• Title/Summary/Keyword: soil sample

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A Study on Disturbance Effect of Clay by Block Sampling (대형자연시료 채취를 통한 시료 교란도 분석에 관한 연구)

  • 신윤섭;김연정;김학중;김영웅
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.325-332
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    • 2003
  • In general, soil characteristics are estimated through the sample gathered by field boring without considering sample disturbance. However, soil characteristics must be changed by the degree of sample disturbance. Therefore it be need to estimate the soil characteristic considering sample disturbance which can be occurred by the change of stress condition, sampling technique and handling method. On this study, we analyzed the sample disturbance by using the methods of volume change, residual effective stress, elastic modulus and the curve of consolidation tests. In order to estimate the relationship between sample disturbance and soil characteristics, we used the piston sample and the block sample. As the results, it should be considered in design that the disturbance of the block sample, which affects the strength and compression properties of clay, is smaller than the disturbance of piston sample.

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Concentration Characteristics of PCBs in Pine Needle and Soil at Rural Area (교외지역에서 소나무 잎과 토양 중 PCBs의 농도 특성)

  • Shin Eun-Sang;Yeo Hyun-Gu
    • Journal of environmental and Sanitary engineering
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    • v.21 no.1 s.59
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    • pp.1-11
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    • 2006
  • This study was to investigate concentration characteristics of atmospheric PCBs in soil sample and pine needle at rural area. Profiles of PCB congener detected in pine needle and soil sample have a difference that low molecular PCBs mainly existed in pine needle, whereas high molecular PCBs were mainly existed in soil sample because of their different vapor pressure and octanol-air partitioning coefficient($K_{OA}$) of each congeners. Correlation coefficients(r) of PCB congeners simultaneously detected in soil and pine needle were significant (r>0.71, p<0.01), which showed that PCB congeners patterns of atmosphere could be estimated in using pine needle and soil sample indirectly. The contributions(%) of higher molecular PCBs(>penta-CB) to total PCBs in soil sample were higher than those of pine needle and the contribution of lower molecular PCBs(

Quantification of Uncertainty Associated with Soil Sampling and Its Reduction Approaches (토양오염도 평가시 시료채취 불확실성 정량화 및 저감방안)

  • Kim, Geonha
    • Journal of Soil and Groundwater Environment
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    • v.18 no.1
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    • pp.94-101
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    • 2013
  • It is well known that uncertainty associated with soil sampling is bigger than that with analysis. In this research, uncertainties for soil sampling when assessing TPH and BTEX concentration in soils were quantified based on actual field data. It is almost impossible to assess exact contamination of the site regardless how carefully devised for sampling. Uncertainties associated with sample reduction for further chemical analysis were quantified approximately 10 times larger than those associated with core sampling on site. Bigger uncertainties occur when contamination level is low, sample quantity is small, and soil particle is coarse. To minimize the uncertainties on field, homogenization of soil sample is necessary and its procedures are proposed in this research as well.

Effect of particle size and scanning cup type for near infrared reflection on the soil property measurement

  • Ryu, Kwan-Shig;Cho, Rae-Kwang;Park, Woo-Churl;Kim, Bok-Jin
    • Near Infrared Analysis
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    • v.1 no.2
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    • pp.35-39
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    • 2000
  • The purpose of this research was to find out suitable soil sample preparation and sample holding tools for NIR reflection radiation for estimating soil components. NIR reflectance was scanned at 2nm intervals from 1,100 to 2,500nm with an InfraAlyzer 500(Bran+Luebbe Co.). Coarse(2.0mm) and fine(0.5mm) soil sample and various sample holding tools were used to obtain mean diffuse reflection of the soil for the calibration and validation of the calibration set in estimating moisture, organic matter and total nitrogen of the soils. Multiple linear regression was used to obtain the best correlation of NIR spectroscopy method. Correlation of NIR spectroscopy method. Correlation of NIR spectra for finely and coarsely sized soil did not show much difference. The standard errors of prediction(SE) using different types of sample holding tools for organic matter, total nitrogen and soil moisture were better than 0.765, 0.041 and 0.63% respectively. From the results it can be concluded that NIR spectroscopy with flow type cell could be used as a fast routine testing method in quantitative determination of organic matter, total nitrogen and soil moisture.

Significant Parameters for Assessing Soil Contaminant-Leaching to Groundwater and Determining Soil Sample Size in Field Survey

  • Jeong, Seung-Woo;An, Youn-Joo
    • Environmental Engineering Research
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    • v.13 no.2
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    • pp.73-78
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    • 2008
  • For a given soil-contaminated site, a level of soil contamination is characterized and decisions on risk may be made from the risk assessment. The study evaluated critical design factors for the determination of sample size in the sampling design plan and the assessment of soil contaminant- leaching to groundwater. Two variables, the minimum relative detectable difference (T) and coefficient of variation (CV) were evaluated for the sample size determination. The minimum number of samples can be appropriately determined by CV under a T value greater than or equal to 0.2. Soil-contaminant leaching to groundwater was evaluated by using the Soil Screening Level equation of U.S. Environmental Protection Agency and the Risk Based Screening Level equation of American Society for Testing and Materials, with the same input parameters. The groundwater concentrations estimated from soil contaminant concentrations were significantly affected by the Darcy velocity of groundwater and the organic content of soil.

