• Title/Summary/Keyword: solid contents

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Study on Electrochemical Performances of PEO-based Composite Electrolyte by Contents of Oxide Solid Electrolyte (산화물계 고체전해질 함량에 따른 PEO 기반 복합전해질 전기화학 성능 연구)

  • Lee, Myeong Ju;Kim, Ju Young;Oh, Jimin;Kim, Ju Mi;Kim, Kwang Man;Lee, Young-Gi;Shin, Dong Ok
    • Journal of the Korean Electrochemical Society
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    • v.21 no.4
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    • pp.80-87
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    • 2018
  • Safety issues in Li-ion battery system have been prime concerns, as demands for power supply device applicable to wearable device, electrical vehicles and energy storage system have increased. To solve safety problems, promising strategy is to replace organic liquid electrolyte with non-flammable solid electrolyte, leading to the development of all-solid-state battery. However, relative low conductivity and high resistance from rigid solid-solid interface hinder a wide application of solid electrolyte. Composite electrolytes composed of organic and inorganic parts could be alternative solution, which in turn bring about the increase of conductivity and conformal contact at physically rough interfaces. In our study, composite electrolytes were prepared by combining poly(ethylene oxide)(PEO) and $Li_7La_3Zr_2O_{12}$ (LLZO). The crystallinity, morphology and electrochemical performances were investigated with the control of LLZO contents from 0 wt% to 50 wt%. From the results, it is concluded that optimum content and uniform dispersion of LLZO in polymer matrix are significant to improve overall conductivity of composite electrolyte.

Preparation of PVDF Membrane by Thermally-Induced Phase Separation

  • Heo, Chi-Haeng;Lee, Kyung-Mo;Kim, Jin-Ho;Kim, Sung-Soo
    • Korean Membrane Journal
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    • v.9 no.1
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    • pp.27-33
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    • 2007
  • PVDF membrane formation via TIPS was performed for PVDF/DBP and PVDF/DMP systems. PVDF/DBP system showed solid-liquid phase separation behavior, while PVDF/DMP system has liquid-liquid phase separation characteristic as well as solid-liquid phase separation characteristic. PVDF contents and cooling conditions had great influence on structure, and the effects of each parameter were examined. Spherulitic structure was obtained due to the dominant PVDF crystallization. Diluent rejected to the outside of spherulite occupied the surface of the PVDF spherulites to result in the microporous spherulite formation and micro-void between spherulites. PVDF/DMP system had competitive solid-liquid and liquid-liquid phase separation depending on the cooling path.

Energy Savings and Strength Improvement of Old Corrugated Container by Application of Wood Flour and Starch (목분과 전분을 이용한 골판지원지의 건조효율 및 물성향상)

  • Seo, Yung Bum;Jung, Jae Gwon;Ji, Sung Gil
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.2
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    • pp.99-105
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    • 2016
  • The increase of wet web solid content after wet press and dry compressive strength were observed in lab study by judicious application of wood flour and starch for the old corrugated container (OCC). Pearl starch was better than cationic starch in strength development, but cationic starch was better for drainage. Application of vacuum on the mixed solution of wood flour and starch helped strength development further without loss of other properties. The effect of wood flour addition on wet web solid content improved as the wet pressing pressure increased. The use of wood flour and starch mixture improved wet web solid contents further.

A Study on the Synthesis of Rutile - Type Ceramic Pigments (Rutile계 안료의 합성에 관한 연구)

  • Eo, Hye-Jin;Lee, Byung-Ha
    • Journal of the Korean Ceramic Society
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    • v.48 no.2
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    • pp.178-182
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    • 2011
  • The Rutile - type brown pigments doped with chromium were synthesized. Samples of $Ti_{1-x}Cr_xO_2$ ($0.02{\leq}X{\leq}0.08$) were synthesized by the solid state method. Solid solution limit of Cr contents to the rutile structure and its coloration were studied. Optimum composition was investigated accordingly. The characteristics of synthesized pigments were analyzed by XRD, SEM, Raman spectroscopy and UV. As a result, single phase of Rutile was observed from $1000^{\circ}C$ by XRD. The maximum limit of solid solution was 0.06 mole $Cr_2O_3$. The glazed sample showed brown color, and the value of CIE $L^*a^*b^*$ was $L^*$ 33.27, $a^*$ 10.64, $b^*$ 20.84.

