• Title/Summary/Keyword: solution coating method

Search Result 549, Processing Time 0.03 seconds

Fabrication of Transparent Heat-element using Single- Walled Carbon Nanotubes

  • Jeong, Hyeok;Vanquy, Nguyen;Lee, Han-Min;Kim, Dong-Hyeon;Kim, Do-Jin
    • Proceedings of the Materials Research Society of Korea Conference
    • /
    • 2009.05a
    • /
    • pp.31.2-31.2
    • /
    • 2009
  • In this research, single walled carbon nano-tube film was manufactured with spray coating method on glass for application as transparent heat element. SWNTs solution to be used for spraying is obtained by dispersion of 0.01 wt% purified SWNTs in dimethylformamide (DMF) solution through ultrasonification and centrifugation. The transmittance and sheet resistance of SWNTs film were determined by the number of spray injection. Manufactured SWNTs film will have sheet resistance range of $200\;\Omega/\square-900\;\Omega/\square$ at transmittance range of 70-90 %. Heat generation characteristic of SWNTs film was measured by applying constant DC voltage of 15V. The result confirmed that SWNTs film with sheet resistance of $200\;\Omega/\square$ reaches surface temperature of $80^{\circ}C$ within several seconds. In addition, PET coating film was coated on top of the SWNTs film by using laminator in order to solve weak adhesive property of the spray coated SWNTs film on the substrate as well as to maintain its electrical and optical properties.

  • PDF

Effect of nano-sized powder addition on the microstructure and superconducting properties of the YBCO thin film. (나노분말 첨가에 따른 YBCO 초전도 박막의 미셀구조 및 초전도 특성변화 연구)

  • Park, Jin-A;Kim, Byung-Joo;Im, Sun-Won;Ahn, Ji-Hyun;Kim, Ho-Jin;Hong, Gye-Won;Lee, Hee-Gyun
    • Proceedings of the KIEE Conference
    • /
    • 2005.07c
    • /
    • pp.1998-2000
    • /
    • 2005
  • The effects of the addition of nanocrystalline Y2O3 powder on the microstructure and superconducting properties have been investigated in YBCO films prepared by TFA-MOD process. Precursor solution doped with extra $Y_2O_3$ Powder was prepared by adding $Y_2O_3$ powder into a stoichiometic precursor solution with a cation ratio of Y:Ba:Cu=1:2:3. Coating solutions with and without $Y_2O_3$ doping were coated on $LaAlO_3(100)$ single crystal by a dip coating method, cacination and conversion heat treatments were performed at the controlled atmosphere containing water vapor Current carry capacity(Jc) of YBCO film was enhanced about 50% by $Y_2O_3$ doping. It is thought that the enhancement of Jc is due to the better connectivity of YBCO grains and/or the flux pinning by the presence of nanocrystalline $Y_2O_3$ Particles embedded in YBCO grains.

  • PDF

Preparation and structural properties of the Pb(Zr, Ti)${O}_{3}$ thin film by Sol-Gel method (Sol-Gel 법에 의한 Pb(Zr, Ti)${O}_{3}$ 박막의 제조 및 구조적 특성)

  • 이영준;정장호;이성갑;이영희
    • The Transactions of the Korean Institute of Electrical Engineers
    • /
    • v.44 no.7
    • /
    • pp.914-918
    • /
    • 1995
  • In this study, Pb(Zr$_{x}$ Ti$_{1-x}$ )O$_{3}$ (x=0.65, 0.52, 0.35) thin films were fabricated by Sol-Gel method. A stock solution with excess Pb 10[mol%] of Pb(Zr$_{x}$ Ti$_{1-x}$ )O$_{3}$ was made and spin-coated on the Pt/SiO$_{2}$/Si substrate at 4000[rpm] for 30[sec.]. Coated specimens were dried on the hot-plate at 400[.deg. C] for 10[min.]. Sintering temperature and time were 500~800[.deg. C] and 1~60[min.]. The coating process was repeated 6 times and the final thickness of the thin films were about 4800[A]. To investigate crystallization condition, PZT thin films were analyzed with sintering temperature, time and composition by the XRD. The microstructure of thin fulms were investigated by SEM. The ferroelectric perovskite phases precipitated under the sintering of 700[.deg. C] for 1 hours. In the PZT(52/48) composition, dielectric constant and dielectric loss were 2133, 2.2[%] at room temperature, respectively.ively.