Soil sampling plan design of key facilities for denuclearization based on data quality objective process

  • Jeon, Yeoryeong;Kim, Yongmin
    • Nuclear Engineering and Technology
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    • v.54 no.10
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    • pp.3788-3794
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    • 2022
  • The possibility of denuclearization of the Korean Peninsula has been continuously debated, and the initiative participation of the Republic of Korea has necessitated preemptive measures against neighboring countries. In this study, we present a proposal for formulating a site survey plan when the amount of site information provided is insufficient and the accuracy of the information is not guaranteed. Considering a case wherein "a soil sample analysis is used to determine the presence or absence of nuclear activity" in a radiochemical laboratory, which is a typical key facility for denuclearization, the optimal soil sample collection plan is designed based on international guidelines and public information. In the event of denuclearization, a scenario that is not based on the expertise of the sample collector is set, and the data quality objective (DQO) process is applied to ensure reality. Consequently, the primary sample collection points can be derived in consideration of accessibility, and the sample collection scale can be adjusted according to the cost. By applying the DQO process to ensure sample representativeness and reality, reliable and resource-efficient soil sample collection can be achieved in radiochemical laboratories and other denuclearization facilities.

Evaluation of Dynamic Properties of Subballast Materials Used in Korea Using Midsize Resonant Column Test Apparatus (중형 공진주 시험기를 이용한 보조도상 재료의 동적특성 정량화)

  • Lim, Yu-Jin;Sin, Joong-Hoon;Park, Kyung-Su;Park, Jae-Hak;Hwang, Jung-Kyu
    • Proceedings of the KSR Conference
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    • 2011.05a
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    • pp.1214-1221
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    • 2011
  • It is an well-known fact that dynamic properties should be considered in design and maintenance of civil structures undergoing dynamic force such as rail track. For designing of the rail tack structures, dynamic properties of track bed soil such as shear modulus (G) and damping coefficients(D) obtained in small to medium range of shear strain must be known. In general, small size sample of D=5 cm and H=10cm has been used mostly for test convenience. However, ratio of largest particle diameter of the soil to sample diameter is very important and affects to the values of dynamic soil properties in track bed. In this study, an RC/TS test apparatus was built and was run for testing a medium size soil sample that can handle with compacted soil sample up to 10 cm diameter and 20 cm height.

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$KMnO_4$를 이용한 TCE 제거 실험 연구(I): -Headspace sample과 liquid sample 분석과 비교-

  • 현승규;우남칠;최인혁;이기철
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.04a
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    • pp.370-375
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    • 2004
  • KMnO$_4$에 의한 TCE 용액의 분해에서 Headspace를 가진 반응 용기는 liquid sample을 headspce의 관측값으로 반응의 특성을 나타낼 수 없다. 이런 특성에 의해 in-situ KMnO$_4$ 이용은 TCE의 제거 효율에서 자연적인 휘발을 고려해야한다. 1:2.45 몰비에서 liquid sample의 결과 반감기는 약 80분이고 160분에 약 67%의 제거율을 보인다. 1:12.27 몰비의 경우 반감기는 10분이고 90분에 95%의 제거효율을 보인다.

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Amelioration of Soil Acidified by Air Pollutant around the Industrial Complexes (대기오염으로 산상화된 공업단지 주변 토양의 개량)

  • 이창석;김진영;유영한
    • The Korean Journal of Ecology
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    • v.21 no.3
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    • pp.313-320
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    • 1998
  • Ameliorating effects of dolomite and sludge on the polluted soil sampled from Ulsan and yeocheon Industrial Complexes were investigated. Ameliorating effects were analysed by changes of soil properties and plant growth after treatment of dolomite and sludge. Soil properties were investigated by analysing organic matter, N, P, K, Ca and Mg contents and pH. Growth of sample plants was investigated by leaf area calculated from length and breadth of leaves and by biomass from diameter and height of sample plants. Quercus serrata and Celtis sinensis selected as tolerant plants in field survey were used as experimental plants. Treatment with dolomite showed ameliorating effects by increassing n, Ca, and Mg com\ntents, and pH of soil and by decreasing Al content. Treatment of sludge showed similar effects by increasing N, Ca, Mg and organic matter contents, and by decreasing A1 content. But treatment of sludge did not show any effect on pH. Both soil ameliorators showed accelerating effects on the growth of experimental plants in Ulsan soil. But those effects in Yeocheon soil were somewhat different. Treatment of sludge showed accelerating effects of the growth of both sample plants but dolomitic liming did not so. From those results, we confirmed availability of sludge, a kind of industrial waste, as one of ameliorators of the polluted soil. In addition, we recognized that soil properties had to be considered to select soil ameliorators suitable for restoration of degraded ecosystems.

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GC-MS/Ms Analysis of Benzo(a)pyrene by Ion Trap Tandem Mass Spectrometry

  • Nam, Jae-Jak;Lee, Sang-Hak
    • Bulletin of the Korean Chemical Society
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    • v.23 no.8
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    • pp.1097-1102
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    • 2002
  • The mass spectrometry using an ion trap tandem mass spectrometer has been investigated to find optimum conditions for the analysis of benzo(a)pyrene (3,4-benzpyrene). The applicability to a real soil sample was also investigated to verify the usef ulness of the MS/MS (or collision induced dissociation, CID) analysis. The optimum CID condition was 1.5 and 0.45 for the RF excitation voltage and the q value, respectively. For comparison, CID and EI were applied to the analysis of a soil sample. CID analysis was more sensitive than EI analysis of the soil sample. The limit of detection (LOD) of benzo(a)pyrene was 3.18 ng mL-1 and 0.85 ng mL,-1 for EI and MS/MS analysis, respectively. The precision at the soil sample for EI and CID showed relative standard deviations of 6.1% and 4.1%, respectively, and the concentrations were 168 ㎍ kg-1 and 162 ㎍ kg-1 , respectively.