Headspace-Solid Phase Microextraction (HS-SPME) Analysis of Korean Fermented Soybean Pastes

  • Lee, Seung-Joo
    • Food Science and Biotechnology
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    • v.18 no.3
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    • pp.700-705
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    • 2009
  • In this study, the volatile compounds in 9 commercial fermented soybean pastes were extracted and analyzed by headspace-solid phase microextraction (HS-SPME) and gas chromatography-mass spectrometry (GC-MS), respectively. A total of 63 volatile components, including 21 esters, 7 alcohols, 7 acids, 8 pyrazines, 5 volatile phenols, 3 ketones, 6 aldehydes, and 6 miscellaneous compounds, were identified. Esters, acids, and pyrazines were the largest groups among the quantified volatiles. About 50% of the total quantified volatile material was contributed by 5 compounds in 9 soybean paste samples; ethyl hexadecanoate, acetic acid, butanoic acid, 2/3-methyl butanoic acid, and tetramethyl-pyrazine. Three samples (CJW, SIN, and HAE) made by Aspergillus oryzae inoculation showed similar volatile patterns as shown in principal component analyses to GC-MS data sets, which showed higher levels in ethyl esters and 2-methoxy-4-vinylphenol. Traditional fermented soybean pastes showed overall higher levels in pyrazines and acids contents.

Optimization of the Spreadable Modified Butter Manufacturing by Response Surface Methodology

  • Suh, Mun Hui;Lee, Keon Bong;Baick, Seung Chun
    • Food Science of Animal Resources
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    • v.32 no.6
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    • pp.783-788
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    • 2012
  • The aim of this study was to optimize the manufacturing condition of spreadable modified butter by RSM. Based on the central composite design, the degree of optimization was expressed as a SFC as a dependent variable (Y, %) determined by NMR with 23 experimental groups. Three independent variables were the contents of butter ($X_1$, 35-75%), the contents of grape seed oil ($X_2$, 15-35%), and the contents of hydrogenated soybean oil ($X_3$, 0-4%). As the result, SFC at $10^{\circ}C$ was ranged from 32.37 to 42.76%. In addition, the regression coefficients were calculated for SFC at $10^{\circ}C$ by RSREG. The regression model equation for the SFC was $Y=39.18-0.04X_1X_3$. Consequently, the optimal contents for manufacturing spreadable modified butter were determined as 55.18% for butter, 40.78% for grape seed oil, and 4.08% for hydrogenated soybean oil, respectively. The predicted response value for SFC at $10^{\circ}C$ was 30.20%, comparable to the actual experimental SFC value as 29.85%. Finally hardness and spreadability in reference butter and spreadable modified butter produced under the optimal conditions was measured. The hardness in spreadable modified butter was 31.80 N as compared to 69.92 N in reference butter. The spreadability in spreadable modified butter was 5.6 point as compared to reference butter. This difference may be due to the contents of solid fat by butter and hydrogenated soybean oil. This study showed that the SFC value at $10^{\circ}C$ could be a suitable indicator for the manufacturing spreadable modified butter to predict important attributes such as mouth feel, hardness and spreadability.