  • PDF

Electrochromic Performance of NiOx Thin Film on Flexible PET/ITO Prepared by Nanocrystallite-Dispersion Sol

  • Kwak, Jun Young;Jung, Young Hee;Park, Juyun;Kang, Yong-Chul;Kim, Yeong Il
    • Journal of the Korean Chemical Society
    • /
    • v.65 no.2
    • /
    • pp.125-132
    • /
    • 2021
  • An electrochromic nickel oxide thin film was fabricated on a flexible PET/ITO substrate using a nanocrystallite- dispersed coating sol and bar coater. Nanocrystalline NiOx of 3-4 nm crystallite size was first synthesized by base precipitation and thermal conversion. This NiOx nanocrystallite powder was mechanically dispersed in an alcoholic solvent mixed with a silane binder to prepare a coating sol for thin film. This sol method is different from the normal sol-gel method in that it does not require the conversion of precursor by heat treatment. Therefore, this method provides a very facile method to prepare NiOx thin films on any kind of substrate and it can be easily applied to mass production. The electrochromic performance of this NiOx thin film on PET/ITO electrode with a thickness of about 400 nm was investigated in a nonaqueous LiClO4 electrolyte solution by cyclic voltammetric and repeated chronoamperometric measurements in conjunction with spectrophotometry. The visible light modulation of 44% and the colorization efficiency of 41 ㎠/C at 550 nm were obtained at the step potentials of -0.8/+1.2 V vs Ag and a duration of 30 s.

The Development of Partial Model for Thermo-Mechanical Stress Analyses of Part with Coated Layer under Contact Load (접촉하중을 받는 코팅층이 있는 부재의 응력해석을 위한 부분 모델 방법의 개발)

  • Kwon, Young-Doo;Kim, Seock-Sam;Goo, Nam-Seo;Park, Jung-Gyu
    • Tribology and Lubricants
    • /
    • v.18 no.3
    • /
    • pp.194-203
    • /
    • 2002
  • This paper is the first step fur thermo-mechanical stress analyses of part with coated layer under contact load. A lot of coated material is applied in many structures to endure severe situation, like thermal stresses, high temperature gradients, irradiation, impacts by microscopic meteorites, and so on. In this part we are going to apply the FEM to analyze space parts with a coated layer subjected to a contact load thermo-mechanically. Coating layer is very thin in comparision with the structure, therefore it should take more times and behaviors to analyze whole model. In these reason we develop the FEM method of analyzing part with coated layer under contact load using partial model. Steady state temperature distribution of the part is obtained first, and then we apply quasi-static external load on the part. To obtain the final stage of solution, we compute the total solution, and by subtracting the thermal strain from the total ones we get the mechanical strains to compute stresses of the parts. In using the FEM, one has to discretize the model into many sub-domain, finite elements. The method is consisited of two steps. First step is to analyze the whole model with rather coarse meshes. Second step we cut a small region near the loading point, and analyze with very fine meshes. This method is allowable by the Saint-Venant's principle. And then, we finally shall check the therma1 load on the stresses of the space part with coating layer with or without substrate cracks. Then, we predict the actual behaviors of the part used in space.

EM wave scattering by bianisotropically coated multilayer cylinder with an impedance sheet[II] (쌍이방성 매질 코팅 다층 원통에 의한 전자파 산란 해석[II])

  • 엄상진;윤중한;이화춘;곽경섭
    • The Journal of Korean Institute of Communications and Information Sciences
    • /
    • v.26 no.4B
    • /
    • pp.391-399
    • /
    • 2001
  • In this paper, electromagnetic wave scattering from a bianisotropicaly coated cylinder is formulated by using wave functions for bianisotropic media and boundary-value method. The cross section of the cylinder is made of a conducting core, a lossless dielectric layer which is both electrically magnetically bianisotropic, and a bianisotropic impedance sheet and a different uniaxial bianisotrpic coating. The solutions to arbitrary polarization angles are presented in two-dimensional. This paper presents and exact solution to the problem of scattering by a long composite circular cylinder using the boundary method. The validity of this solution is verified by comparing numerical results with those in literature. The numerical results for various geometrical and electrical parameters on bistatic scattering cross-section are presented.

