• Title/Summary/Keyword: solid

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Assessment of mechanical Properties of Thixotropic Al-Si Materials in Semi-Solid Forming Process (반용융 성형공정에서 Thixotropic Al-Si 소재의 기계적 성질 평가)

  • 허재찬
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2000.04a
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    • pp.56-62
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    • 2000
  • Semi-solid forming process has some advantages such as successful manufacturing of high quality components with less inner defects suitable for less machining high productivity and energy-saving effect. the thixotropic behavior(solid-like in the unperturbed state and liquid-like during shearing) has been the basis for the semi-solid forming process. The main focus of this article is the investigation of the effect of T6 heat treatment and alloying elements on the mechanical properties in the semi-solid formed products using thixotropic hypoeutectic (A357 and ALTHIX 86S) and hypereutectic(A390) materials. The new methods to produce semi-solid formed components with high quality are also proposed and discussed in terms of a die design and the development of a lubricant.

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A Study on the Analytical Methods Using Solid-phase Extraction for the Determination of Phenols in Water

  • Jeon, Chi-Wan;Lee, Jung-Hwa;Lee, Sang-Hak
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11a
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    • pp.135-138
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    • 2003
  • Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

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Solid medium integrated impedimetric biosensor for detection of microorganisms (미생물 검침을 위한 고체 배지 임피던스 센서)

  • Choi, Ah-Mi;Park, Jae-Sung;Jung, Hyo-Il
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1629-1632
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    • 2008
  • Rapid, real-time detection of pathogenic microorganisms is an emerging and quickly evolving field of research, especially with regard to microorganisms that pose a major threat to public health. Herein, a new method that uses bioimpedance and solid culture medium for the real-time detection of microorganisms is introduced. We fabricated a new impedimetric biosensor by integrating solid media and two plane electrodes attached on two facing sides of an acryl well. During bioelectrical impedance analysis, the solid medium showed the characteristics of a homogenous conductive material. In a real-time impedance measurement, our solid-medium biosensor could monitor bacterial growth in situ with a detection time of ${\sim}4$ hrs. Our data indicate that the solid-medium biosensor is useful for detecting airborne microorganisms, thereby providing a new analytical tool for impedance microbiology.

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A FE-simulation for forming process of semi-solid material considering induction heating (유도가열을 고려한 반용융 재료의 성형공정에 관한 유한요소 시뮬레이션)

  • 최원도;고대철;김병민;최재찬
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1996.11a
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    • pp.110-114
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    • 1996
  • The objective of this study is to consider the induction heating process and to develop the finite element program to analyze the behaviour of semi-solid materials. The semi-solid material is assumed to be composed of solid region as rigid visco-plastic model and liquid region following Darcy's law. Induction heating process is analyzed using finite element software, ANSYS, and also the behaviour of a semi-solid material considering induction heating is analyzed using developed finite element program.

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Solid and Papillary Cystic Neoplasm of Pancreas in Children (소아에서 발생한 췌장의 유두상 낭성 종양 2예)

  • Choi, Sung-Il;Oh, Soo-Myung
    • Advances in pediatric surgery
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    • v.6 no.2
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    • pp.134-138
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    • 2000
  • Solid and papillary cystic neoplasm of pancreas is an uncommon low grade malignant tumor. It is predominant in young female between the second and third decades of life, and amenable to cure by surgical treatment. The authors report two cases of solid and papillary neoplasm of pancreas pathologically verified at Kyung Hee University Hospital. The first case was an 11-years old female patient and the other case was a 12-years old male. Symptoms were abdominal discomfort, nausea and vomiting in both cases and abdominal pain in the female patient. CT finding included a solid and papillary neoplasm of pancreas. The mass was well-demarcated with solid and cystic necrosis components. In the female patient, a large hematoma was found. Gross findings revealed apparent encapsulation, cystic degeneration and hemorrhagic necrosis. Microscopically the tumors were characterized by distinctive solid and papillary patterns of cellular arrangement without local invasion. Both patients were discharged after surgery and followed up without any problem.

