• 제목/요약/키워드: solid-water ratio

검색결과 364건 처리시간 0.023초

Extraction of β-glucosidase from Bagasse Fermented by Mixed Culture under Solid State Fermentation

  • Shata, Hoda Mohamed Abdel Halim;Farid, Mohamed Abdel Fattah
    • Journal of Applied Biological Chemistry
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    • 제57권3호
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    • pp.197-203
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    • 2014
  • Various parameters such as solvent selection, concentration, solid/liquid ratio, soaking time, temperature, stationary, shaking conditions, and repeated extractions were investigated in order to determine the optimum extraction conditions of ${\beta}$-glucosidase from bagasse fermented by mixed culture of Aspergillus niger NRC 7A and Aspergillus oryzae NRRL 447. Among various solvents tested, non ionic detergents gave the best results than the inorganic or organic salt solutions and distilled water. The optimum conditions for extraction of ${\beta}$-glucosidase were 30 min soaking time at $40^{\circ}C$ under shaking condition at 150 rpm, with solid/liquid ratio 1:15 (w/v), which yielded $2882.74{\pm}95.52U/g$ fermented culture (g fc) of enzyme activity. With repeated washes under the above optimum conditions, the results showed that enzyme extracted in the $1^{st}$ and $2^{nd}$ washes represents about 90% of the total activity.

섬유상 고상 추출물질을 이용한 알킬페놀 화합물 분석 가능성 (Feasibility of Fibrous Solid Phase Extraction to Alkylphenols Analysis)

  • 정용준
    • 한국물환경학회지
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    • 제27권3호
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    • pp.329-333
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    • 2011
  • 흡착제로서의 PBO 섬유가 수용성 알킬페놀 화합물의 고상 추출용으로 사용되었다. 초기농도 $100{\mu}gL^{-1}$ 에서 10 종류의 알킬페놀에 대한 제거율은 16.8~96.3%였고, 제거율은 섬유무게/액체부피비의 증가에 따라 증가하였다. log K는 log P와 일치하였다. 흡착된 알킬페놀은 아세트니트릴과 디클로로메탄의 혼합액으로 충분히 탈착되었다.

납슬러지 고형화 및 용출 특성 (The Characteristics of Solidification and Leachability of Lead Sludge)

  • 연익준;주소영;김광렬
    • 환경위생공학
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    • 제14권3호
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    • pp.22-30
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    • 1999
  • This study was carried out to examine the compressive strength characteristics of solids solidified with the lead sludge with mixture of cement and fly ashes as additive. And the additives are commercial fly ash and ESP(Electrostatic precipitator) fly ash. The compressive strength of solidified lead sludge solid was increased by adding fly ash up to 46~62%, which was the results of pozzolanic reaction. When replaced the cement with 10%of commercial fly ash, the solid showed the highest value $210{\;}kg/cm^2$, and the solidification conditions were 0.55 of the water/cement ratio and curing for 14 days. Also, the results of leaching test by EPT(Environmental Protection Agency-Toxicity Test) were showed that the solidified lead has leached out under 10%, which was less than 0.173 mg/L of EPA standard. As leaching solutions, the demineralized water, 0.1N acetic acid solution, and synthetic brine were used. and the observations by SEM of the solidified lead-laden solid after EPT leaching test were indicated the severe erosion on solid surface.

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다양한 분체를 이용한 W/O와 O/W 형 에멀젼의 안정화 (Stability of W/O and O/W Type Emulsions by Various Solid Particles)

  • 이상길;김영호;표형배;이동규
    • 한국응용과학기술학회지
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    • 제27권3호
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    • pp.353-360
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    • 2010
  • This study was carried out to investigate the possibility of solid particles as a stabilizing agent instead of surfactant for preparing emulsions in the cosmetics. The type of emulsions stabilized by solid particles was dependent on wettability of the particles for water and oil. The optimal conditions of emulsions stabilized by solid particles were determined with ratio of water and oil phase, polarity of oils and amount of stabilizers. In the foundation appling the optimal condition of emulsions stabilized by solid particles without surfactant, the stable emulsion type foundation was successfully prepared. As a result, this work indicates that emulsions stabilized by solid particles can be applied to make-up cosmetics.

케토프로펜-${\beta}$-시클로덱스트린 고체분산체의 마이크로캅셀화 및 제어 방출 (Preparation and Controlled Release of Microcapsules Containing $Ketoprofen-{\beta}-Cyclodextrin$ Solid Dispersion)

  • 전인구;박정화
    • Journal of Pharmaceutical Investigation
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    • 제22권1호
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    • pp.33-40
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    • 1992
  • This study was aimed to control the release characteristics of ketoprofen by microencapsulating $ketoprofen-{\beta}-cyclodextrin\;(KF-{\beta}-CyD)$ solid dispersion with Eudragit RS by the phase separation method using a nonaqueous vehicle. KF alone was also microencapsulated with Eudragit RS by the evaporation process in water phase. The results obtained showed that it was not possible to microencapsulate KF alone by phase separation in a chloroform-cyclohexane system while it was easy to microencapsulate $(KF-{\beta}-CyD)$ solid dispersion system. For the microcapsules, the release test was performed in the first fluid (pH 1.2) and the second fluid (pH 6.8) of K.P.V disintegration medium at $37^{\circ}C$. The release of KF from $(KF-{\beta}-CyD)$ solid dispersion microcapsules (1:1 core wall ratio) was more sustained than that from KF microcapsules, and followed zero-order kinetics. Especially, solid dispersion microcapsules showed pH-independent release patterns with higher wall to core ratio (1:1 w/w).