  • PDF

Zinc oxide seed layer 형성 조건 제어를 통한 나노 구조체 형상 조절 연구

  • Lee, Jae-Hyeok;Kim, Seong-Hyeon;Lee, Gyeong-Il;Lee, Cheol-Seung;Jo, Jin-U;Kim, Seon-Min
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2011.02a
    • /
    • pp.386-386
    • /
    • 2011
  • sol-gel 및 hydrothermal growth method를 이용한 zinc oxide nanorod는 제작 시 고가의 장비가 필요치 않기에 저비용 대면적 박막을 제작하는데 적합하지만 rod들의 array 및 density 조절에서 어려움을 가지고 있다. 본 연구에서는 이러한 nanorod array 형상 조절을 위하여 zinc oxide seed layer 형성 과정 중 precursor solution에 이종 나노 입자를 첨가하였다. 첨가한 seed precursor solution을 spin coating한 이후에 후처리 하여 hydrothermal method를 이용해 성장시켰다. 합성한 rod들을 optic과 FE-SEM으로 측정해 rod들의 density 변화를 확인할 수 있었다.

  • PDF

TWO-DIMENSIONAL STAGNATION FLOW TOWARD A PLANE WALL COATED WITH MAGNETIC FLUID OF UNIFORM THICKNESS (균일 두께의 자성유체 피막이 있는 평면 벽을 향하는 2차원 정체 유동)

  • Ko, Hyung-Jong;Kim, Kyoung-Hoon;Kim, Se-Woong
    • Journal of computational fluids engineering
    • /
    • v.12 no.4
    • /
    • pp.20-27
    • /
    • 2007
  • Two-dimensional stagnation flow toward a plane wall coated with magnetic fluid of uniform thickness is investigated. The flow field is represented as a similarity solution of the Navier-Stokes equation for this incompressible laminar flow. The resulting third order ordinary differential equation is solved numerically by using the shooting method and by determining two shooting parameters so as to satisfy the boundary and interface conditions. Features of the flow including streamline patterns are investigated for the varying values of density ratio, viscosity ratio, and Reynolds number. An adverse flow with double eddy pair in magnetic fluid region is found to emerge as the Reynolds number becomes higher than a threshold value. The results for the interface velocity, interface and wall shear stress, and boundary layer and displacement thickness are also presented.

Axisymmetric bending of a circular plate with stiff edge on a soft FGM layer

  • Volkov, Sergey S.;Litvinenko, Alexander N.;Aizikovich, Sergey M.;Wang, Yun-Che;Vasiliev, Andrey S.
    • Structural Engineering and Mechanics
    • /
    • v.59 no.2
    • /
    • pp.227-241
    • /
    • 2016
  • A circular plate with constant thickness, finite radius and stiff edge lying on an elastic halfspace is considered. The half-space consists of a soft functionally graded (FGM) layer with arbitrary varying elastic properties and a homogeneous elastic substrate. The plate bends under the action of arbitrary axisymmetric distributed load and response from the elastic half-space. A semi-analytical solution for the problem effective in whole range of geometric (relative layer thickness) and mechanical (elastic properties of coating and substrate, stiffness of the plate) properties is constructed using the bilateral asymptotic method (Aizikovich et al. 2009). Approximated analytical expressions for the contact stresses and deflections of the plate are provided. Numerical results showing the qualitative dependence of the solution from the initial parameters of the problem are obtained with high precision.

Preparation and Characterization of Spherical Silica-coated Ceria Nanoparticles by Sol-Gel Method

  • Ahn, Yang-Kyu;Jeoung, Hae-Chan
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2010.02a
    • /
    • pp.96-96
    • /
    • 2010
  • Monodispersed spherical silica-coated ceria nanoparticles were prepared through a sol-gel process using tetraethylorthosilicate (TEOS) and ceria fine particles. In this process, ceria fine particles were also prepared from cerium nitrate. The mean size of ceria particles was 300nm. Silica nanoparticles with narrow particle size distribution were prepared by controlled hydrolysis of TEOS solution. The silica sols were obtained by peptization, the process of redispersing a coagulated colloid, and were coated on ceria particles by the control of the weight ratio of silica/ceria and the pH of the mixture in aqueous solution. The morphologies of particles were characterized with scaning electron microscopy(SEM), transmission electron microscopy(TEM) and atomic force microscopy(AFM). The coating thickness of silica particles obtained by using this method was controlled in the range of 30 - 70nm.

  • PDF