filled morphologies whereas the obtained ITO particles with organic additives solution had more hollow and porous morphologies with increasing mole of organic additives. The micron-sized ITO particle with organic additives was changed fully to nano-sized ITO particle whereas the micron-sized ITO particle without organic additives was not changed fully to nano-sized ITO particle after post-treatment at $700^{\circ}C$ for 2 hours and wet-ball milling for 24 hours. The size of primary ITO particle by Debye-Scherrer formula and surface resistance of ITO pellet were measured.