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Solid-state Chracterization of the HIV Protease Inhibitor

  • Kim, Yong-Ae;Kim, Ae-Ri
    • Bulletin of the Korean Chemical Society
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    • v.23 no.12
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    • pp.1729-1732
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    • 2002
  • The LB71350,(3S, 4R)-Epoxy-(5S)-[[N-(1-methylethoxy)carbonyl]-3-(methylsulfonyl)-L-valinyl]amino]-N-[2-methyl-(1R)-[(phenyl)carbonylpropyl-6-phenylhexanamide, is a novel HIV protease inhibitor. Its equilibrium solubility at room temperature was less than $40{\mu}g/mL.$ It was speculated that the low aqueous solubility might be due to the high crystalline lattice energy resulting from intermolecular hydrogen bonds. The present study was carried out to learn the solid-state characteristics of LB71350 using analytical methods such as NMR, FT-IR and XRD. $^{13}C$ Solid-state NMR, solution NMR, and FT-IR spectra of the various solid forms of LB71350 were used to identify the conformation and structure of the solid forms. The chemical shifts of $^{13}C$ solid-state NMR spectra suggest that the crystalline form might have 3 intermolecular hydrogen bondings between monomers.

Sampling Methods for Quantification of Solid-state Phases in Powder Samples with Solid-state NMR Spectroscopy

  • Han, Oc-Hee;Kim, Sun-Ha;Ko, Tae-Jung
    • Bulletin of the Korean Chemical Society
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    • v.30 no.5
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    • pp.1077-1079
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    • 2009
  • To minimize the variance in the quantification of solid-state phases in powder samples, gently placing polycrystalline samples one next to another directly in a sample holder is better than trying to mix them homogeneously prior to transferring to a sample holder. However, the solid-state cross polarization-magic angle spinning (CP-MAS) nuclear magnetic resonance (NMR) spectroscopy results demonstrated that it is essential in this sampling method to place all the samples in the location of consistent signal sensitivity. The same sampling method may be employed in other spectroscopic quantification techniques of solid-state phases if the method to limit the sample to the location with uniform signal sensitivity in the sample holder is adapted to each technique.

Development of Components in Micro Solid Propellant Thruster. (마이크로 고체 추진제 추력기의 요소 개발)

  • 이종광;이대훈;권세진
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2003.05a
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    • pp.147-150
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    • 2003
  • The purpose of this research was to develope components of micro solid propellant thruster. Micro solid propellant thruster had four basic components: combustion chamber, nozzle, solid propellant and micro heater for ignition. A performance of micro heater and characteristic of solid propellant was investigated. Micro heater was fabricated by conventional MEMS process and Platinum layer was used for heating element. Effect of geometry parameters on micro heater was tested. The temperature responses of heater with respect to each parameters was compared for a given electrical power. The characteristic of solid propellant(HTPB/AP) was investigated to obtain burning velocity in small chamber. Additionally, a capacity of filling propellant with high viscosity in small chamber was checked to guarantee for the micro fabrication.

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Performance Evaluation of Components of Micro Solid Propellant Thruster (마이크로 고체 추진제 추력기 요소의 성능 평가)

  • Lee, Jong-Kwang;Lee, Dae-Hoon;Kwon, Se-Jin
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1280-1285
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    • 2004
  • Microsystem technology has been applied to space technology and became one of the enabling technology by which low cost and high efficiency are achievable. Micro propulsion system is a key technology in the miniature satellite because micro satellite requires very small and precise thrust force for maneuvering and attitude control. In this paper research on micro solid propellant thruster is reported. Micro solid propellant thruster has four basic components; micro combustion chamber, micro nozzle, solid propellant and micro igniter. In this research igniter, solid propellant and combustion chamber are focused. Micro igniter was fabricated through typical micromachining and evaluated. The characteristic of solid propellant was investigated to observe burning characteristic and to obtain burning velocity. Change of thrust force and the amount of energy loss following scale down at micro combustion chamber were estimated by numerical simulation based on empirical data and through the calculation normalized specific impulses were compared to figure out the efficiency of combustion chamber.

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Welding analysis with linear solid-shell element (선형 Solid-shell 을 이용한 용접해석)

  • Choi, Kang-Hyouk;Kim, Ju-Wan;Im, Se-Young
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.728-732
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    • 2004
  • In the FE analysis of sheet metal forming, efficient results can be obtained by using shell elements rather than using solid elements. However, shell elements have some limitations to describe three-dimensional material laws. In the recent years, solid-shell element, which has only translational degree of freedom like solid element, has been presented. The assumed nature strain (ANS) and enhanced assumed strain (EAS) methods can be used to remove several solid-shell locking problems. In this paper, ANS method was used for diminish transverse shear locking and EAS method for thickness locking. Using the element, the steel pipe making process from flat plate analyzed effectively, which is including bending and welding.

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