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Tricalcium Silicate의 초기수화반응(I) (Early Hydration of Ticalcium Silicate(I))

  • 오희갑;최상흘
    • 한국세라믹학회지
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    • 제23권5호
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    • pp.35-40
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    • 1986
  • The early hydration of tri-calcium silicate $(C_3S)$ with different cooling conditions was studied by varing water/solid ratio and atmosphere. The cooling condition and water/solid ratio affected to the second peak of heat liberation but it had no correlation to the induction period. The $Ca^{2+}$ concentration in the aqueous solution was maximized at the starting point of the second peak of heat liberation but in the $CO_2$ exsistence the $Ca^{2+}$ concentration was low and $SiO_2$ con-centration was increased. The hydration rate of $C_3S$ was so accelerated that the induction period could not appear in the $CO_2$ exsistence.

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충진층식 스크러버의 스프레이 시스템 최적 설계에 대한 수치해석적 연구 (NUMERICAL STUDY ON THE OPTIMAL DESIGN OF SPRAY SYSTEM IN PACKED BED SCRUBBER)

  • 고승우;노경철;유홍선
    • 한국전산유체공학회지
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    • 제12권1호
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    • pp.28-34
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    • 2007
  • This study evaluates the performance of the packed bed scrubber and proposes the optimization of spray system for improvements of collection efficiency. The packed bed scrubber is used primarily in the semiconductor manufacturing process. The mean diameter of entering solid particles in scrubber is the submicron. The impaction between water droplets and solid particles is an important factor in removing the solid particles. Thus, the coverage area of spray system influences on the collection efficiency. The collection efficiency of a single droplet is calculated through the mathematical model and numerical calculations are performed for coverage area for each nozzle type (Droplet diameters: 500, 319.5, $289.5{\mu}m$) and injected directions (0, 15, $30^{\circ}$). In case of nozzle type 3, the collection efficiency of a single droplet is highest but the collection efficiency of spray system has lowest value because the ratio of flow rate between the gas and water is below 0.1. The results show the coverage area ratio is about 85% in the case of nozzle type 3 and downward sirection $15^{\circ}$. It was shown that a coverage area increase by two times than an existing spray system. In simulation of demister, collection efficiency by demister is predicted about 80% and the pressure drop in demister is below 3.5 Pa.

내화물 슬레이트용 고체윤활제의 연구 (Studies on solid inflammable lubricants for refractory slates)

  • 노승백;이학일;손기훈
    • 한국산학기술학회논문지
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    • 제16권3호
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    • pp.2308-2313
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    • 2015
  • 본 논문은 내화물 슬레이트용 고체윤활제를 제조하기 위하여 Starch 및 Graphite의 함량 변화를 통하여 점도, 마찰계수 및 마모성능을 평가하여 Starch, Graphite와 water 간의 적절한 함량 조합을 찾고자 하였다. 먼저 starch 15 wt%일 때 점도는 graphite 함량에 따라 점도 상승이 커짐을 알 수 있었다. 또한 마찰계수 시험에서는 starch 15 wt%이고, graphite 30 wt%일 때 마찰계수가 가장 적었다. 이는 물의 함량이 줄어들고 고체의 비율이 높아짐에 따라 흡착력이 낮아져 표면에서 피막이 조금씩 탈락되며 마찰계수가 상승하는 것으로 판단된다. 마모 시험결과 starch 15 wt%이면서, graphite 25 wt% 혹은 30 wt%일 때 가장 양호한 결과를 얻었다.

Aspergillus niger 의 고체상태 발효 시스템에서의 β-Glucosidase 회수 (β-Glucosidase Recovery from a Solid-State Fermentation System by Aspergillus niger)

  • 수보쉬 찬드라;라자세카 레디;최용락
    • 생명과학회지
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    • 제20권7호
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    • pp.999-1004
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    • 2010
  • 밀기울 발효에서 효소회수의 모델로 Aspergillus niger를 고체상태로 발효시켜 조사하였다. 발효시킨 밀기울에서 증류수로 효소추출 효율은 초산 완충액, 구연산 완충액, 구연산-인산 완충액 및 5% 메탄올 처리보다 높았다. 따라서, 추출 용매로 증류수를 이용하여 최적 조건을 상세히 검토하였다. 최적 조건은 고체와 액체 용매를 1:5의 비율로 증류수로서 세 번 세척하였을 때에 최대 회수율을 0.025 U/g으로 확보하였다.

Molecular Weight Distribution of Liquid Phase AN and Solid Phase Polymer in Precipitation Polymerization of AN By Changing Solution Composition and Temperature

  • Liu, Weiwei;Zhang, Shuangkun;Wang, Jing;Ryu, Seung Kon;Jin, Ri-Guang
    • Carbon letters
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    • 제13권3호
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    • pp.133-138
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    • 2012
  • According to kinetic mechanisms, liquid phase polymerization and solid phase polymerization are different in acrylonitrile (AN) polymerization, and so the relationship between the contribution ratio and molecular weight distribution (MWD) was obtained through theoretic analysis. The precipitation homopolymerization of AN was carried out in a mixture solution of dimethyl sulfoxide (DMSO) and water at $50{\sim}65^{\circ}C$ using ${\alpha}$,${\alpha}^{\prime}$-azobisisobutyronitrile as an initiator. The contribution ratio decreased and approached 0; the MWD also decreased and approached 2 with the increase of the $H_2O$/DMSO ratio from 10/90 to 90/10. The experimental data were found to coincide well with the theoretical equation derived from the mechanisms.