The Effects of Skin Contact Time and Suspended Solid on The White Wine Quality (Skin Contact와 Suspended Solid가 백포도주 품질에 미치는 영향)

  • Rho, Tae-Uk;Kim, Chanjo;Sung, Chang;Moon, Youngja;Kim, Bong-Nan;Oh, Manjin
    • Korean Journal of Agricultural Science
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    • v.24 no.2
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    • pp.290-297
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    • 1997
  • Danored is considered as the most favorable grape variety for national wine manufacturing in terms of sugar, organic acid contents, annual production amount, as well as quality control convenience after harvest. This study was canied out to know the influence of suspended solid(SS) and skin contact time(SCT) with Danored variety on the white wine quality. The results are summarized as follows; 1. Suspended solid and skin contact time did not greatly influence on the chemical composition of Danored juice. But skin contact time provided slightly increaseness to the content of phenol compounds 2. Suspended solid accelerated fermentation rate of white wine manufacturing. Although the content of suspended solid are less amount than 0.3% in must, wine fermentation was completed to dryness in concentration of sugar. 3. When the content of suspended solid was around 3%, higher alcohol in white wine was increased by the 20%. This result is relatively small increasement compared to the other reported results. 4. Because Danored contained less amount of phenol compounds comparison with other grape varieties, browning capacity in white wine was much favorable to quite low concentration. Especially, phenolic compounds was decreased remarkably as one of fermentation characteristics of Danored variety. 5. As a result of sensory evaluation, wine quality was A-1> B-1> A-2> B-2 in its favorable ranking orders. It was so concluded that A-1 might be the most acceptable one from this study.

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Effect of Mo and Cu Contents on Work Hardening of Cold Drawn Stainless Steel 304H Wires for Spring (스프링용 스테인레스강 304H 신선재의 가공경화에 미치는 Mo와 Cu 농도의 영향)

  • Kim S. W.
    • Korean Journal of Materials Research
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    • v.15 no.10
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    • pp.632-638
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    • 2005
  • To investigate the effect of Mo and Cu contents on tensile strength of cold drawn stainless steel 304H wires, metallographical and mechanical tests were performed for the wire specimens drawn to different drawing strains at room temperature. It was confirmed that the contents of Mo ana Cu have little influence on the tensile strength of drawn specimens, even though the strain induced martensite transformation decreased with increasing the contents of Mo and Cu. These results were explained by the strengthening of the formed martensite itself due to the solid solution effect of interstitial solutes, carbon and nitrogen. The contents of these elements were slightly higher in the specimens containing additionally added Mo and Cu.

Fabrication and Mechanical Properties of Powder Metallurgical High Speed Steels with Various Co Contents (Co 함량이 다른 분말고속도공구강의 제조 및 기계적 특성)

  • 홍성현;배종수;김용진
    • Journal of Powder Materials
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    • v.9 no.5
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    • pp.303-306
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    • 2002
  • P/M high speed steels with various Co contents were fabricated by gas atomization and Canning/HIP process. As Co content in P/M high speed steel increased, hardness, transverse rupture strength and yield strength in compressive testing increased due to solid solution hardening of Co in matrix. Especially, PM high speed steels with Co have high deformation resistance to repeated compressive loading.

An Analysis on the Variation of the Solid State Wastes Generation of Local Government (지자체별 폐기물 처리 실적 변화 추이 분석)

  • Kim, Jaehee
    • Proceedings of the Korea Contents Association Conference
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    • 2017.05a
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    • pp.117-118
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    • 2017
  • 산업화에 따른 대량생산, 그리고 소비 증가 및 일회용 생활양식 등으로 인해 생활 폐기물의 발생량이 증가하고 있다. 그리고 발생되는 폐기물의 종류도 매우 다양해지고 있다. 또한 환경에 대한 관심이 높아짐에 따라 추가 매립지의 확보가 현실적으로 어려워지고 있어, 매립위주 정책에서 벗어나 소각, 재활용 등에 대한 요구가 커지고 있다. 이런 배경에서 실제 지자체 폐기물 처리실적의 변화 추이를 분석함으로써 각 지자체가 변화하는 폐기물 처리 정책에 적절히 대응하고 있는 지를 파악하고자 하였다.

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